This article describes a high-efficiency experimental configuration for a self-referenced lattice comparator with a `brush beam' of synchrotron radiation from a bending magnet and two linear position-sensitive photon-counting-type X-ray detectors. The efficiency is more than ten times greater compared with the `pencil-beam' configuration and a pair of zero-dimensional detectors. A solution for correcting the systematic deviation of d-spacing measurements caused by the horizontal non-uniformity of the brush beam is provided. Also, the use of photon-counting-type one-dimensional detectors not only improves the spatial resolution of the measurements remarkably but can also adjust the sample's attitude angles easily.

The title compound, C11H11NO5, has a nearly planar geometry. In the crystal, the molecules are assembled into chains parallel to the [overline{1}11] direction by O—H...O and C—H...O hydrogen bonds.

Insights were obtained into the structure of the 4-hydroxy-tetrahydrodipicolinate synthase from the thermoacidophilic methanotroph Methylacidiphilum fumariolicum SolV and the phylogeny of the aminotransferase pathway for the biosynthesis of lysine.

In southeastern Greenland, two rivers of ice named Helheim and Kangerdlugssuaq flow in spurts and starts toward the coast. They are much like any other […]

The post Astrophysical Observatory scientists are monitoring the mysterious movements of glaciers appeared first on Smithsonian Insider.

Already under siege from overfishing, disease and poor water quality, the oyster population in the Chesapeake Bay today stands at 2 percent of what it was in colonial times. Now, new data show that rising acidity in the Bay will have a negative impact on oyster shells.

The post Rising acidification of estuary waters spells trouble for Chesapeake Bay oysters appeared first on Smithsonian Insider.

A recent experiment by scientists at the Smithsonian Tropical Research Institute in Panama has revealed just how rising atmospheric carbon dioxide will deliver a one-two […]

The post Rising ocean temperatures and acidity may deliver deadly one-two punch to the world’s corals appeared first on Smithsonian Insider.

A team of scientists from the Smithsonian Environmental Research Center in Edgewater, Md., is taking a closer look at how rising acidification of ocean water may be impacting estuaries and near shore environments on the Chesapeake Bay

The post Oysters on floating plates help scientists study acidification and shell growth appeared first on Smithsonian Insider.

Looking at more than 200 skulls dating to 20th and 16th century Spain, as well as approximately 50 skulls from 20th century Portugal, the researchers found that craniofacial differences between contemporary men and women are less pronounced than they were in the 16th century.

The post Study finds facial structure of men and women has become more similar over time appeared first on Smithsonian Insider.

The Smithsonian Tropical Research Institute has released the first completely portable bilingual species identification guide for the shore fishes of the tropical Eastern Pacific as a free iPhone application.

The post First fish App from the Smithsonian free on iTunes. “The Smithsonian Guide to the Shore Fishes of the Tropical Eastern Pacific” appeared first on Smithsonian Insider.

Two new species of blind snakes found living on small, low-lying atolls in the Caroline Islands, are an unexpected discovery that is quite difficult to explain,

The post Not on a plane, but how did blind snakes ever get to the Pacific’s Caroline Islands? appeared first on Smithsonian Insider.

The Smithsonian-Mason School of Conservation, a unique program in terms of its academic offerings and contributions to the field of conservation, celebrated the completion of its expansive new academic facilities today, Oct. 18, at the Smithsonian Conservation Biology Institute in Front Royal, Va.

The post Smithsonian Conservation Biology Institute and George Mason University dedicate new academic facilities in Front Royal, Va. appeared first on Smithsonian Insider.

A new coral species, Psammogorgia hookeri, has been collected by scuba divers from rocky ledges at depths to 25 meters in Peru’s Paracas National Reserve. The […]

The post Fiery-red coral species discovered in the Peruvian Pacific appeared first on Smithsonian Insider.

Eaten raw and thinly sliced, the dark-red belly meat of the Pacific bluefin tuna is highly prized—and priced—for its rich oily flavor by sashimi and […]

The post Desire for Pacific bluefin puts fish on red list of threatened species appeared first on Smithsonian Insider.

Higher acidity in coastal waters can make fish more sensitive to low oxygen, causing them to become debilitated and suffocate in water with oxygen levels […]

The post Acidification, Low Oxygen Can be Deadly Combination for Fish appeared first on Smithsonian Insider.

