synthesis

Hydrogen blamed for interfering with nickelate superconductors synthesis

Prof. ZHONG Zhicheng's team at the Ningbo Institute of Materials Technology and Engineering has investigated the electronic structure of the recently discovered nickelate superconductors NdNiO2. They successfully explained the experimental difficulties in synthesizing superconducting nickelates, in cooperation with Prof. Karsten Held at Vienna University of Technology.




synthesis

MdMYB6 regulates anthocyanin formation in apple both through direct inhibition of the biosynthesis pathway and through substrate removal




synthesis

Digital synthesis of histological stains using micro-structured and multiplexed virtual staining of label-free tissue




synthesis

Extra-adrenal glucocorticoid biosynthesis: implications for autoimmune and inflammatory disorders




synthesis

Blood pressure and nitric oxide synthesis capacity in physically active and inactive groups: the SABPA study




synthesis

Rad53 limits CMG helicase uncoupling from DNA synthesis at replication forks




synthesis

Structure of a proton-dependent lipid transporter involved in lipoteichoic acids biosynthesis




synthesis

Targeting cellular fatty acid synthesis limits T helper and innate lymphoid cell function during intestinal inflammation and infection




synthesis

Nanomolar-scale, high throughput chemical synthesis of drug-like molecules

A high throughput, miniaturized chemical synthesis platform could enable rapid discovery of lead compounds.




synthesis

Relationship between markers of malnutrition and clinical outcomes in older adults with cancer: systematic review, narrative synthesis and meta-analysis




synthesis

Rheticus project teams German giants to harvest CO2 in artificial photosynthesis

Evonik and Siemens announce two-year project to demonstrate feasibility of "technical photosynthesis" using eco-electricity to convert carbon dioxide into valuable chemicals




synthesis

New Method of DNA Synthesis Helps Tackle COVID-19 Pandemic

DNA synthesis is transforming diagnosis and treatment of COVID-19, and may play a vital role in halting the pandemic. Allie Nawrat, Senior Medical




synthesis

Small Reservoirs in Africa: A Review and Synthesis to Strengthen Future Investment

Small reservoirs are a critical coping mechanism in water-stressed rural areas in Africa, providing immense livelihood benefits that include improved food and water security, entrepreneurial activities and climate resilience. Challenges associated with the implementation of investments in small reservoirs include appropriate site selection, weak institutions, insufficient maintenance and sedimentation. The findings from this study suggest […]




synthesis

OECD releases guidance on Synthesised texts for providing clarity on the impact of the Multilateral Instrument

This new guidance presents a clear overview of the modifications to tax treaties resulting from the Multilateral BEPS Convention which entered into force on 1 July 2018. A Secretariat note, also released today, clarifies the entry into effect rules for tax treaties of jurisdictions that deposited their ratification instruments last September.




synthesis

Workshop on Integrating Omics and Policy for Healthy Ageing: Synthesis Report

An ageing population brings new challenges both to healthcare systems and to medicine in terms of the increased manifestation of specific diseases primarily seen in the elderly. Biomedical innovation, and in particular research into "omics technologies", offers the promise of new means of detection, prevention and treatment of age-related disabilities and diseases.




synthesis

Final NAEC Synthesis Report

The report discusses the changes in perspective and changes in the OECD’s analysis, instruments and tools that are required to gear the OECD towards addressing future challenges in an increasingly interconnected and complex global economy. It maps the policy trade-offs and complementarities and discusses the policy implications and recommendations deriving from NAEC projects to support an inclusive and sustainable growth agenda.




synthesis

Womanhood: A synthesis through many forms


Shoma A Chatterji writes on Samanway 7, a unique theatre festival showcasing performances conceived of and crafted exclusively by women, which evolved into a well-blended expression of feminist questions that have sustained through the ages.




synthesis

[ASAP] Scrabbling around in Synthetic Nuances Managing Sodium Compounds: Bisphenol/Bisnaphthol Synthesis by Hydroxyl Group Masking

Inorganic Chemistry
DOI: 10.1021/acs.inorgchem.0c00310




synthesis

[ASAP] Design and Synthesis of Cyclometalated Iridium(III) Complexes—Chromophore Hybrids that Exhibit Long-Emission Lifetimes Based on a Reversible Electronic Energy Transfer Mechanism

Inorganic Chemistry
DOI: 10.1021/acs.inorgchem.0c00363




synthesis

[ASAP] Fast, Low-Cost Synthesis of ZnO:Eu Nanosponges and the Nature of Ln Doping in ZnO

