synthesis

Development and Functionalization of Magnetic Nanoparticles as Stable and Reusable Catalyst for Triacetin Synthesis

New J. Chem., 2020, Accepted Manuscript
DOI: 10.1039/D0NJ00488J, Paper
Abida Khan, Bhupendra Chudasama, Amjad Ali
The application of magnetic nanoparticles as an adsorbent and catalyst support in solving the environmental issues has recently received great attention due to their unique physical and chemical properties, such...
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synthesis

Controllable synthesis of an intercalated SnS2/aEG structure for enhanced NO2 gas sensing performance at room temperature

New J. Chem., 2020, Accepted Manuscript
DOI: 10.1039/D0NJ01005G, Paper
Laifeng Ma, Xueyi Zhang, Jue Wang, Muhammad Ikram, Mohib Ullah, He Lv, Hongyuan Wu, Keying Shi
Intercalated SnS2/actived expanded graphite (SnS2/aEG) nanocomposites (NCs) were prepared via vacuum-assistant and facile solvothermal technique. It suggests that SnS2 nanoflowers (NFs) evenly distribute on the surface and interlayer of aEG...
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synthesis

Ultrasonic Promoted Synthesis of Ag Nanoparticles Decorated Thiourea–Functionalized Magnetic Hydroxyapatite: A Robust Inorganic–Organic Hybrid Nanocatalyst for Oxidation and Reduction Reactions

New J. Chem., 2020, Accepted Manuscript
DOI: 10.1039/D0NJ00829J, Paper
Saeed Bahadorikhalili, Hosein Arshadi, Zahra Afrouzandeh, Leila Ma'mani
In this research, ultrasonic synthesis is applied for the fabrication of a novel catalyst, based on immobilization of silver nanoparticles (AgNPs) on thiourea functionalized magnetic hydroxyapatite. Recoverable Ag nano–catalyst is...
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synthesis

An expedient synthesis of new imino-thiazolidinone grafted dispiro-pyrrolidine-oxindole/indeno hybrids via a multicomponent [3+2] cycloaddition reaction in a deep eutectic solvent

New J. Chem., 2020, Advance Article
DOI: 10.1039/D0NJ00801J, Paper
Ruby Singh, Munna Ram Saini, Diksha Bhardwaj, Aakash Singh
A facile and selective synthesis of novel factionalized dispiro-pyrrolidines via a three component [3+2] cycloaddition reaction using a deep eutectic solvent.
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synthesis

A facile synthesis of Ru/N–C as an efficient and cost-effective electrocatalyst for hydrogen evolution

New J. Chem., 2020, Advance Article
DOI: 10.1039/D0NJ01227K, Paper
Zichuang Li, Yu Pei, Qiangjian Ju, Beibei Guo, Yifan Hu, Qian Liu, Yufang Zhu, Jiacheng Wang
This work provides a HER catalyst synthesis strategy with performance comparable to commercial Pt/C at a cost of only 0.6%.
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synthesis

Physicochemical properties of a urea/zinc chloride eutectic mixture and its improved effect on the fast and high yield synthesis of indeno[2,1-c]quinolines

New J. Chem., 2020, Advance Article
DOI: 10.1039/D0NJ01342K, Paper
Diana Peña-Solórzano, Vladimir V. Kouznetsov, Cristian Ochoa-Puentes
An environmentally friendly and efficient method for the synthesis of indeno[2,1-c]quinolines is developed using a urea/zinc chloride eutectic mixture as a green mildly acidic medium.
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synthesis

Non-Photoisomerizable Butterfly Shaped Tetrasubstituted Azobenzenes: Synthesis and Photophysical Studies

New J. Chem., 2020, Accepted Manuscript
DOI: 10.1039/D0NJ01092H, Paper
Raman Arunachalam, Afeefah U Neelambra, Venugopal Karunakaran, Easwaramoorthi Shanmugam
The trans-azobenzene (AB) substituted derivatives with bulky carbazole (1), phenothiazine (2), and phenyl (3) have been synthesized to understand the effect of steric crowding around –N=N– linkage on the photoisomerization...
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synthesis

