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Orientational disorder of mono­methyl-quinacridone investigated by Rietveld refinement, structure refinement to the pair-distribution function and lattice-energy minimizations

The crystal structure of the nanocrystalline pigment mono­methyl-quinacridone was solved from X-ray powder data. The orientational disorder was investigated using Rietveld refinements, structure refinement to the pair-distribution function, and lattice-energy minimizations of various ordered structural models.




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Genetic surprise: Magnificent frigatebird living on Galapagos Islands is distinct species

Researchers at the Smithsonian Conservation Biology Institute conducted three different kinds of genetics tests and all yielded the same result—the Galapagos seabirds have been genetically different from the magnificent frigatebirds elsewhere for more than half a million years.

The post Genetic surprise: Magnificent frigatebird living on Galapagos Islands is distinct species appeared first on Smithsonian Insider.




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Bone fragment is only Ice Age artwork from America to show a “proboscidean”

Researchers from the Smithsonian Institution and the University of Florida have announced the discovery of a bone fragment, approximately 13,000 years old, in Florida with an incised image of a mammoth or mastodon.

The post Bone fragment is only Ice Age artwork from America to show a “proboscidean” appeared first on Smithsonian Insider.




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Dictionary captures traditional ice knowledge of the Inupiaq people of Wales, Alaska

To prevent the loss of Inupiaq words for ice and the knowledge that it embodies, Igor Krupnik, ethnologist at the Arctic Studies Center of the National Museum of Natural History, and Wales native Winton Weyapuk Jr., recently compiled an illustrated dictionary of some 120 Kingikmiut words used in Wales to describe different types of ice.

The post Dictionary captures traditional ice knowledge of the Inupiaq people of Wales, Alaska appeared first on Smithsonian Insider.




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Recreating a slice of the universe

Scientists at the Harvard-Smithsonian Center for Astrophysics and their colleagues at the Heidelberg Institute for Theoretical Studies have invented a new computational approach that can accurately follow the birth and evolution of thousands of galaxies over billions of years.

The post Recreating a slice of the universe appeared first on Smithsonian Insider.




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“Hear My Voice”: Smithsonian identifies 130-year-old recording as Alexander Graham Bell’s voice

The inventions of Alexander Graham Bell—most famously the telephone but also methods of recording sound—have allowed people to hear each other’s voices for more than […]

The post “Hear My Voice”: Smithsonian identifies 130-year-old recording as Alexander Graham Bell’s voice appeared first on Smithsonian Insider.




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Smithsonian/Wisconsin police narrow search in 20 year mystery

Investigators from Rock County, Wisconsin, are one step closer to solving the mystery surrounding the death of an unknown teenager thanks to Smithsonian scientists. Christine […]

The post Smithsonian/Wisconsin police narrow search in 20 year mystery appeared first on Smithsonian Insider.







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With voices joined in chorus, giant otter families create a distinct sound signature

With a non-stop babble of hums, grunts and shrill squeals as they argue over fish and defend their territories, the Amazon’s giant otters are one […]

The post With voices joined in chorus, giant otter families create a distinct sound signature appeared first on Smithsonian Insider.




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Space is the best place to eat ice cream

Imagine a place where ice cream never drips. Ice cream lovers, how far would you be willing to go to avoid that heartbreaking moment where […]

The post Space is the best place to eat ice cream appeared first on Smithsonian Insider.



  • History & Culture
  • Science & Nature
  • Space
  • National Air and Space Museum

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Structure–function study of AKR4C14, an aldo-keto reductase from Thai jasmine rice (Oryza sativa L. ssp. indica cv. KDML105)