Inorganic Chemistry
DOI: 10.1021/acs.inorgchem.0c00472




synthesis

[ASAP] Programmable One-Pot Synthesis of Oligosaccharides

Biochemistry
DOI: 10.1021/acs.biochem.9b00613




synthesis

[ASAP] Synthesis of 3-<italic toggle="yes">O</italic>-Sulfated Disaccharide and Tetrasaccharide Standards for Compositional Analysis of Heparan Sulfate

Biochemistry
DOI: 10.1021/acs.biochem.9b00838




synthesis

[ASAP] Biosynthesis of the Maresin Intermediate, 13S,14S-Epoxy-DHA, by Human 15-Lipoxygenase and 12-Lipoxygenase and Its Regulation through Negative Allosteric Modulators

Biochemistry
DOI: 10.1021/acs.biochem.0c00233




synthesis

[ASAP] Controllable Synthesis of Peapod-like Sb@C and Corn-like C@Sb Nanotubes for Sodium Storage

ACS Nano
DOI: 10.1021/acsnano.0c00366




synthesis

[ASAP] Self-Templating Synthesis of Hollow Co<sub>3</sub>O<sub>4</sub> Nanoparticles Embedded in N,S-Dual-Doped Reduced Graphene Oxide for Lithium Ion Batteries

ACS Nano
DOI: 10.1021/acsnano.0c00712




synthesis

[ASAP] A4 Paper Chemistry: Synthesis of a Versatile and Chemically Modifiable Cellulose Membrane

ACS Nano
DOI: 10.1021/acsnano.0c02211




synthesis

Mercury and the Everglades [Electronic book] : a Synthesis and Model for Complex Ecosystem Restoration. Volume II, Aquatic Mercury Cycling and Bioaccumulation in the Everglades / Darren G. Rumbold, Curtis D. Pollman, Donald M. Axelrad, editors.

Cham : Springer, 2020.




synthesis

Rates of evolution: a quantitative synthesis / Philip D. Gingerich, University of Michigan

Dewey Library - QH366.2.G524 2019




synthesis

Synthesis and enantioseparation of proline-derived helical polyacetylenes as chiral stationary phases for HPLC

Polym. Chem., 2020, Advance Article
DOI: 10.1039/D0PY00205D, Paper
Ge Shi, Xiao Dai, Yue Zhou, Jie Zhang, Jun Shen, Xinhua Wan
Proline-derived aliphatically substituted polyacetylenes with stable helical conformations exhibit an excellent enantioseparation ability as chiral stationary phases of HPLC.
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synthesis

Synthesis of star-shaped polyzwitterions with adjustable UCST and fast responsiveness by a facile RAFT polymerization

Polym. Chem., 2020, Advance Article
DOI: 10.1039/D0PY00318B, Paper
Zhi Li, Hao Li, Zhonghe Sun, Botao Hao, Tung-Chun Lee, Anchao Feng, Liqun Zhang, San H. Thang
We describe crosslinking of polyzwitterions for the formation of novel star-shaped polymers with low polydispersities and dual-responsiveness using RAFT polymerization.
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synthesis

Poly(alanine-nylon-alanine) as a bioplastic: chemoenzymatic synthesis, thermal properties and biological degradation effects

Polym. Chem., 2020, Advance Article
DOI: 10.1039/D0PY00137F, Paper
Open Access
Prashant G. Gudeangadi, Kei Uchida, Ayaka Tateishi, Kayo Terada, Hiroyasu Masunaga, Kousuke Tsuchiya, Hitoshi Miyakawa, Keiji Numata
Poly(amino acids) such as polypeptides and proteins are attractive biomass-based polymers that potentially contribute to circular economy for plastic.
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synthesis

Surfactant-free synthesis of layered double hydroxide-armored latex particles

Polym. Chem., 2020, Advance Article
DOI: 10.1039/D0PY00140F, Paper
Open Access
  This article is licensed under a Creative Commons Attribution 3.0 Unported Licence.
X. G. Qiao, P.-Y. Dugas, V. Prevot, E. Bourgeat-Lami
MgAl-layered double hydroxide (LDH)-armored latexes were produced by Pickering emulsion polymerization of styrene using 2-hydroxyethyl methacrylate (HEMA) and methyl methacrylate (MMA) as auxiliary comonomers.
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synthesis

Rapid metal-free synthesis of pyridyl-functionalized conjugated microporous polymers for visible-light-driven water splitting

Polym. Chem., 2020, Advance Article
DOI: 10.1039/D0PY00249F, Communication
Zhonghua Cheng, Lei Wang, Yan He, Xingjia Chen, Xiaojun Wu, Hangxun Xu, Yaozu Liao, Meifang Zhu
A rapid metal-free synthetic approach was applied to synthesize pyridyl-functionalized conjugated microporous polymers (PCMPs) via an aminative cyclization between aryl aldehydes and ketones without any metal catalysts.
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synthesis

