synthesis

Two amino acid-templated metal phosphates: surfactant-thermal synthesis, water stability, and proton conduction

Dalton Trans., 2020, 49,5440-5444
DOI: 10.1039/D0DT00966K, Communication
Lijuan Huang, Lei Wang, Yan Zhao, Ling Huang, Jian Bi, Guohong Zou, Zhien Lin, Daojiang Gao
An amino acid-templated gallium phosphate with a zeolitic topology has been prepared under surfactant-thermal conditions and it shows exceptional water stability and interesting proton-conducting properties.
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synthesis

Pyridylamido hafnium complexes with a silylene bridge: synthesis and olefin polymerization

Dalton Trans., 2020, Advance Article
DOI: 10.1039/D0DT01031F, Paper
Pavel S. Kulyabin, Dmitry V. Uborsky, Alexander Z. Voskoboynikov, Jo Ann M. Canich, John R. Hagadorn
Pyridylamido hafnium complexes with a silylene bridge were synthesized, characterized with X-ray crystal structure analysis and shown to polymerize 1-hexene and propene and copolymerize ethylene and 1-octene.
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synthesis

Synthesis and characterisation of light lanthanide bis-phospholyl borohydride complexes

Dalton Trans., 2020, Advance Article
DOI: 10.1039/D0DT01241F, Paper
Jingjing Liu, Lydia E. Nodaraki, Philip J. Cobb, Marcus J. Giansiracusa, Fabrizio Ortu, Floriana Tuna, David P. Mills
Two families of lanthanide(III) phospholyl borohydride complexes are reported (carbon = grey, hydrogen = white, oxygen = red, boron = yellow, phosphorus = magenta, potassium = blue, lanthanides = teal; only BH4 hydrogens are shown for clarity).
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synthesis

Facile synthesis of Mn-doped NiCo2O4 nanoparticles with enhanced electrochemical performance for a battery-type supercapacitor electrode

Dalton Trans., 2020, Advance Article
DOI: 10.1039/D0DT01177K, Paper
To Van Nguyen, Le The Son, Vu Van Thuy, Vu Dinh Thao, Masahito Hatsukano, Koichi Higashimine, Shinya Maenosono, Sang-Eun Chun, Tran Viet Thu
We report the synthesis of manganese-doped nickel cobalt oxide (Mn-doped NiCo2O4) nanoparticles (NPs) by an efficient hydrothermal and subsequent calcination route.
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synthesis

Rapid mechanochemical synthesis of metal–organic frameworks using exogenous organic base

Dalton Trans., 2020, Advance Article
DOI: 10.1039/D0DT01240H, Paper
Zihao Wang, Zongzhe Li, Marcus Ng, Phillip J. Milner
We describe the mechanochemical, solvent-free synthesis of metal–organic frameworks using liquid organic base for the first time.
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synthesis

Synthesis and reactivity of cyclobutadiene nickel bromide

Dalton Trans., 2020, Advance Article
DOI: 10.1039/D0DT01510E, Paper
Nikita V. Shvydkiy, Egor A. Dlin, Klimentiy V. Ivanov, Anastasiya G. Buyanovskaya, Yulia V. Nelyubina, Dmitry S. Perekalin
The reaction of NiBr2 with 3-hexyne provides new access to various cyclobutadiene nickel complexes.
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synthesis

Selenotungstates incorporating organophosphonate ligands and metal ions: synthesis, characterization, magnetism and catalytic efficiency in Knoevenagel condensation reaction

Dalton Trans., 2020, Accepted Manuscript
DOI: 10.1039/D0DT00444H, Paper
Jingyang Niu, Hui Kong, Peipei He, Zongfei Yang, Qiaofei Xu, Jiawei Wang, Ran Ban, Pengtao Ma, Jingping Wang
Three sandwich-type TM-containing (TM = transition metal) organophosphonate-based polyoxotungstate clusters, [TM(H2O)4(SeW6O21)2{Co(OOCCH2NCH2PO3)2}3]12– (TM = Co, Ni), have been successfully synthesized, which is the first reported TMs-containing organophosphonate-based selenotungstates. They were structurally...
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synthesis

Mystic synthesis in Java : a history of Islamization from the fourteenth to the early nineteenth centuries / M.C. Ricklefs

Ricklefs, M. C. (Merle Calvin), 1943- author




synthesis

[ASAP] Comparative Proteomics Analysis Reveals That Lignin Biosynthesis Contributes to Brassinosteroid-Mediated Response to <italic toggle="yes">Phytophthora sojae</italic> in Soybeans

Journal of Agricultural and Food Chemistry
DOI: 10.1021/acs.jafc.0c00848




synthesis

[ASAP] Transcriptome Analysis Reveals Candidate Genes for Petroselinic Acid Biosynthesis in Fruits of <italic toggle="yes">Coriandrum sativum</italic> L.

