New J. Chem., 2024, Accepted Manuscript
DOI: 10.1039/D4NJ00543K, Paper

Ragini Jain, Ravi Shankar
The study describes the synthesis of disiloxanes, R₃SiOSiR₃, tetraorganodisiloxanes-1,3-diols, (RR¹SiOH)₂O, and silanol, t-Bu₂Si(H)OH by AuNP-catalyzed hydrolytic oxidation of Si-H bond(s) in organosilanes. The method relies upon en route formation of...
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New J. Chem., 2024, Accepted Manuscript
DOI: 10.1039/D4NJ00463A, Paper

Priya Singh, Vijay K. Singh, Dipti Kakkar, Anjani Kumar Tiwari
The 18 kDa Translocator protein (TSPO) serves as a promising target for drug delivery and imaging applications. In this investigation, we have encapsulated MCBP, a TSPO compound based on acetamidobenzoxazolone,...
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New J. Chem., 2024, Accepted Manuscript
DOI: 10.1039/D4NJ00209A, Paper

Vu Ngoc Toan, Nguyen Dinh Thanh, Do Son Hai, Nguyen Minh Tri
A series of thioureas 7a-k containing pyrimidine and D-glucose moiety have been synthesized through the reaction between substituted 2-aminopyrimidines 3a-k and tetra-O-acetyl-β-D-glucopyranosyl isothiocyanate 6. The yields achieved were 55‒77%. The...
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New J. Chem., 2024, Accepted Manuscript
DOI: 10.1039/D3NJ05774G, Paper

Moaz M. Abdou, Essam Eliwa, Mohamed Abdel Reheim, Ahmed Abu-Rayyan, Shimaa M. Abd El-Gilil, Mohammed Abu-Elghait , Mohamed H. Sharaf, Mohamed Kalaba, Ahmed Halawa, Walid Elgammal
Herein, the chemical synthesis of new thiazoles-based benzenesulfonamide-linked morpholine 4a,b–7 via late-stage thiazolation of the corresponding thiosemicarbazone 3 was reported. The skeletal formulas of the new compounds were confirmed by...
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New J. Chem., 2024, 48,7235-7243
DOI: 10.1039/D4NJ00530A, Paper

Yiwen Dai, Bin Guan, Xingxiang Wang, Jiaqi Liu, Zehua Huang, Bin Dai, Jichang Liu, Jiangbing Li
In this study, a uniform micro/mesoporous core–shell composite HZSM-@MCM-41 comprising zeolite was successfully prepared by coating mesoporous MCM-41 shells on nanosized ZSM-5 cores using a two-step hydrothermal method.
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New J. Chem., 2024, 48,7265-7276
DOI: 10.1039/D4NJ00321G, Paper

Ashok Kumar, Kanchan Negi, Sumanta Kumar Sahu
This work describes the gram-scale synthesis of N/S-doped carbon dots for red emissive properties. The developed carbon dots can be used in WLEDs, fingerprinting, bioimaging, fluorescent ink, and room-temperature phosphorescence.
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New J. Chem., 2024, 48,7300-7307
DOI: 10.1039/D3NJ05843C, Paper

Chunxiong Lu, Dandan Zhu, Peng Zhou, Kangxia Yu, Yaling Liu, Hongyong Wang, Hao Wu, Jun Wu, Guoqing Han, Pei Zou
Illustration of [^99mTc]Tc-SG2C-CBM for imaging PD-L1.
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New J. Chem., 2024, 48,7308-7322
DOI: 10.1039/D3NJ05440C, Paper

Rimpa Mondal, Aratrika Chakraborty, Ennio Zangrando, Madhulata Shukla, Tanmay Chattopadhyay
The synthesis of a magnetically separable nanocatalyst Fe₃O₄@ISNA@CuL¹ used as a catalyst for oxidation of alcohols and reduction of nitrophenols.
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New J. Chem., 2024, 48,7125-7133
DOI: 10.1039/D4NJ00492B, Paper

Mengxiang Wu, Ling Chen, Xiaohan Yang, Yahong Li
Five magnesium compounds were synthesized. They are active precatalysts for the hydroboration of nitriles and alkynes. The catalytic reactions feature mild reaction conditions, excellent functional group tolerance, and high yields.
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New J. Chem., 2024, 48,7370-7378
DOI: 10.1039/D4NJ00389F, Paper

