The sin2ψ and cosα methods are compared via diffracting-grain identification from electron backscatter diffraction maps. Artificial textures created by the X-ray diffraction measurements are plotted and X-ray elastic constants of the diffracting-grain sets are computed.

Book review

Book review

This article presents the capability of the QMAX furnace, devoted to reciprocal space mapping through X-ray scattering at high temperature up to 2000 K.

The proton-conducting material (NH4)4H2(SeO4)3 is examined to check whether its conductivity spectra are sensitive to subtle changes in the crystal structure and proton dynamics caused by external pressure. The AC conductivity was measured using impedance spectroscopy, in the frequency range from 100 Hz to 1 MHz, at temperatures 260 K < T < 400 K and pressures 0.1 MPa < p < 500 MPa. On the basis of the impedance spectra, carefully analyzed at different thermodynamic conditions, the p–T phase diagram of the crystal is constructed. It is found to be linear in the pressure range of the experiment, with the pressure coefficient value dTs/dp = −0.023 K MPa−1. The hydrostatic pressure effect on proton conductivity is also presented and discussed. Measurements of the electrical conductivity versus time were performed at a selected temperature T = 352.3 K and at pressures 0.1 MPa < p < 360 MPa. At fixed thermodynamic conditions (p = 302 MPa, T = 352.3 K), the sluggish solid–solid transformation from low conducting to superionic phase was induced. It is established that the kinetics of this transformation can be described by the Avrami model with an effective Avrami index value of about 4, which corresponds to the classical value associated with the homogeneous nucleation and three-dimensional growth of a new phase.

The proton-conducting crystal (NH4)4H2(SeO4)3 is examined to check whether its conductivity spectra and the phase transition to the superprotonic phase are sensitive to subtle changes in the crystal structure and proton dynamics caused by various thermodynamic conditions. It is established that the kinetics of this transformation can be described using the Avrami model with an effective Avrami index value associated with homogeneous nucleation and three-dimensional growth of a new phase.

Most articles dealing with R2TSi3 compounds are only interested in one specific composite or in a series of composites with varying T elements while keeping R fixed (or vice versa). The present work gives an overview of the complete range of 2:1:3 silicides, similar those of Hoffmann & Pöttgen (2001) and Pan et al. (2013). In contrast to the work of Hoffmann & Pöttgen (2001), reasons for formation of the different symmetries and superstructures are discussed. Here, crystallographic properties are in[the] focus, whereas physical and magnetic properties are omitted because those are given by Pan et al. (2013). READS LIKE AN ABSTRACT, please re-write and remove references if possible. Should be two sentences max.

The title compound, C11H11NO5, has a nearly planar geometry. In the crystal, the molecules are assembled into chains parallel to the [overline{1}11] direction by O—H...O and C—H...O hydrogen bonds.

In the title compound, {[Cu(C14H8O4)(C11H10N4O)(H2O)]·1.25H2O}n, the CuII cations are coordinated in a square-pyramidal fashion by trans carboxylate O-atom donors from two diphenate (dip) ligands, trans pyridyl N-atom donors from two bis(4-pyridyl)urea (bpu) ligands, and a ligated water molecule in the apical position. [Cu(H2O)(dip)(bpu)]n coordination polymer layer motifs are oriented parallel to (overline{1}02). These layer motifs display a standard (4,4) rectangular grid topology and stack in an AAA pattern along the a-axis direction to form the full three-dimensional crystal structure of the title compound, mediated by N—H...O and O—H...O hydrogen bonding patterns involving the water molecules of crystallization.

A single-chain, tailless Xenopus laevis H2A/H2B dimer construct (scH2BH2A) was engineered by directly fusing the C-terminus of H2B to the N-terminus of H2A without an artificial linker sequence. A high-resolution crystal structure of scH2BH2A shows that it adopts a nearly identical fold to that of nucleosomal H2A/H2B and may be useful for future structural studies of many H2A/H2B-interacting proteins.

This article reports conformational polymorphisms of the EF-hand protein MCFD2 which is involved in glycoprotein transport..