Synthesis of 3-halochromones with simple KX halogen sources enabled by in situ halide oxidation

New J. Chem., 2020, Advance Article
DOI: 10.1039/D0NJ00825G, Paper
Yan Lin, Jie-Ping Wan, Yunyun Liu
An in situ oxidation strategy for generating molecular halogen has been developed for the synthesis of 3-halochromones by employing simple potassium halides as halogen sources.
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synthesis

Synthesis of characteristic polyisoprenes using rationally designed iminopyridyl metal (Fe and Co) precatalysts: investigation of co-catalysts and steric influence on their catalytic activity

New J. Chem., 2020, Advance Article
DOI: 10.1039/D0NJ00942C, Paper
Wenhua Lin, Liping Zhang, Hongyi Suo, Arumugam Vignesh, Nighat Yousuf, Xiang Hao, Wen-Hua Sun
A series of iminopyridyl ligand-based iron and cobalt complexes are utilized as catalysts in isoprene polymerization, in which the microstructure of resultant polyisoprenes was investigated.
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synthesis

Synthesis of eight isostructural 2D lanthanide coordination polymers assembled by rigid furan-2,5-dicarboxylic acid and flexible adipic acid as linkers and exploration of luminescent Eu/Tb polymers as efficient and sensitive sensors for nitroaromatic comp

New J. Chem., 2020, Advance Article
DOI: 10.1039/D0NJ01018A, Paper
Zaib ul Nisa, Lobzang Tashi, Charanjeet Sen, Nargis Akhter Ashashi, Subash Chandra Sahoo, Haq Nawaz Sheikh
Eight isostructural coordination polymers were synthesized by a solvothermal method. The luminescent Eu/Tb polymers function as efficient sensors for nitroaromatics via turn-off mode.
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synthesis

Recent progress and approaches on the synthesis of Mn-doped zinc oxide nanoparticles: A theoretical and experimental investigation on the photocatalytic performance

New J. Chem., 2020, Accepted Manuscript
DOI: 10.1039/D0NJ01530J, Paper
Joyce Silva, Nivaldo Freire Andrade Neto, Marisa Carvalho Oliveira, Renan Pontes Ribeiro, S Lazaro, Yara Gomes, Carlos Paskocimas, Mauricio Bomio, Fabiana Motta
Transition metal-doped semiconductors are promising to conduct the future of environmental remediation from photocatalysis. In this study, the role of Mn-doping on the structural, electronic, morphological, optical, and photocatalytic properties...
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synthesis

Synthesis and herbicidal application of turpentine derivative p-menthene type secondary amines as sustainable agrochemicals

New J. Chem., 2020, Advance Article
DOI: 10.1039/D0NJ00583E, Paper
Huanhuan Dong, Shichao Xu, Jing Wang, Hongmei Zhang, Yuxiang Chen, Liangwu Bi, Zhendong Zhao
Compound 3a showed excellent herbicidal activity against barnyard grass with IC50 = 7.0 mg L−1, and exhibited good selection for rice, wheat, and radish at 100 mg L−1.
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synthesis

Synthesis of a new Ni complex supported on CoFe2O4 and its application as an efficient and green catalyst for the synthesis of bis(pyrazolyl)methane and polyhydroquinoline derivatives

New J. Chem., 2020, Advance Article
DOI: 10.1039/D0NJ00223B, Paper
Taiebeh Tamoradi, Seyedeh Masoumeh Mousavi, Masoud Mohammadi
A novel and magnetic nanocatalyst was synthesized for the synthesis of multicomponent compounds.
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synthesis

A Size-Controlled Green Synthesis of Silver Nanoparticles by the Berry Extract of Sea Buckthorn and the Biological Activities

New J. Chem., 2020, Accepted Manuscript
DOI: 10.1039/D0NJ01335H, Paper
Simin Wei, Yinghui Wang, Zhishu Tang, Jinhang Hu, Su Rui, Lin Jingjie, Zhou Tuan, Hui Guo, Wang Nan, Xu Rongrong
Green synthesis of silver nanoparticles (AgNPs) has been extensively studied by using a variety of plant extracts for the applications in biomedical sciences and engineering. However, there are no reports...
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synthesis