Synthesis of acrylamide-based block-copolymer brushes under flow: monitoring real-time growth and surface restructuring upon drying

Polym. Chem., 2020, Advance Article
DOI: 10.1039/D0PY00219D, Paper
Open Access
Joydeb Mandal, Andrea Arcifa, Nicholas D. Spencer
Block-copolymer brushes of water-soluble acrylamides have been synthesised by SI-ATRP under continuous flow and their growth monitored in situ by means of a quartz-crystal microbalance with dissipation (QCM-D).
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synthesis

Simple improvements to Gilch synthesis and molecular weight modulation of MEH-PPV

Polym. Chem., 2020, 11,2831-2837
DOI: 10.1039/D0PY00072H, Paper
Riley O'shea, Wallace W. H. Wong
The solvent and temperature used in the Gilch synthesis of poly[2-methoxy-5-(2-ethylhexyloxy)-1,4-phenylenevinylene] (MEH-PPV) were varied to achieve an improved set of reaction conditions.
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synthesis

Synthesis of a side-chain hole transporting polymer through Mitsunobu post-functionalization for efficient inverted perovskite solar cells

Polym. Chem., 2020, 11,2883-2888
DOI: 10.1039/D0PY00134A, Paper
Liuyuan Lan, Xiang Deng, Jie Zhang, Jingdong Luo, Alex K.-Y. Jen
Mitsunobu post-functionalization was utilized to construct a new efficient dopant-free side-chain hole transporting polymer for inverted perovskite solar cells, exhibiting a power conversion efficiency of 17.75% and a high fill factor over 81%.
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synthesis

Synthesis of biscarboxylic acid functionalised EDTA mimicking polymers and their ability to form Zr(IV) chelation mediated nanostructures

Polym. Chem., 2020, 11,2799-2810
DOI: 10.1039/D0PY00304B, Paper
Meike N. Leiske, Julia A. Walker, Aadarash Zia, Nicholas L. Fletcher, Kristofer J. Thurecht, Thomas P. Davis, Kristian Kempe
We present a new biscarboxylic acid acrylate, which is used for the synthesis of double hydrophilic EDTA-mimicking block copolymers capable of self-assembly upon zirconium complexation.
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synthesis

Amide transformation as an efficient postpolymerization modification approach for the synthesis of functional polyacetylenes

Polym. Chem., 2020, Advance Article
DOI: 10.1039/D0PY00398K, Paper
Juntao Ren, Heng Liu, Xuequan Zhang, Yanming Hu, Guangyuan Zhou, Toshio Masuda
Modification of a precursor polyacetylene with various amines and alcohols through amide transformation gives access to a series of functional polymers showing nonlinear optical, luminescence, enhanced surface energy, and redox active properties.
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synthesis

Sequential and alternating RAFT single unit monomer insertion: model trimers as the guide for discrete oligomer synthesis

Polym. Chem., 2020, Advance Article
DOI: 10.1039/D0PY00390E, Paper
Ruizhe Liu, Lei Zhang, Zixuan Huang, Jiangtao Xu
A complete set of model trimers and their synthetic kinetics are established to guide the synthesis of diverse sequence-defined polymers.
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synthesis

Room Temperature Synthesis of Block Copolymer Nano-Objects with Different Morphologies via Ultrasound Initiated RAFT Polymerization-Induced Self-Assembly (Sono-RAFT-PISA)

Polym. Chem., 2020, Accepted Manuscript
DOI: 10.1039/D0PY00461H, Paper
Jing Wan, Bo Fan, Yiyi Liu, Tina Hsia, Kaiyuan Qin, Tanja Junkers, Boon M. Teo, San Thang
Polymerization-induced self-assembly (PISA), which allows scalable synthesis of nano-objects, has drawn significant research attention in the past decade. However, the initiation methods in most of the current reported PISA are...
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synthesis

Synthesis of well-defined heteroglycopolymers via combining sequential click reactions and PPM: the effects of linker and heterogeneity on Con A binding

Polym. Chem., 2020, 11,3054-3065
DOI: 10.1039/D0PY00302F, Paper
Meina Liu, Xingyou Wang, Dengyun Miao, Caiyun Wang, Wei Deng
A versatile post- polymerization modification strategy to synthesize well-defined glycopolymers via the combination of RAFT polymerization and sequential CuAAC and thiol–ene click reactions was developed.
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synthesis

Synthesis of conjugated polymers via cyclopentannulation reaction: promising materials for iodine adsorption