Whales from both poles migrate long distances to breed in tropical waters. Smithsonian scientist Hector M. Guzman and Fernando Félix at the Salinas Whale Museum […]

The post Whale tagging in Southeast Pacific provides data for species protection appeared first on Smithsonian Insider.

Marine mammologist Matthew Leslie aims his crossbow from the bow of a moving boat at the dolphins riding the breaking waves below. A dolphin will […]

The post Some dolphins cross the Pacific more easily than others. Why that matters for protecting them appeared first on Smithsonian Insider.

When the heat and humidity of the Washington, D.C. summer sends its residents scrambling for air conditioning and iced coffee, the animal care specialists at […]

The post How do National Zoo animals beat the heat? Bloodsicles and other frozen delicacies appeared first on Smithsonian Insider.

Pullulanase (EC 3.2.1.41) is a well known starch-debranching enzyme that catalyzes the cleavage of α-1,6-glycosidic linkages in α-glucans such as starch and pullulan. Crystal structures of a type I pullulanase from Paenibacillus barengoltzii (PbPulA) and of PbPulA in complex with maltopentaose (G5), maltohexaose (G6)/α-cyclodextrin (α-CD) and β-cyclodextrin (β-CD) were determined in order to better understand substrate binding to this enzyme. PbPulA belongs to glycoside hydrolase (GH) family 13 subfamily 14 and is composed of three domains (CBM48, A and C). Three carbohydrate-binding sites identified in PbPulA were located in CBM48, near the active site and in domain C, respectively. The binding site in CBM48 was specific for β-CD, while that in domain C has not been reported for other pullulanases. The domain C binding site had higher affinity for α-CD than for G6; a small motif (FGGEH) seemed to be one of the major determinants for carbohydrate binding in this domain. Structure-based mutations of several surface-exposed aromatic residues in CBM48 and domain C had a debilitating effect on the activity of the enzyme. These results suggest that both CBM48 and domain C play a role in binding substrates. The crystal forms described contribute to the understanding of pullulanase domain–carbohydrate interactions.

Don your clean room clothing and take a glimpse into the Smithsonian's new Antarctic meteorite storage facility in Suitland, Md., where all of the Antarctic meteorites in the national collection are kept under tight security and tight airlocks.

The post Glimpse into the Smithsonian National Museum of Natural History’s new meteorite storage facility appeared first on Smithsonian Insider.

The post Indo-Pacific lionfish, an invasive species, invade the Atlantic appeared first on Smithsonian Insider.

Smithsonian Tropical Research Institute MarineGEO Postdoctoral Fellow Maggie Johnnson outlines her research studying the effects of ocean acidification on marine coral near Bocas del Toro, […]

The post Coral reefs and ocean acidification appeared first on Smithsonian Insider.

What plant species has just been discovered but is almost gone? Bidens meyeri–a just discovered flowering plant from the small South Pacific island of Rapa, […]

The post New South Pacific cliff flower is critically endangered appeared first on Smithsonian Insider.

The crystal structures of caesium di­hydrogen arsenate(V) bis­[tri­hydrogen arsen­ate(V)], Cs(H2AsO4)(H3AsO4)2, ammonium di­hydrogen arsenate(V) tri­hydrogen arsenate(V), NH4(H2AsO4)(H3AsO4), and dilithium bis­(di­hydrogen phosphate), Li2(H2PO4)2, were solved from single-crystal X-ray diffraction data. NH4(H2AsO4)(H3AsO4), which was hydro­thermally synthesized (T = 493 K), is homeotypic with Rb(H2AsO4)(H3AsO4), while Cs(H2AsO4)(H3AsO4)2 crystallizes in a novel structure type and Li2(H2PO4)2 represents a new polymorph of this composition. The Cs and Li compounds grew at room temperature from highly acidic aqueous solutions. Li2(H2PO4)2 forms a three-dimensional (3D) framework of PO4 tetra­hedra sharing corners with Li2O6 dimers built of edge-sharing LiO4 groups, which is reinforced by hydrogen bonds. The two arsenate compounds are characterized by a 3D network of AsO4 groups that are connected solely via multiple strong hydrogen bonds. A statistical evaluation of the As—O bond lengths in singly, doubly and triply protonated AsO4 groups gave average values of 1.70 (2) Å for 199 As—OH bonds, 1.728 (19) Å for As—OH bonds in HAsO4 groups, 1.714 (12) Å for As—OH bonds in H2AsO4 groups and 1.694 (16) Å for As—OH bonds in H3AsO4 groups, and a grand mean value of 1.667 (18) Å for As—O bonds to nonprotonated O atoms.