Single-pot template-free synthesis of a glycerol-derived C–Si–Zr mesoporous composite catalyst for fuel additive production

New J. Chem., 2020, Advance Article
DOI: 10.1039/D0NJ00523A, Paper
Saurabh Kumar, Nagabhatla Viswanadham, Sandeep K. Saxena, Arumugam Selvamani, Jitendra Diwakar, Ala’a H. Al-Muhtaseb
The C–Si–Zr material synthesized from bio-derived waste glycerol, ZrO(NO3)2 and TEOS exhibits excellent catalytic activity for tri-acetin production from low-value glycerol.
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synthesis

Design, Synthesis and Evaluation of A Novel Glutamine Derivative (2S,4R)-2-amino-4-cyano-4-[18F]fluoro-butanoic acid

New J. Chem., 2020, Accepted Manuscript
DOI: 10.1039/D0NJ00410C, Paper
song Liu, Renbo Wu, Yuli Sun, Karl Ploessl, Yan Zhang, Yajing Liu, zehui wu, Lin Zhu, H. F. Kung
Glutamine is an important source of nutrient for tumor proliferation. Designing new glutamine-metabolizing PET imaging agents is useful for tumor diagnosis and treatment. Herein, a novel glutamine derivative, (2S,4R)-2-amino-4-cyano-4-[18F]fluoro-butanoic acid,...
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synthesis

Conjugated Small Organic Molecules: Synthesis and Characterization of 4- Arylpyrazole-decorated Dibenzothiophenes

New J. Chem., 2020, Accepted Manuscript
DOI: 10.1039/D0NJ01887B, Paper
M. Bhanuchandra, Satyajit Panda, Ram Singh Jat, Amir Fayaz, Jony Saha, Ramalingam Thirumoorthi , Tapta Kanchan Roy
4-Arylpyrazole-decorated dibenzothiophenes have been synthesized. The synthesis involves the treatment of 2,8-dibromodibenzothiophene with pyrazole under Ullmann-type amination conditions for the dual C-N bond formation. The selective bromination of the resulting...
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synthesis

[ASAP] Structural and Biological Basis of Small Molecule Inhibition of <italic toggle="yes">Escherichia coli</italic> LpxD Acyltransferase Essential for Lipopolysaccharide Biosynthesis

ACS Infectious Diseases
DOI: 10.1021/acsinfecdis.9b00127




synthesis

[ASAP] Design, Synthesis, and Bioactivity of Cyclic Lipopeptide Antibiotics with Varied Polarity, Hydrophobicity, and Positive Charge Distribution

ACS Infectious Diseases
DOI: 10.1021/acsinfecdis.0c00056




synthesis

Emerging investigator series: synthesis of magnesium oxide nanoparticles fabricated on a graphene oxide nanocomposite for CO2 sequestration at elevated temperatures

Environ. Sci.: Nano, 2020, 7,1225-1239
DOI: 10.1039/C9EN01442J, Paper
C. A. Gunathilake, G. G. T. A. Ranathunge, R. S. Dassanayake, S. D. Illesinghe, Amanpreet S. Manchanda, C. S. Kalpage, R. M. G. Rajapakse, D. G. G. P. Karunaratne
MONP and MONP–GO sorbents exhibited relatively high CO2 sorption capacity (2.79–3.34 mmol g−1) under elevated temperature conditions.
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synthesis

Designed synthesis of unique ZnS@CdS@Cd0.5Zn0.5S-MoS2 hollow nanospheres for efficient visible-light-driven H2 evolution

CrystEngComm, 2020, 22,2743-2755
DOI: 10.1039/D0CE00064G, Paper
Bowen Sun, Hui Wang, Jiakun Wu, Yanling Geng, Jixiang Xu, Yaowei Wang, Yanyan Li, Haifeng Lin, Lei Wang
Unique ZnS@CdS@Cd0.5Zn0.5S-MoS2 hollow nanospheres with abundant active sites and enhanced light-harvesting and charge separation demonstrate efficient H2 evolution from visible-light-driven water-splitting.
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synthesis