Yonghong Qin, Shahriman Zainal Abidin, Azhari Bin Md Hashim, Oskar Hasdinor Hassan, Xiaojun Zhao
Novel few-layered MoO₃–MoSe₂ encapsulated in a 3D NC skeleton is constructed to improve the electrochemical performances of SIBs.
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New J. Chem., 2024, 48,7356-7361
DOI: 10.1039/D4NJ00886C, Paper

Zefeng Li, Caihang Zhang, Yingxuan Zheng, Ping Deng, Yan Yu
The palladium-catalyzed solvent-free and ligand-free oxidative homocoupling reactions of aryl boronic acids via ball-milling are developed to synthesize a series of biphenyl-derived organic fluorescent materials.
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New J. Chem., 2024, 48,7517-7523
DOI: 10.1039/D4NJ00366G, Paper

Yijie Xiao, Lijie Lv, Nanxuan Luo, Peirui Zhao, Yao Chen, Zhangshun Luo, Houhua Yin, Yi He, Shenyou Nie
C(sp)–C(sp) cross-coupling of terminal alkynes represents a robust tool for building biologically active 1,3-diynes although confronted with huge challenges regarding selectivity control.
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New J. Chem., 2024, 48,7489-7496
DOI: 10.1039/D3NJ05757G, Paper

Peixue Wang, Shimin Liu, Xinjiang Cui, Yang Wu, Feng Shi
Effective synthesis of diethyl carbonate from ethyl carbamate and ethanol using Mg–Y composite oxides.
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New J. Chem., 2024, 48,7134-7147
DOI: 10.1039/D4NJ00430B, Paper

Iveta S. Turomsha, Maxim Y. Gvozdev, Nikolai P. Osipovich, Viktoryia A. Staravoitava, Dmitriy I. Shiman, Natalia V. Loginova
Phenolic Schiff bases and their Cu(II) complexes have been synthesized and characterized by physicochemical methods. The complexes exhibit low cell toxicity and high antioxidant and antibacterial activity, as evidenced by molecular docking studies.
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New J. Chem., 2024, Advance Article
DOI: 10.1039/D4NJ00995A, Paper

Marija Bakija, Berislav Perić, Srećko I. Kirin
Oxazoline amino acid bioconjugates were synthesized; the relative stability of a supramolecular dimer of a tris-derivative was investigated using mean absolute error values (MAE), derived from ¹H NMR experiments and DFT calculations.
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New J. Chem., 2024, Advance Article
DOI: 10.1039/D3NJ05813A, Paper

Zhuoran Yang, Yao Xu, Xiaoming Liao, Wenjun Wang, Chang Lyu, Xiaoxiang Zhang
Aryl amides were prepared through KOH-mediated [3+2] cycloaddition/Wolff rearrangement from organic azides and 1,3-dicarbonyl compounds.
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New J. Chem., 2024, Advance Article
DOI: 10.1039/D4NJ00447G, Paper

Kavyashree Kuppayya Gond, Mahagundappa Rachappa Maddani
Facile synthesis of spiro-pyrazolone-tetrahydrofurans & pyrans by base-mediated cascade ipso-cyclization of haloalcohols & arylidine pyrazolones is realised. Features include brief reaction time, practicality, good yields and mild reaction conditions.
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New J. Chem., 2024, Advance Article
DOI: 10.1039/D4NJ01034E, Paper

Yasmin Milena Loth Bueno, Filipe Kalil da Silva Naves, Tamires Pereira Rosa, Odivaldo Cambraia Alves, Marcel Guimarães Martins, Marla Karolyne dos Santos Horta, Giane Gonçalves Lenzi, Celio Lucas Valente Rodrigues, Jéssica Dornelas da Silva, Rodrigo Brackmann
This study aimed to synthesize magnetite nanoparticles proposing a new core with maltodextrin using the coprecipitation method in an alkaline medium, with the potential application in magnetic hyperthermia for cancer treatment.
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New J. Chem., 2024, Accepted Manuscript
DOI: 10.1039/D4NJ01321B, Paper

Zili Xu, Yuankang Bao, Xun Xu, Ping Li, Hao Zhang, Deliang Li, Shuwang Duo
Seawater, a plentiful natural resource, is promising for hydrogen production compared to traditional electrocatalytic methods based on high-purity freshwater. This strategy shift addresses the challenge of limited freshwater resources and...
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New J. Chem., 2024, Accepted Manuscript
DOI: 10.1039/D4NJ00563E, Paper