Endoplasmic reticulum (ER)-associated degradation (ERAD) is a protein quality-control pathway in eukaryotes in which misfolded ER proteins are polyubiquitylated, extracted and ultimately degraded by the proteasome. This process involves ER membrane-embedded ubiquitin E2 and E3 enzymes, as well as a soluble E2 enzyme (Ubc7 in Saccharomyces cerevisiae and UBE2G2 in mammals). E2-binding regions (E2BRs) that recruit these soluble ERAD E2s to the ER have been identified in humans and S. cerevisiae, and structures of E2–E2BR complexes from both species have been determined. In addition to sequence and structural differences between the human and S. cerevisiae E2BRs, the binding of E2BRs also elicits different biochemical outcomes with respect to E2 charging by E1 and E2 discharge. Here, the Schizosaccharomyces pombe E2BR was identified and purified with Ubc7 to resolve a 1.7 Å resolution co-crystal structure of the E2BR in complex with Ubc7. The S. pombe E2BR binds to the back side of the E2 as an α-helix and, while differences exist, it exhibits greater similarity to the human E2BR. Structure-based sequence alignments reveal differences and conserved elements among these species. Structural comparisons and biochemistry reveal that the S. pombe E2BR presents a steric impediment to E1 binding and inhibits E1-mediated charging, respectively.

The crystal structure of MgCoGa2 (magnesium cobalt digallide) was solved by direct methods and refined in two space groups as P21/c (standard choice) and P21/n (non-standard choice). The refined lattice parameters for the standard choice are a = 5.1505 (2), b = 7.2571 (2), c = 8.0264 (3) Å and β = 125.571 (3)°, and for the non-standard choice are a = 5.1505 (2), b = 7.2571 (2), c = 6.5464 (2) Å and β = 94.217 (3)°. All parameters for MgCoGa2 refined to R1 = 0.027 and wR2 = 0.042 using 594 reflections. The crystal structure peculiarities of this compound are discussed. Particular attention has been given to relationships with other similar structures, such as YPd2Si and Fe3C. Crystallographic analysis, together with linear muffin-tin orbital electronic structure calculations, reveals the presence of three-dimensional polyatomic nets with partial covalent bonding between the Ga atoms.

The Smithsonian Center for Education and Museum Studies is hosting “Climate Change,” a three-day, free, education online conference Tuesday, Sept. 29 through Thursday, Oct. 1. This […]

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A major new exhibition hall dedicated to the discovery and understanding of human origins will open next year at the Smithsonian's National Museum of Natural History: The David H. Koch Hall of Human Origins

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White, who was a student at Columbian College from Accomack County, Va., died of pneumonia and complications from a mitral heart defect. When his coffin was unearthed, his identity was a deep mystery.

The post Remains of William Taylor White (1837-1852) donated to Smithsonian with his coffin and clothing appeared first on Smithsonian Insider.

Long before dawn on a recent morning, Katie Milton and a group of stalwart volunteers, each armed with flashlight and compass, spread out into the jungle to take up positions at 35 listening stations marked on maps of the island.

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The funding will allow the National Science Resources Center to validate its LASER (Leadership Assistance for Science Education Reform) Model. LASER, a systemic approach to reform, is a set of processes and strategies designed to help state, district and school leadership teams effectively implement and sustain
high-quality science education for elementary, middle and secondary school students.

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Data from a recent study of wild takins in the high-altitude forests of the Tangjiahe National Nature Reserve in southeast China has shown that the […]

The post Great Sichuan earthquake of 2008 had little impact on of China’s wild takins appeared first on Smithsonian Insider.

“Places of Invention,” a planned 3,500-square-foot exhibition at the National Museum of American History scheduled to open in 2014, will feature a selection of “hot spots” of invention and innovation—places where a critical mass of inventive people, networks, institutions, funding and other resources come together and creativity flourishes.

The post Lemelson Center receives $2.6 million grant for informal science education appeared first on Smithsonian Insider.

The awarded film features STRI marine biologist Héctor M. Guzman diving with a group of five whale sharks while traveling in the Tropical Eastern Pacific. In the video, Guzmán tags a radiotransmitter to one of the sharks in order to follow its voyages.

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Giant squid eye, 2008 Giant squid have the largest eyes in the animal kingdom—at up to 10 inches in diameter, they are the size of […]

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Collecting trips for Charles Doolittle Walcott (1850-1927), paleontologist and fourth Secretary of the Smithsonian Institution, were often a family affair. This 1910 photograph shows their […]

The post Charles Doolittle Walcott (1850-1927) family campsite in the Canadian Rockies appeared first on Smithsonian Insider.