Heterobimetallic complexes from 0D clusters to 3D networks based on various polycyanometallates and [Cu(dmpn)2]2+ (dmpn = 2,2-dimethyl-1,3-diaminopropane): synthesis, crystal structures and magnetic properties

CrystEngComm, 2020, 22,2806-2816
DOI: 10.1039/D0CE00235F, Paper
Xiaoyun Hao, Jingwen Shi, Yong Dou, Tong Cao, Zhen Zhou, Lu Yang, Dacheng Li, Qingyun Liu, Jianzhuang Jiang, Daopeng Zhang
Six new cyanide-bridged complexes (0–3D) have been assembled by employing one copper compound and six cyano precursors. Investigation of the magnetic properties revealed the ferro- or antiferromagnetic coupling between FeIII/CrI ion and CuII ion.
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synthesis

Synthesis of all-silica hollow zeolites by selective demetallation

CrystEngComm, 2020, 22,2845-2848
DOI: 10.1039/D0CE00263A, Paper
Open Access
Teng Li, Frank Krumeich, Jeroen A. van Bokhoven
Exploiting the protective role of extra-framework aluminum species on the crystal rim, all-silica hollow zeolites are efficiently produced by demetallation.
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synthesis

Synthesis and investigation alkaline energetic coordination polymers based on 1,2,3-triazole-4,5-dicarboxylic acid for green component of pyrotechnic

CrystEngComm, 2020, Accepted Manuscript
DOI: 10.1039/D0CE00317D, Paper
Zhen-Li Yang, Jian Qin, Jun- Qing Yang , Jianguo Zhang
Research on novel energetic coordination polymers (ECPs) is becoming increasingly important for energetic materials, numerous ECPs were reported and found to be potential energetic materials. In this study, 4,5-dicarboxylic-1,2,3-triazolean was...
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synthesis

Mesoporogen-free synthesis of hierarchical HZSM-5 for LDPE catalytic cracking

CrystEngComm, 2020, Accepted Manuscript
DOI: 10.1039/D0CE00255K, Paper
Yunhao Zang, Jinying Wang, Jianfeng Gu, Jiangying Qu, Feng Gao
Herein, a mesoporogen-free, and steam-assisted route is proposed to synthesize highly crystalline hierarchical HZSM-5 using Stöber silica spheres as the precursor. The effect of crystallization time on the morphology and...
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synthesis

Synthesis of the finger-like MoS2@VS2 micro-nano composite with enhanced field emission performance

CrystEngComm, 2020, Accepted Manuscript
DOI: 10.1039/D0CE00347F, Paper
Yu Feng, Erwei Du, Shijing Gong, Ke Yu, Xiaofan Chen, Ziqiang Zhu
The MoS2@VS2 micro-nano composite was synthesized via a two-step hydrothermal method. The field emission properties of MoS2@VS2 micro-nano composite were investigated for the first time. The finger-like VS2 has a...
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synthesis

A novel synthesis of YVO4:Ln3+ (Ln = Eu, Sm, and Dy) porous/hollow submicro-ellipsoids and their luminescence properties

CrystEngComm, 2020, Advance Article
DOI: 10.1039/D0CE00526F, Paper
Shuang Zhao, Baiqi Shao, Yang Feng, Senwen Yuan, Langping Dong, Liang Zhang, Hongpeng You
A novel synthesis strategy of porous/hollow YVO4 submicro-ellipsoids with multicolor emissions has been developed based on the high structural matching of LYH and YVO4.
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synthesis

Graphene-based SiC nanowires with nanosheets: synthesis, growth mechanism and photoluminescence properties

CrystEngComm, 2020, Advance Article
DOI: 10.1039/D0CE00297F, Paper
Zhihui Hu, Zhi Chen, Juntong Huang, Mingge Yan, Meng Zhang, Lei Zhang, Xibao Li, Zhijun Feng
3C-SiC nanowires with nanosheets were synthesized via a direct reaction of Si vapor (from solid silicon) and SiO vapor (from silicon and silicon dioxide) with graphene nanosheets at 1500 °C without any additional metal catalyst.
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synthesis