Sravanthi Baddepuri, G. Rama Krishna, Jyothi Kumari, Sriram Dharmarajan, Srinivas Basavoju
The aim of the study is to develop the synthesis of a novel series of potent anti-tubercular (anti-TB) activity of 1,3-diphenylpyrazole-based spirooxindolopyrrolizidine derivatives via an efficient green approach achieved by...
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Environ. Sci.: Nano, 2024, Advance Article
DOI: 10.1039/D3EN00978E, Paper

Lian Zhang, Xiaona Li, Le Yue, Xuesong Cao, Bingxu Cheng, Chuanxi Wang, Zhenyu Wang
Herein, the effect of selenium engineered nanomaterials (Se ENMs) on soybean photosynthesis and fatty-acid synthesis by regulating ferredoxin (Fd) and iron–sulfur (Fe/S) protein synthesis and acetyl CoA carboxylase (ACC) activity was explored.
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Environ. Sci.: Nano, 2024, Advance Article
DOI: 10.1039/D3EN00911D, Paper

Yang Luo, Hong Li, Hailan Yang, Zhiming Yang, Chuang Li, Shaoheng Liu, Qiang Chen, Weihua Xu, Wei Zhang, Xiaofei Tan
The critical role of dissolved oxygen and iron–copper synergy in dual-metal/char catalyst system was studied.
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Environ. Sci.: Nano, 2024, Accepted Manuscript
DOI: 10.1039/D3EN00827D, Communication

cheng chen, Yuchen Liu, Houpu Zhang, Jie Ren, Chao Zhang, Mao Xu, Dan Liu, Yuru Wang, Weiwei Lei, Xiaoli Zhao
As a thriving group of two-dimensional (2D) nanomaterials, MXenes offer tremendous application and development prospects because of their excellent physical and chemical properties. Rhizosphere bacteria colonize the narrow ecosystem region...
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Environ. Sci.: Nano, 2024, Accepted Manuscript
DOI: 10.1039/D3EN00859B, Paper

Open Access

  This article is licensed under a Creative Commons Attribution-NonCommercial 3.0 Unported Licence.

Andrea Muñoz-Garcia, Pablo Montoro Leal, María Mar López Guerrero, Carlos Vereda-Alonso, Elisa Vereda Alonso
Securing the enduring sustainability of global phosphorus (P) utilization has become a key societal priority. The application of green chemistry and green engineering presents an opportunity to mitigate these challenges...
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Environ. Sci.: Nano, 2024, 11,1636-1653
DOI: 10.1039/D3EN00789H, Paper

Ravi Pratap, Nurul Hassan, Monika Yadav, Saurabh Kumar Srivastava, Shilpi Chaudhary, Anita Kamra Verma, Jayeeta Lahiri, Avanish S. Parmar
Due to the excessive residues and serious adverse effects, it is urgent to develop an efficient method to detect Hg²⁺ and As³⁺ in drinking water to protect human health.
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CrystEngComm, 2024, 26,2009-2017
DOI: 10.1039/D4CE00096J, Paper

Yang Zhou, Dan Wang, Qiuxiang Feng, Qi Wu, Feng Cao, Li Jiang, Qianli Zhang, Jie Liu
Ce-UiO-66-NH₂ was synthesized in water and ethanol at room temperature for effective removal of MB in aqueous solution.
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CrystEngComm, 2024, Advance Article
DOI: 10.1039/D4CE00019F, Paper

Pinky Chauhan, Poornenth Pushpanandan, Mangalampalli Ravikanth
Bis(3-pyrrolyl BODIPY)s were used to prepare rare examples of hexapyrrolic ligands by demasking BF₂ units. The hexapyrrolic ligands, without isolating, were used to prepare novel examples of double-stranded bis-Zn(II) helicate complexes.
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CrystEngComm, 2024, Advance Article
DOI: 10.1039/D4CE00206G, Paper

Wen-Long Mou, Cheng-Jie Gao, Zi-Xi Li, Si-Jie Fan, Chuan-Bin Hou, Jing-Tong Zhao, Shuai Zhang, Zhong-Feng Li, Hong-Liang Han, Chun-Bo Duan, Guo Wang, Qiong-Hua Jin
High quantum yield (72–88%) yellow-emitting Cu(I) complexes obtained by tuning the nitrogen ligands and anions.
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CrystEngComm, 2024, Advance Article
DOI: 10.1039/D4CE00038B, Paper

Open Access

  This article is licensed under a Creative Commons Attribution 3.0 Unported Licence.