Astronomers have discovered a new comet that they expect will be visible to the naked eye in early 2013.A preliminary orbit computed by the Minor Planet Center at the Smithsonian Astrophysical Observatory in Cambridge, Mass., shows that the comet will come within about 30 million miles of the sun in early 2013, about the same distance as Mercury. The comet will pose no danger to Earth.

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University of Florida and Smithsonian Tropical Research Institute scientists describe a new 20-foot extinct species of crocodile discovered in the same Colombian coal mine with Titanoboa, the world’s largest snake.

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The fastest wind ever discovered blowing off a disk around a stellar-mass black hole has been observed by a team of astronomers using NASA’s Chandra X-ray Observatory.

The post Chandra X-ray Observatory clocks stellar wind at 20 million mph appeared first on Smithsonian Insider.

Jeholopsyche liaoningensis is a new genus and species of flying insect from northeastern China, recently revealed in two new fossil specimens.

The post Meet the 125-million-year-old pollinator “Jeholopsyche liaoningensis” appeared first on Smithsonian Insider.

This composite image from the Chandra X-ray Observatory (operated for NASA by the Smithsonian Astrophysical Observatory) shows the distribution of dark matter, galaxies, and hot […]

The post Chandra image of the core of the merging galaxy cluster Abell 520 appeared first on Smithsonian Insider.

An international team of scientists has discovered an ‘ordinary’ black hole in the galaxy Centaurus A. This is the first time that a normal-size black hole has been detected away from the immediate vicinity of our own Galaxy.

The post “Ordinary” black hole discovered in a galaxy 12-million-light-years away appeared first on Smithsonian Insider.

To celebrate the 10th anniversary of researchers producing the first complete human genome sequence — the genetic blueprint of the human body — the Smithsonian’s National Museum of Natural History, will open a new high-tech, high-intensity exhibition in 2013.

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“The Age of Plastic: Ingenuity + Responsibility” a public Smithsonian Symposium that will take an uncommon look at the most common of materials. On Thursday, June […]

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Coral reefs worldwide are being destroyed by changes in ocean temperature and chemistry faster than at any time since the last reef crisis 55 million years ago, thousands of marine scientists warned from the International Coral Reef Symposium in Cairns, Australia.

The post Coral reef emergency: 2,600 scientists call for worldwide rescue appeared first on Smithsonian Insider.

A July 12 news alert from NASA indicates a X1.4 class solar flare erupted from the center of the Sun, peaking July 12 at 12:52 P.M.

The post Coronal mass ejection from July 12 solar flare headed toward Earth; minor geomagnetic storm activity predicted appeared first on Smithsonian Insider.

Deep observations with NASA's Chandra X-ray Observatory of Cygnus OB2 have been used to detect the X-ray emission from the hot outer atmospheres, or coronas, of young stars in the cluster and to probe how these great star factories form and evolve.

The post Cygnus OB2: Probing a nearby stellar cradle appeared first on Smithsonian Insider.

This image shows the active star-forming galaxy M82 in three wavelengths: UV (blue), near-infrared (green) and far-infrared (red). New research indicates that even in the […]

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Domestic cats in the United States kill some 2.4 billion birds and 12.3 billion mammals each year, most of them native mammals like shrews, chipmunks […]

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In our solar system, only one planet is blessed with an ocean: Earth. Our home world is a rare, blue jewel compared to the deserts […]

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Investigators from Rock County, Wisconsin, are one step closer to solving the mystery surrounding the death of an unknown teenager thanks to Smithsonian scientists. Christine […]

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While it seems that we can find just about anything on the Internet, it doesn’t mean we know everything yet. Every year, Smithsonian scientists discover […]

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For the first time, scimitar-horned oryx are going to be reintroduced to the wild in Chad. Extinct in the wild since the mid-1980s, the species’ […]

The post 25 Scimitar-Horned Oryx to be Reintroduced to the Wild in Chad appeared first on Smithsonian Insider.

Ricardo Moreno, research associate at the Smithsonian Tropical Research Institute (STRI) in Panama and director of the Yaguará Panamá Foundation, reported at the 20th Congress […]

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“Probably no genus of birds in the American avifauna has received the amount of attention that has been bestowed upon the turkeys…there has been no […]

The post Happy Thanksgiving! Here are 25 fun turkey-related objects in Smithsonian collections! appeared first on Smithsonian Insider.

When “2001: A Space Odyssey” premiered April 2, 1968 at Washington, D.C.’s Uptown Theater—not far from the Smithsonian’s National Air and Space Museum—not everyone was […]

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