Hydrothermal synthesis and tunable up-conversion white luminescence properties of KSc(MoO4)2:Ln3+ (Ln = Yb, Er, Tm and Ho) crystals

CrystEngComm, 2020, Advance Article
DOI: 10.1039/D0CE00253D, Paper
Yini Mao, Li Jiang, Pengfei Xian, Qiongfen Fu, Shanshan Hu, Jun Yang
Pure hexagonal phase KSc(MoO4)2 crystals with a hexagonal block shape were successfully synthesized via a one-step hydrothermal method.
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synthesis

Lanthanide doped bismuth-based fluoride nanoparticles: controlled synthesis and ratiometric temperature sensing

CrystEngComm, 2020, Accepted Manuscript
DOI: 10.1039/D0CE00435A, Paper
Pengpeng Lei, Ran An, Chengyu Li, Jing Feng, Hongjie Zhang
Bismuth-based nanoparticles, especially NaBiF4, have attracted extensive attention as hosts of lanthanides (Ln3+) ions and other luminescent ions in recent years. However, controllable synthesis of NaBiF4 nanoparticles remains a challenge....
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synthesis

Biological activity tuning of antibacterial urotropine via co-crystallization: synthesis, biological activity evaluation and computational insight

CrystEngComm, 2020, Advance Article
DOI: 10.1039/D0CE00226G, Paper
Nida Tabassum, Panayiotis C. Varras, Fiza Arshad, Muhammad I. Choudhary, Sammer Yousuf
Urotropine (1) is a synthetic heterocyclic antibacterial agent.
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synthesis

New pronounced progress in the synthesis of group 5 polyoxometalates

CrystEngComm, 2020, Advance Article
DOI: 10.1039/D0CE00315H, Highlight
Joanna Dopta, Lisa K. Mahnke, Wolfgang Bensch
This highlight summarizes new developments made in group 5 polyoxometalate science of high nuclearity clusters with focus on synthetic approaches.
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synthesis

Synthesis, Structural Characterization, Physicochemical Properties and Transformations of Dehydroevodiamine and Its Hydrochloride Salts

CrystEngComm, 2020, Accepted Manuscript
DOI: 10.1039/D0CE00136H, Paper
Guoshun Zhang, xiaoqing shang, wei han, lifeng zhang, guolian ren, Shuqiu Zhang
As a quinazolinocarboline alkaloid, dehydroevodiamine (DHED) derived from Evodia rutaecarpa has recently gained attention because it improves memory failure in Alzheimer's mice. However, its solid forms, which have not yet...
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synthesis

Facile One–pot Solvothermal Synthesis of CdTe Nanorods and Their Photoelectrical Properties

CrystEngComm, 2020, Accepted Manuscript
DOI: 10.1039/D0CE00459F, Communication
Binnian Zhong, Weifeng Kang, Zhiwei Zhang, Linhui Zhang, Bin Ma
Uniform CdTe NRs were synthesized by a one-pot PVP-assisted solvothermal process under mild conditions. By adjusting the amounts of the surfactant, reducing agent and the reaction temperature, CdTe NRs with...
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synthesis

Nanostructured semiconductors in porous alumina matrices: modeling, synthesis, and properties / Rishat G. Valeev, PhD, Alexander V. Vakhrushev, DSc, Aleksey Yu. Fedotov, PhD, Dmitrii I. Petukhov, PhD ; editorial board members, A.N. Beltiukov, A.L. Trigub,

Online Resource




synthesis

Nanowires and nanotubes--synthesis, properties, devices and energy applications od one-dimensional materials: symposium held April 9-13, 2012, San Francisco, California, U.S.A. / editors, Junichi Motohisa ... [et al.]

Hayden Library - TA418.9.N35 N396 2012




synthesis

Nanowires: properties, synthesis, and applications / Vincent Lefèvre, editor

Barker Library - TK7874.85.N365 2012




synthesis

Solution synthesis of inorganic films and nanostructured materials: symposium held April 9-13, 2012, San Francisco, California, U.S.A. / editors, Menka Jain ... [et al.]