Journal of Agricultural and Food Chemistry
DOI: 10.1021/acs.jafc.0c01487




synthesis

[ASAP] Proteome Analysis of Hordein-Null Barley Lines Reveals Storage Protein Synthesis and Compensation Mechanisms

Journal of Agricultural and Food Chemistry
DOI: 10.1021/acs.jafc.0c01410




synthesis

[ASAP] Synthesis and Antiviral/Fungicidal/Insecticidal Activities Study of Novel Chiral Indole Diketopiperazine Derivatives Containing Acylhydrazone Moiety

Journal of Agricultural and Food Chemistry
DOI: 10.1021/acs.jafc.0c00875




synthesis

[ASAP] Design, Synthesis, and Anti-ToCV Activity of Novel 4(3<italic toggle="yes">H</italic>)-Quinazolinone Derivatives Bearing Dithioacetal Moiety

Journal of Agricultural and Food Chemistry
DOI: 10.1021/acs.jafc.0c00086




synthesis

Simple synthesis for shapeshifting molecules

Bullvalene's constant metamorphosis could be exploited in sensing applications




synthesis

Simple synthesis for shape-shifting molecules

Bullvalene's constant metamorphosis could be exploited in sensing applications




synthesis

A radial setup helps automated synthesis branch out

Reactors arranged around a central switching station gives chemists more options for making molecules remotely




synthesis

Combining heat with light boosts methanol synthesis from CO&lt;sub&gt;2&lt;/sub&gt;

Study unravels reaction mechanism occurring on common catalyst




synthesis

Synthesis of a flower-like MoS2/carbon nanocomposite with enhanced adsorption performance toward Eu(III): the cooperative effects between S atoms and carboxyl groups

Environ. Sci.: Water Res. Technol., 2020, 6,1482-1494
DOI: 10.1039/D0EW00155D, Paper
Chaofeng Zhao, Pengcheng Gu, Xuewei Liu, Tao Wen, Yuejie Ai
Combining experimental studies and theoretical calculations to investigate the performance and mechanism of a MoS2/carbon composite for the effective elimination of Eu(III) from wastewater.
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synthesis

[ASAP] Prodrug Approach for Posterior Eye Drug Delivery: Synthesis of Novel Ganciclovir Prodrugs and in Vitro Screening with Cassette Dosing

Molecular Pharmaceutics
DOI: 10.1021/acs.molpharmaceut.0c00037




synthesis

[ASAP] Amiodarone Alters Cholesterol Biosynthesis through Tissue-Dependent Inhibition of Emopamil Binding Protein and Dehydrocholesterol Reductase 24

ACS Chemical Neuroscience
DOI: 10.1021/acschemneuro.0c00042




synthesis

Analog synthesizers: understanding, performing, buying from the legacy of Moog to software synthesis / Mark Jenkins

STACK BOOKS ML1092.J47 2020




synthesis

Gas phase synthesis of amorphous silicon nitride nanoparticles for high-energy LIBs

Energy Environ. Sci., 2020, 13,1212-1221
DOI: 10.1039/C9EE03857D, Communication
Sujong Chae, Seungkyu Park, Kihong Ahn, Gyutae Nam, Taeyong Lee, Jaekyung Sung, Namhyung Kim, Jaephil Cho
We introduce a highly homogenous phase design of Si with N by scalable gas phase synthesis using a specially customized vertical furnace, which tackles the intrinsic challenges of Si anodes.
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synthesis

Rewiring photosynthesis: a photosystem I-hydrogenase chimera that makes H2 in vivo

Energy Environ. Sci., 2020, Advance Article
DOI: 10.1039/C9EE03859K, Paper
Andrey Kanygin, Yuval Milrad, Chandrasekhar Thummala, Kiera Reifschneider, Patricia Baker, Pini Marco, Iftach Yacoby, Kevin E. Redding
Photosystem I-hydrogenase chimera intercepts electron flow directly from the photosynthetic electron transport chain and directs it to hydrogen production.
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synthesis

[ASAP] Eco-Friendly Synthesis of SO<sub>3</sub>H-Containing Solid Acid via Mechanochemistry for the Conversion of Carbohydrates to 5-Hydroxymethylfurfural