Aldo-keto reductases (AKRs) are NADPH/NADP+-dependent oxidoreductase enzymes that metabolize an aldehyde/ketone to the corresponding alcohol. AKR4C14 from rice exhibits a much higher efficiency in metabolizing malondialdehyde (MDA) than do the Arabidopsis enzymes AKR4C8 and AKR4C9, despite sharing greater than 60% amino-acid sequence identity. This study confirms the role of rice AKR4C14 in the detoxification of methylglyoxal and MDA, and demonstrates that the endogenous contents of both aldehydes in transgenic Arabidopsis ectopically expressing AKR4C14 are significantly lower than their levels in the wild type. The apo structure of indica rice AKR4C14 was also determined in the absence of the cofactor, revealing the stabilized open conformation. This is the first crystal structure in AKR subfamily 4C from rice to be observed in the apo form (without bound NADP+). The refined AKR4C14 structure reveals a stabilized open conformation of loop B, suggesting the initial phase prior to cofactor binding. Based on the X-ray crystal structure, the substrate- and cofactor-binding pockets of AKR4C14 are formed by loops A, B, C and β1α1. Moreover, the residues Ser211 and Asn220 on loop B are proposed as the hinge residues that are responsible for conformational alteration while the cofactor binds. The open conformation of loop B is proposed to involve Phe216 pointing out from the cofactor-binding site and the opening of the safety belt. Structural comparison with other AKRs in subfamily 4C emphasizes the role of the substrate-channel wall, consisting of Trp24, Trp115, Tyr206, Phe216, Leu291 and Phe295, in substrate discrimination. In particular, Leu291 could contribute greatly to substrate selectivity, explaining the preference of AKR4C14 for its straight-chain aldehyde substrate.




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New Book: “Across Atlantic Ice : The Origin of America’s Clovis Culture”

Supplying archaeological and oceanographic evidence, this book persuasively links Clovis technology with the culture of the Solutrean people who occupied France and Spain more than 20,000 years ago.

The post New Book: “Across Atlantic Ice : The Origin of America’s Clovis Culture” appeared first on Smithsonian Insider.




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New book reveals Ice Age mariners from Europe were America’s first inhabitants

Some of the earliest humans to inhabit America came from Europe according to a new book "Across Atlantic Ice: The Origin of America's Clovis Culture."

The post New book reveals Ice Age mariners from Europe were America’s first inhabitants appeared first on Smithsonian Insider.




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Magnificent Dom Pedro aquamarine to go on view in the Smithsonian’s Natural History Museum

The National Museum of Natural History will permanently display the Dom Pedro Aquamarine, which is the largest single piece of cut-gem aquamarine in the world, beginning Dec. 6.

The post Magnificent Dom Pedro aquamarine to go on view in the Smithsonian’s Natural History Museum appeared first on Smithsonian Insider.




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The transformation matrices (distortion, orientation, correspondence), their continuous forms and their variants. Corrigenda

Appendices B4 and B5 of Cayron [Acta Cryst. (2019), A75, 411–437] contain equations involving the point group and the metric tensor in which the equality symbol should be substituted by the inclusion symbol.




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XGANDALF – extended gradient descent algorithm for lattice finding

Serial crystallography records still diffraction patterns from single, randomly oriented crystals, then merges data from hundreds or thousands of them to form a complete data set. To process the data, the diffraction patterns must first be indexed, equivalent to determining the orientation of each crystal. A novel automatic indexing algorithm is presented, which in tests usually gives significantly higher indexing rates than alternative programs currently available for this task. The algorithm does not require prior knowledge of the lattice parameters but can make use of that information if provided, and also allows indexing of diffraction patterns generated by several crystals in the beam. Cases with a small number of Bragg spots per pattern appear to particularly benefit from the new approach. The algorithm has been implemented and optimized for fast execution, making it suitable for real-time feedback during serial crystallography experiments. It is implemented in an open-source C++ library and distributed under the LGPLv3 licence. An interface to it has been added to the CrystFEL software suite.




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Elastic propagation of fast electron vortices through amorphous materials

This work studies the elastic scattering behavior of electron vortices when propagating through amorphous samples. A formulation of the multislice approach in cylindrical coordinates is used to theoretically investigate the redistribution of intensity between different angular momentum components due to scattering. To corroborate and elaborate on our theoretical results, extensive numerical simulations are performed on three model systems (Si3N4, Fe0.8B0.2, Pt) for a wide variety of experimental parameters to quantify the purity of the vortices, the net angular momentum transfer, and the variability of the results with respect to the random relative position between the electron beam and the scattering atoms. These results will help scientists to further improve the creation of electron vortices and enhance applications involving them.