Polym. Chem., 2020, 11,3066-3074
DOI: 10.1039/D0PY00286K, Paper
Open Access
Noorullah Baig, Suchetha Shetty, Saleh Al-Mousawi, Bassam Alameddine
A new class of conjugated polymers is prepared by means of a versatile palladium-catalyzed cyclopentannulation reaction using a series of specially designed diethynyl aryl synthons with the commercially available 9,10-dibromoanthracene DBA monomer.
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synthesis

Double-click synthesis of polysiloxane third-order nonlinear optical polymers with donor–acceptor chromophores

Polym. Chem., 2020, 11,3046-3053
DOI: 10.1039/C9PY01771B, Paper
Zhitao Li, Dong Wang, Daniele Ramella, Hong Gao, Hui Cao, Yuzhen Zhao, Zongcheng Miao, Zhou Yang, Wanli He
A series of third-order nonlinear polysiloxane polymer materials were prepared by thiol–ene click polymerization and [2 + 2] click chemistry. All the polymers exhibit good electron transfer capabilities and nonlinear optical properties.
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synthesis

Synthesis, thermoresponsivity and multi-tunable hierarchical self-assembly of multi-responsive (AB)mC miktobrush-coil terpolymers

Polym. Chem., 2020, 11,3003-3017
DOI: 10.1039/D0PY00245C, Paper
Xiaomin Zhu, Jian Zhang, Cheng Miao, Siyu Li, Youliang Zhao
Stimuli-responsive miktobrush-coil terpolymers can exhibit unique physical properties and hierarchical self-assembly behaviors dependent on composition, concentration and external stimuli.
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synthesis

Facile synthesis and exploration of excited state assisted two-photon absorption properties of D–A–D type thiophene–pyridine derivatives

Photochem. Photobiol. Sci., 2020, Advance Article
DOI: 10.1039/D0PP00047G, Paper
Viprabha Kakekochi, Sathish Chatnahalli Gangadharappa, Nikhil P. P., Chandrasekharan Keloth, Ezequiel Wolcan, Udaya Kumar D
Diagrammatic representation of excited state assisted two-photon absorption (2PA) behavior of a donor–acceptor type conjugated polymer (P2TPy) exhibiting an extremely low optical limiting threshold.
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synthesis

Bioinspired polydopamine nanoparticles: synthesis, nanomechanical properties, and efficient PEGylation strategy

J. Mater. Chem. B, 2020, Advance Article
DOI: 10.1039/C9TB02769F, Paper
Islam Zmerli, Jean-Philippe Michel, Ali Makky
We established tightly controlled experimental conditions to synthesize polydopamine nanoparticles with well-defined and reproducible physicochemical properties such as size, yield and nanomechanics.
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synthesis

Multivalent cationic dendrofullerenes for gene transfer: synthesis and DNA complexation

J. Mater. Chem. B, 2020, Advance Article
DOI: 10.1039/D0TB00113A, Paper
Beatriz M. Illescas, Alfonso Pérez-Sánchez, Araceli Mallo, Ángel Martín-Domenech, Ignacio Rodríguez-Crespo, Nazario Martín
Non-viral nucleic acid vectors able to display high transfection efficiencies with low toxicity and overcoming the multiple biological barriers are needed to further develop the clinical applications of gene therapy.
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synthesis

One-pot synthesis of trypsin-based magnetic metal–organic frameworks for highly efficient proteolysis

J. Mater. Chem. B, 2020, Advance Article
DOI: 10.1039/C9TB02315A, Paper
Chao Zhong, Zhixian Lei, Huan Huang, Mingyue Zhang, Zongwei Cai, Zian Lin
A facile approach was developed for one-pot synthesis of trypsin-based magnetic ZIF-8, which could be applied as an immobilized enzyme microreactor for rapid digestion of proteins.
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synthesis

[ASAP] Critical Coupling of Visible Light Extends Hot-Electron Lifetimes for H<sub>2</sub>O<sub>2</sub> Synthesis

ACS Applied Materials & Interfaces
DOI: 10.1021/acsami.0c00825




synthesis

Synthesis and Photophysics of Gold(I) Alkynyls Bearing a Benzothiazole-2,7-Fluorenyl Moiety: A Comparative Study Analyzing Influence of Ancillary Ligand, Bridging Moiety, and Number of Metal Centers on Photophysical Properties

Phys. Chem. Chem. Phys., 2020, Accepted Manuscript
DOI: 10.1039/D0CP01539C, Paper
Joseph J Mihaly, Alexis Phillips, David J Stewart, Zachary M Marsh, Christopher McCleese, Joy E. Haley, Matthias Zeller, Tod Grusenmeyer, Thomas Gray
Three new gold(I) alkynyl complexes (Au-ABTF(0-2)) containing a benzothiazole fluorenyl moiety, with either an organic phosphine or N-heterocyclic carbene as ancillary ligand, have been synthesized and photophysically characterized. All three...
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