ACS Sustainable Chemistry & Engineering
DOI: 10.1021/acssuschemeng.0c00784




synthesis

[ASAP] One-Pot Synthesis of Cyclic Biofuel Intermediates from Biomass in Choline Chloride/Formic Acid-Based Deep Eutectic Solvents

ACS Sustainable Chemistry & Engineering
DOI: 10.1021/acssuschemeng.9b07300




synthesis

[ASAP] Design and Synthesis of Highly Performing Bifunctional Ni-NiO-MoNi Hybrid Catalysts for Enhanced Urea Oxidation and Hydrogen Evolution Reactions

ACS Sustainable Chemistry & Engineering
DOI: 10.1021/acssuschemeng.0c01637




synthesis

[ASAP] Solvothermal Synthesis of Defect-Rich Mixed 1T-2H MoS<sub>2</sub> Nanoflowers for Enhanced Hydrodesulfurization

ACS Sustainable Chemistry & Engineering
DOI: 10.1021/acssuschemeng.0c00736




synthesis

[ASAP] Functionalized Biochar with Superacidity and Hydrophobicity as a Highly Efficient Catalyst in the Synthesis of Renewable High-Density Fuels

ACS Sustainable Chemistry & Engineering
DOI: 10.1021/acssuschemeng.9b07367




synthesis

[ASAP] Bioinspired Enzymatic Synthesis of Terpenoid-Based (Meth)acrylic Monomers: A Solvent-, Metal-, Amino-, and Halogen-Free Approach

ACS Sustainable Chemistry & Engineering
DOI: 10.1021/acssuschemeng.0c02307




synthesis

[ASAP] Enhanced Photosynthesis of Carotenoids in Microalgae Driven by Light-Harvesting Gold Nanoparticles

ACS Sustainable Chemistry & Engineering
DOI: 10.1021/acssuschemeng.0c00315




synthesis

Polyketide synthesis in Stagnospora nodorum / Christian Krill

Krill, Christian




synthesis

Bridging the gap between industry and synchrotron: an operando study at 30 bar over 300 h during Fischer–Tropsch synthesis

React. Chem. Eng., 2020, Advance Article
DOI: 10.1039/C9RE00493A, Paper
Open Access
  This article is licensed under a Creative Commons Attribution 3.0 Unported Licence.
M. Loewert, M.-A. Serrer, T. Carambia, M. Stehle, A. Zimina, K. F. Kalz, H. Lichtenberg, E. Saraçi, P. Pfeifer, J.-D. Grunwaldt
Long-term operando spectroscopic study of a Fischer–Tropsch catalyst at a synchrotron radiation facility under realistic conditions with full product analysis.
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synthesis

Continuous flow synthesis of the URAT1 inhibitor lesinurad

React. Chem. Eng., 2020, 5,865-872
DOI: 10.1039/C9RE00483A, Paper
Mariana C. F. C. B. Damião, Henrique M. Marçon, Julio Cezar Pastre
A 5-steps continuous flow synthesis of lesinurad is provided and delivers this API in 68% overall yield.
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synthesis

Ultrafast synthesis of 2-(benzhydrylthio)benzo[d]oxazole, an antimalarial drug, via an unstable lithium thiolate intermediate in a capillary microreactor

React. Chem. Eng., 2020, 5,849-852
DOI: 10.1039/D0RE00038H, Communication
Bandaru T. Ramanjaneyulu, Shinde Vidyacharan, Gwang-Noh Ahn, Dong-Pyo Kim
We present an ultrafast approach for the synthesis of 2-(benzhydrylthio)benzo[d]oxazole, an antimalarial drug, in 75% yield from benzo[d]oxazole-2-thiol and benzhydryl bromide via an unstable lithium thiolate intermediate in the presence of n-BuLi.
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synthesis

Design and development of 3D printed catalytically-active stirrers for chemical synthesis

React. Chem. Eng., 2020, 5,853-858
DOI: 10.1039/C9RE00492K, Communication
Open Access
Matthew R. Penny, Stephen T. Hilton
In a novel approach, 3D-printed pTsOH containing stirrer beads have been used to catalyse the Mannich reaction.
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synthesis

Synthesis of 3-trifluoromethylated 1,3-butadienes via a Pd(0)-catalyzed fluorinated Heck reaction

React. Chem. Eng., 2020, 5,961-966
DOI: 10.1039/D0RE00093K, Paper
Yang Li, Meng Hao, Ming Xia, Ning Sun, Cai-Lin Zhang, Wen-Qing Zhu
1,3-Butadienes play a key role in modern synthetic chemistry and biochemistry because they are well-known precursors for the synthesis of retinoids.
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synthesis