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Converting three-space matrices to equivalent six-space matrices for Delone scalars in S6

The transformations from the primitive cells of the centered Bravais lattices to the corresponding centered cells have conventionally been listed as three-by-three matrices that transform three-space lattice vectors. Using those three-by-three matrices when working in the six-dimensional space of lattices represented as Selling scalars as used in Delone (Delaunay) reduction, one could transform to the three-space representation, apply the three-by-three matrices and then back-transform to the six-space representation, but it is much simpler to have the equivalent six-by-six matrices and apply them directly. The general form of the transformation from the three-space matrix to the corresponding matrix operating on Selling scalars (expressed in space S6) is derived, and the particular S6matrices for the centered Delone types are listed. (Note: in his later publications, Boris Delaunay used the Russian version of his surname, Delone.)




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Smithsonian volcanologist Rick Wunderman talks about volcanos and the recent eruptions in Iceland

Rick Wunderman of the Global Volcanism Program at the Smithsonian's National Museum of Natural History talks about the current volcanic activity in Iceland.

The post Smithsonian volcanologist Rick Wunderman talks about volcanos and the recent eruptions in Iceland appeared first on Smithsonian Insider.




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Smithsonian entomologist Gary Hevel gives information and advice about stinkbugs in your home

Here come the stinkbugs...With the cooler temperatures of fall the brown marmorated stinkbug begins a determined quest to find a warm place to spend the winter. Crowding around window screens and searching for other ways to get inside, homeowners in the United States will share their indoor living space this winter with millions of brown marmorated stinkbugs. In this video Gary Hevel, an entomolgist at the Smithsonian's National Museum of Natural History, shares some information about these interesting creatures, as well as some advice about how to deal with those that inevitably gain entry to your home.

The post Smithsonian entomologist Gary Hevel gives information and advice about stinkbugs in your home appeared first on Smithsonian Insider.




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Device at the Smithsonian Environmental Research Center examines how phytoplankton would react if the ozone layer vanished

The post Device at the Smithsonian Environmental Research Center examines how phytoplankton would react if the ozone layer vanished appeared first on Smithsonian Insider.





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The artistry of Tlingit weaving is practiced by a dedicated few including artists Teri Rofkar and Shelly Laws of Alaska

It takes a Tlingit artist up to 2,000 hours, or 83 days, to weave just one ceremonial robe. Not surprisingly, this art form is practiced by a dedicated few including Tlingit artists Teri Rofkar and Shelly Laws of Alaska. In their presentation for the Smithsonian Spotlight series hosted by the Arctic Studies Center at the Anchorage Museum, Rofkar and Laws discuss the methods and cultural significance of robes, spruce root baskets and more.
For more information, go to http://www.mnh.si.edu/arctic/html/alaska.htm

The post The artistry of Tlingit weaving is practiced by a dedicated few including artists Teri Rofkar and Shelly Laws of Alaska appeared first on Smithsonian Insider.



  • Video
  • National Museum of Natural History


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Astronaut advice: Peggy Whitson

  Find your passion,” says veteran Astronaut Peggy Whitson. The Iowa native holds the record for time in space by an American. Learn all about […]

The post Astronaut advice: Peggy Whitson appeared first on Smithsonian Insider.



  • History & Culture
  • Science & Nature
  • Space
  • Video
  • National Air and Space Museum

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Mixed results for Hollywood at the summer box office

Business Update with Mark Lacter

Now that we have a deal between Time Warner Cable and CBS, we can turn our Hollywood focus back on the movie industry.

Steve Julian: Business analyst Mark Lacter, would you agree it's been an up and down summer at the box office?

Mark Lacter: It's been a flaky summer for Hollywood, Steve.  On the plus side, ticket revenue was up more than 10 percent, and attendance increased around six-and-a-half percent compared with last year (this covers the first week of May through Labor Day weekend).  The problem is that the studios and their investors spent huge amounts of money to make a lot of these movies, and they had to compete in a very crowded market - 23 big-budget films came out this summer, which is way higher than normal, and some of them never had a chance.

Julian: Some examples?