Edita Garskaite, Math Bollen, Enock Mulenga, Mathis Warlo, Glenn Bark, Espen Olsen, Dalia Brazinskiene, Denis Sokol, Dietrich Buck, Dick Sandberg
An affordable, scalable, and easily adoptable solution-based processing route provides a potential way of converting waste Si solar cells into aluminosilicate minerals to contribute to sustainability in the solar energy value chain.
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CrystEngComm, 2024, Accepted Manuscript
DOI: 10.1039/D4CE00168K, Paper

Fernando Igoa, Agustín López Cabrera, Javier Gonzalez-Platas, Leopoldo Suescun, Carlos Kremer, Julia Torres
Here, we present the synthesis and crystal structure of a series of heteronuclear metal-organic frameworks, which consists of cobalt(II) and lanthanide(III) ions or yttrium(III), connected by oxydiacetato (oda2-) as ligand....
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CrystEngComm, 2024, Advance Article
DOI: 10.1039/D4CE00201F, Paper

Binshan Zhao, Baolong Kuang, Mou Sun, Tingwei Wang, Chao Zhang, Meiqi Xu, Cong Li, Zujia Lu, Jian-guo Zhang
A novel heat-resistant energetic compound 3-(3,5-dinitrophenyl)-5-amino-1,2,4-oxadiazole with low mechanical sensitivity on the basis of combining dinitrobenzene and aminooxadiazole was synthesized through a simple method in this work.
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CrystEngComm, 2024, Accepted Manuscript
DOI: 10.1039/D4CE00210E, Paper

Jakub Gawraczynski, Piotr J Leszczynski, Michal Ksawery Cyranski, Łukasz Dobrzycki, Wiktor Koźmiński, Karol J. Fijalkowski, Wojciech Grochala, Tomasz Jaroń
A series of sulfates (S) and hydrogen sulfates (HS) containing tetramethylphosphonium (TMP), tetraethylphosphonium (TEP) and tetrabutylphosphonium (TBP) cations have been prepared from the respective bromides using ion metathesis reactions. The...
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CrystEngComm, 2024, 26,2155-2165
DOI: 10.1039/D3CE01208E, Paper

Wenxiu Yao, Pengfei Wu, Yidan Xie, Xinyu Shen, Shuwei Xia, Liangmin Yu
A series of charge transfer cocrystals with fluorescence properties involving 1,2,4,5-tetracyanobenzene as acceptor, fluorene, 2-bromofluorene, carbazole and 2-bromocarbazole as donor were synthesized via cocrystal design strategies.
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CrystEngComm, 2024, 26,2172-2179
DOI: 10.1039/D4CE00247D, Paper

Yan Gao, Xiao Yang, Taohong Ren, Dingxian Jia
3D iodoargentates [Co(en)₃(Ag₂I₄)]_n (1), [Fe(en)₃(Ag₂I₄)]_n (2) and [Co(dien)₂(Ag₂I₄)]_n·nH₂O (3) were prepared by solvothermal methods. Compounds 1–3 were catalytic activity for photodegradation of crystal violet under visible light irradiation.
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Org. Biomol. Chem., 2024, Advance Article
DOI: 10.1039/D4OB00093E, Paper

Balasubramaniyam Manikandan, Subbiah Thamotharan, Olivier Blacque, Subramaniapillai Selva Ganesan
One-pot, two-step methodology utilized for the sequential C–O/C–N cleavage followed by intramolecular/intermolecular annulation reaction.
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Org. Biomol. Chem., 2024, Advance Article
DOI: 10.1039/D4OB00237G, Paper

Arun Kumar Manna, Mizuki Doi, Keiya Matsuo, Hiroto Sakurai, Ch. Subrahmanyam, Kohei Sato, Tetsuo Narumi, Nobuyuki Mase
Fairy chemicals (FCs) such as 2-azahypoxanthine (AHX), isolated from naturally occurring sources, are potential phytohormones in plants and efficiently synthesized by fine bubble technology consisting of micro- to nano-sized bubbles.
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Org. Biomol. Chem., 2024, Advance Article
DOI: 10.1039/D4OB00232F, Paper