Assessing the impact of deviations in optimized multistep flow synthesis on the scale-up

React. Chem. Eng., 2020, 5,838-848
DOI: 10.1039/D0RE00025F, Perspective
M. K. Sharma, J. Raval, Gwang-Noh Ahn, Dong-Pyo Kim, A. A. Kulkarni
This manuscript highlights the unavoidable connection between manual and self-optimized flow synthesis protocols for multistep flow synthesis and its scale-up.
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synthesis

Optimization of the direct synthesis of dimethyl ether from CO2 rich synthesis gas: closing the loop between experimental investigations and model-based reactor design

React. Chem. Eng., 2020, 5,949-960
DOI: 10.1039/D0RE00041H, Paper
Open Access
Nirvana Delgado Otalvaro, Markus Kaiser, Karla Herrera Delgado, Stefan Wild, Jörg Sauer, Hannsjörg Freund
Kinetic modeling, model-based optimization and experimental validation for the direct DME synthesis.
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synthesis

Organic electrosynthesis: from academia to industry

React. Chem. Eng., 2020, Advance Article
DOI: 10.1039/D0RE00064G, Review Article
Matthew C. Leech, Anthony D. Garcia, Alessia Petti, Adrian P. Dobbs, Kevin Lam
The growing impetus to develop greener and more cost-efficient synthetic methods has prompted chemists to look for new ways to activate small organic molecules. In this review, we cover the most recent industrial developments in electrosynthesis.
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synthesis

Continuous liquid-phase synthesis of nickel phosphide nanoparticles in a helically coiled tube reactor

React. Chem. Eng., 2020, Accepted Manuscript
DOI: 10.1039/D0RE00010H, Paper
Huidong Zheng, Donglin Li, Jingjing Chen, Jie Liu, Zuoyi Yan, S. Ted Oyama
The continuous liquid phase synthesis of nickel phosphide (Ni2P) nanoparticles was studied in a helically coiled tube (HCT) reactor both in single-phase and two-phases slug flow. The reactants were nickel...
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synthesis

[ASAP] Synthesis and Cytotoxicity Studies of Stilbene Long-Chain Fatty Acid Conjugates

Journal of Natural Products
DOI: 10.1021/acs.jnatprod.0c00027




synthesis

[ASAP] Synthesis of the 1,2,4-Thiadiazole Alkaloid Polyaurine B

Journal of Natural Products
DOI: 10.1021/acs.jnatprod.0c00166




synthesis

[ASAP] Correction to Corrected Structure of Natural Hyacinthacine C<sub>1</sub> via Total Synthesis

Journal of Natural Products
DOI: 10.1021/acs.jnatprod.0c00389




synthesis

[ASAP] Total Synthesis of Isohericenone J via a Stille Coupling Reaction

Journal of Natural Products
DOI: 10.1021/acs.jnatprod.9b01251




synthesis

[ASAP] Advances in the Biosynthesis of Pyranocoumarins: Isolation and <sup>13</sup>C-Incorporation Analysis by High-Performance Liquid Chromatography–Ultraviolet–Solid-Phase Extraction–Nuclear Magnetic Resonance Data

Journal of Natural Products
DOI: 10.1021/acs.jnatprod.9b00607




synthesis

Breast Cancer Screening Using Tomosynthesis in Combination With Digital Mammography

Interview with Sarah M. Friedewald, MD, author of Breast Cancer Screening Using Tomosynthesis in Combination With Digital Mammography




synthesis

[ASAP] Controlling Cluster Intermediates Enables the Synthesis of Small PbS Nanocrystals with Narrow Ensemble Line Widths

Chemistry of Materials
DOI: 10.1021/acs.chemmater.0c00984




synthesis

[ASAP] Hydrothermal Stability of High-Surface-Area a-Al<sub>2</sub>O<sub>3</sub> and Its Use as a Support for Hydrothermally Stable Fischer–Tropsch Synthesis Catalysts

Chemistry of Materials
DOI: 10.1021/acs.chemmater.0c01587




synthesis

ISLAM IN THE NIGER DELTA 1890-2017: a synthesis of the accounts of indigenes and migrants.

Rotch Library -




synthesis

[ASAP] Development of a Robust Protocol for the Synthesis of 6-Hydroxybenzofuran-3-carboxylic Acid

Organic Process Research & Development
DOI: 10.1021/acs.oprd.9b00546