Lacter: Probably the biggest clunker was "The Lone Ranger," which could end up losing close to $200 million for Disney.  Another big disappointment was "White House Down," which was distributed by Sony and brought in only $140 million, which for a big-budget action film is really bad.  Even a film like "Pacific Rim," which did well at the box office, might still end up in the red because the production and marketing costs were so high.

Julian: And summer, of course, is the time when studios want to bring out these monster releases -

Lacter: - right, what they call "tent poles" - and in that category, the biggest winner was Disney's "Iron Man," which took in $1.2 billion.  Also having a great summer was "Monsters University" from Pixar, with $700 million.  You also had "Despicable Me 2" and "Fast and Furious 6," which might not be our cup of tea (speak for yourself, it takes me back to my police car days!), but did very well for Universal.  Eight of the top 12 films this summer were sequels - and yet, sequels were no guarantee of success (a number of them really struggled).  And, some non-blockbuster films found considerable success: "Now You See Me" from Lionsgate only cost $75 million to make.

Julian: So, in some ways, Hollywood was its usual unpredictable self.

Lacter: That's right - and don't expect any big changes in strategy when it comes to big-budget films.  The prospect of having huge success with one of these blockbusters is just too great, but perhaps more important is the fact that many of these films are financed by multiple groups of investors, and so the risk is spread around.  It's not like the old days when a studio bankrolled the whole thing.

Julian: Though, sounds like it's bad news for the city of Los Angeles: the "Man of Steel" sequel is going to be shot in Michigan?

Lacter: Mayor Garcetti has actually declared a state of emergency because the city keeps losing business to other states that offer big tax incentives to films - what's known as runaway production.  The truth is that business has been lost over the years, but L.A. is hardly in any danger of losing its spot as the center of entertainment.  And, you can see that with the L.A. County Board of Supervisors signing off on Disney's plan for a TV and movie production facility near Santa Clarita that will add more than a half-million square feet of studio space.

Julian: And, Universal's expanding, too.

Lacter: Earlier this year, Universal was given the approval to build more production facilities, and Paramount is planning an expansion, as well.  Now, these are all very ambitious projects - not the sort of investments that would be made if these studios were looking elsewhere to make movies and TV shows.  And, of course, they mean jobs - actually, employment levels in the entertainment industry have remained fairly steady going back the last decade.

Julian: Are there states that are pulling back their incentives?

Lacter: Yes, the state of North Carolina, which has been especially aggressive in using tax incentives to draw in movies and television going back to the 80s, is phasing out the giveaways because legislators have decided that the economic benefits aren't worth the tax revenues being lost.  And, other states with tax incentive programs are pulling back as well - they're finding that the payback is very difficult to measure.

Mark Lacter writes for Los Angeles Magazine and pens the business blog at LA Observed.com.

This content is from Southern California Public Radio. View the original story at SCPR.org.




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A request for advice regarding setting up a sensible basic build with Vista




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National Park Service natural history collections transferred to care of the Smithsonian

The National Park Service and the Smithsonian Institution have announced a new partnership to share responsibility for selected National Park Service natural history collections, making them more readily available to researchers through the Smithsonian.

The post National Park Service natural history collections transferred to care of the Smithsonian appeared first on Smithsonian Insider.




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Ancient algal ‘tree rings’ show dramatic decline in Arctic and sub-Arctic sea ice

An ancient new player has entered the debate over global warming and it is pink. Labrador fishermen call them “red rocks” because underwater they resemble […]

The post Ancient algal ‘tree rings’ show dramatic decline in Arctic and sub-Arctic sea ice appeared first on Smithsonian Insider.




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Of mice and macchiato: Bird Friendly coffee gives a paw-up to small mammals as well

Finding a mouse in your morning coffee might give you an unwelcome jolt, but there’s a strong connection between small mammals, birds and the plantations […]

The post Of mice and macchiato: Bird Friendly coffee gives a paw-up to small mammals as well appeared first on Smithsonian Insider.




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Selling reduction versus Niggli reduction for crystallographic lattices

The unit-cell reduction described by Selling and used by Delone (whose early publications were under the spelling Delaunay) is explained in a simple form. The transformations needed to implement the reduction are listed. The simplicity of this reduction contrasts with the complexity of Niggli reduction.




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