The inversion of X-ray reflectivity to reveal the topography of a one-dimensional interface is evaluated through model calculations.

(The Paypers) SnapPay has announced the availability of facial recognition payment technology for North...

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The same artificial intelligence technique typically used in facial recognition systems could help improve prediction of hailstorms and their severity, according to a new, National Science Foundation-funded study. Instead of zeroing in on the features of an individual face, scientists trained a deep learning model called a convolutional neural network to recognize features of individual storms that affect the formation of hail and how large the hailstones will be, both of which are notoriously difficult to predict. The promising results highlight the importance of taking into account a storm's entire structure, something that's been challenging to do with existing hail-forecasting techniques.

Image credit: Carlye Calvin

The U.S. Department of Energy should place a higher priority on developing an accurate and actionable inventory of agency-owned or managed properties that can be leased or sold for energy development, says a new report from the National Academies of Sciences, Engineering, and Medicine.

A number of strategies used by the police to proactively prevent crimes have proved to be successful at crime reduction, at least in the short term, and most strategies do not harm communities’ attitudes toward police, finds a new report by the National Academies of Sciences, Engineering, and Medicine.

NASA’s investment in new instruments to analyze extraterrestrial samples is insufficient to provide for replacement of existing instruments, says a new report from the National Academies of Sciences, Engineering, and Medicine.

We tend to think of the process of seeing as fairly objective — that our eyes are similar to cameras, neutrally taking in light and turning it into pictures. But research has shown that biases buried beneath our awareness can powerfully shape how we see.

Rwanda’s Human Resources for Health (HRH) Program – funded in part by the U.S. President’s Emergency Plan for AIDS Relief (PEPFAR) from 2012 to 2017 – more than tripled the country’s physician specialist workforce and produced major increases in the numbers and qualifications of nurses and midwives, says a new report from the National Academies of Sciences, Engineering, and Medicine.

Research by NAM Pharmacy Fellow Dima M. Qato has shed light on “pharmacy deserts” and closures that reduce people’s access to medications.

Santa Monica Beach, a very wide, artificially built, and regularly maintained beach. Photographed on September 9, 2019 in Santa Monica, California.; Credit: James Bernal for KPCC

Jacob Margolis

You may not know this, but oftentimes in newsrooms we write obituaries ahead of time so that they're ready to publish when the person passes away. But what if the obit wasn't for a person, but for a place that's been the home of magical memories for generations?

Sea levels could rise by more than three feet by the end of the century, and that's going to mean many things you love about our coast are not going to be around much longer.

As part of our Covering Climate Now collaboration, we thought it was appropriate to start preparing an obit for one of Southern California's most prized areas of Pacific Coast Highway: Santa Monica to Malibu. 

It's slated to run in 80 years or so - the year 2100. 

This content is from Southern California Public Radio. View the original story at SCPR.org.

Researchers have found that ocean acidification leads to changes in the ways that clownfish normally respond to sound. As many species rely on hearing for orientation, habitat selection, avoiding predators and communication, ocean acidification could compromise auditory behaviour crucial for survival.

A recent study has investigated how waste disposal sites in southern Italy have affected residents living nearby. Villagers reported being annoyed by odours, but the perceptions of residents living in the village closest to the facilities were possibly influenced by receiving financial compensation for the presence of the facilities.

Mediterranean red coral (Corallium rubrum), already endangered due to over-harvesting, is likely to suffer still further under increasing ocean acidification as a result of rising CO2 emissions. Research has shown that under more acidic conditions the structural development of red coral skeletons is abnormal and growth rate is reduced.

The most comprehensive glacier assessment yet reveals that glacier melt was responsible for 27mm of sea level rise between 1961 and 2016. Ice loss from glaciers is now the second biggest contributor to rising sea levels after warming water. If glaciers continue to melt at current rates, most — including many in central Asia, central Europe, western Canada and the USA — will vanish during the second half of this century.

A recent study has investigated how waste disposal sites in southern Italy have affected residents living nearby. Villagers reported being annoyed by odours, but the perceptions of residents living in the village closest to the facilities were possibly influenced by receiving financial compensation for the presence of the facilities.

Parts of Africa and the Asia-Pacific region may be vulnerable to outbreaks of the Zika virus, including some of the world's most populous countries and many with limited resources to identify and respond to the mosquito-borne disease, a new study says.

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