Open Access

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Muhammad Ehtisham Ibraheem Khan, Tomas Lighuen Cassini, Marino Petrini, Alessandro Palmieri
β-Nitroenones were converted into 3,5-disubstituted isoxazoles via a domino reaction promoted by tin(II) dichloride. The protocol efficiently works under both microwave and flow conditions.
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Org. Biomol. Chem., 2024, Advance Article
DOI: 10.1039/D3OB01986A, Paper

Carlos Cruz-Hernández, Perla Y. López-Camacho, Gustavo Basurto-Islas, Aaron Rojas, Patricia Guadarrama, Melchor Martínez-Herrera
Click chemistry is a valuable methodology for obtaining dendronized malonate derivatives to derivatize C60 using the Bingel–Hirsch reaction.
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Org. Biomol. Chem., 2024, Advance Article
DOI: 10.1039/D4OB00336E, Paper

Open Access

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Bintu Kumar, Anindita Bhatta, Prakriti Saraf, Taur Prakash Pandurang, Krishnan Rangan, Madhushree Sarkar, Sivaprasad Mitra, Dalip Kumar
Using readily available BODIPY and iodoarenes various BODIPY(aryl)iodonium salts were prepared and successfully utilized for the direct syntheses of functionalized BODIPYs, bis-BODIPYs and for the selective detection of serum protein.
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Org. Biomol. Chem., 2024, Advance Article
DOI: 10.1039/D4OB00256C, Paper

Min Zhang, Liang Shi, Li Chen, Zhengyu Liu, Ting Zhao, Chunyin Zhu, Liuqing Yang
A total of 27 novel spirooxindoles were synthesized through a water mediated three-component reaction of isatin, 4-aminocoumarin, and 1,3-cyclodicarbonyl compounds. Several compounds showed excellent antifungal activity against Physalospora piricola.
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Org. Biomol. Chem., 2024, Advance Article
DOI: 10.1039/D4OB00190G, Paper

Kai-Cheng Yang, Shi-Lu Zheng, Zhong Wen, Yu-Shan Zhang, Hai-Liang Ni, Long Chen
A HOTf or Fe(OTf)₃-catalyzed dehydrative alkynylation of 3-hydroxyisoindolinones with terminal alkynes was developed, which represents a brand-new procedure for the synthesis of 3-alkynylated 3,3-disubstituted isoindolinones.
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Org. Biomol. Chem., 2024, Advance Article
DOI: 10.1039/D4OB00112E, Paper

Debojyoti Bag, Sanghapal D. Sawant
Herein, we describe a highly diastereoselective approach for synthesizing polyfunctionalized spiroindolines from indolyl-ynones involving an ipso-iodocyclization/nucleophile addition cascade.
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Org. Biomol. Chem., 2024, Advance Article
DOI: 10.1039/D4OB00304G, Paper

Michela Eleuteri, Jenny Desantis, Gabriele Cruciani, Raimondo Germani, Laura Goracci
Selective degradation of disease-causing proteins using proteolysis targeting chimeras (PROTACs) has gained great attention, thanks to its several advantages over traditional therapeutic modalities.
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Org. Biomol. Chem., 2024, Advance Article
DOI: 10.1039/D4OB00229F, Paper

Kalleshappa Sheela, Chikkappaiahnayaka Santhosh, Krishna Ravi Singh, Kalleshappa Sharath, Maralinganadoddi P. Sadashiva
Herein, we report an efficient strategy to synthesize functionalized 1,3-thiazoles using alkyl 2-amino-2-thioxoacetates.
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Org. Biomol. Chem., 2024, Advance Article
DOI: 10.1039/D4OB00414K, Paper

Auqib Rashid, Waseem I. Lone, Preeti Dogra, Showkat Rashid, Bilal A. Bhat
An expeditious metal free C-3 alkylation of indoles and its NIS-mediated deviation to indolo[2,3-b]quinolines is reported. Applications of these strategies in accessing bioactive natural products have also been demonstrated.
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Org. Biomol. Chem., 2024, Advance Article
DOI: 10.1039/D4OB00402G, Paper

Yuta Ito, Hisato Tanaka, Ayana Murakami, Yasufumi Fuchi, Yoshiyuki Hari
5-(Benzimidazol-2-yl)- and 5-(benzothiazol-2-yl)-pyrimidine bases-modified oligonucleotides were prepared by post-synthetic trifluoromethyl conversion and their fluorescence properties were measured.
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