Hayden Library - TA418.9.N35 S967 2012




synthesis

Sustainable Synthesis of Nanomaterials: November 28 - December 3, 2011, Boston, Massachusetts, USA / editors H. Fan, M. Knez, S. S. Wong, W. Lee

Hayden Library - TA418.9.N35 S87 2011




synthesis

Solution synthesis of inorganic functional materials -- films, nanoparticles and nanocomposites: symposium held April 1-5, 2013, San Francisco, California, U.S.A. / editors, Menka Jain, Quanxi Jia, Teresa Puig, Hiromitsu Kozuba

Hayden Library - TA418.9.N35 S656 2013




synthesis

Magnetic nano- and microwires: design, synthesis, properties and applications / edited by Manuel Vázquez

Barker Library - TK7874.85




synthesis

Semiconductor nanowires - synthesis, properties and applications: April 21-25, 2014, San Francisco, California, USA / editors, Y. Zhu, S. Gradecak, Y. Gu, J. Spanier

Hayden Library - TK7874.85.M425 2014




synthesis

In-situ characterization of material synthesis and properties at the nanoscale with TEM: April 21-25 2014, San Francisco California, USA / editors, M. Chi

Hayden Library - TK7874.85.I55 2014




synthesis

Nanotechnology: synthesis to applications / edited by Sunipa Roy, Chandan Kumar Ghosh, and Chandan Kumar Sarkar

Hayden Library - T174.7.N345524 2018




synthesis

Synthesis of Biaryl Ketones by Arylation of Weinreb Amides with Functionalized Grignard Reagents under Thermodynamic Control vs. Kinetic Control of N,N-Boc2-Amides

Org. Biomol. Chem., 2020, Accepted Manuscript
DOI: 10.1039/D0OB00813C, Communication
Guangchen Li, Michal Szostak
A highly efficient method for chemoselective synthesis of biaryl ketones by arylation of Weinreb amides (N-methoxy-N- methylamides) with functionalized Grignard reagents is reported. This protocol offers rapid entry to functionalized...
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synthesis

Highly Z-selective synthesis of 1,3-oxathiol-2-ylidenes and 4-methylene-oxazolidine-2-thiones via atom-specific 5-exo-dig cyclization of propargyl alcohol with isothiocyanate

Org. Biomol. Chem., 2020, Advance Article
DOI: 10.1039/D0OB00083C, Paper
S. Antony Savarimuthu, D. G. Leo Prakash, S. Augustine Thomas, Thirumanavelan Gandhi, Mrinal K. Bera
The Z-selectivity observed in imine and alkene motifs after 5-exo-dig cyclization of propargyl alcohol and isothiocyanate is rare in the literature and this selectivity can be attributed to electronic and steric factors of the imine and alkene motif respectively.
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synthesis

Selenium-promoted electrophilic cyclization of arylpropiolamides: synthesis of 3-organoselenyl spiro[4,5]trienones

Org. Biomol. Chem., 2020, Advance Article
DOI: 10.1039/D0OB00609B, Paper
Ana Maria S. Recchi, Pedro H. P. Rosa, Davi F. Back, Gilson Zeni
A synthetic approach to regioselective synthesis of 3-organochalcogenyl spiro[4,5]trienones and 3-organochalcogenyl[4,5]triene-2,6-diones is described through the reaction of arylpropiolamides with an electrophilic chalcogen source.
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synthesis

Diversity oriented multi-component reaction (DOS–MCR) approach to access natural product analogues: regio- and chemo-selective synthesis of polyheterocyclic scaffolds via one-pot cascade reactions

Org. Biomol. Chem., 2020, 18,3082-3092
DOI: 10.1039/D0OB00368A, Paper
Lakshmanan Palanivel, Vasuki Gnanasambandam
Skeletally diverse and complex polyheterocyclic hybrid scaffolds have been accessed via one-pot three-component reaction by exploiting the build/couple/pair strategy of diversity oriented synthesis.
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synthesis

Regio- and stereoselective synthesis of 1,4-enynes by iron-catalysed Suzuki–Miyaura coupling of propargyl electrophiles under ligand-free conditions

Org. Biomol. Chem., 2020, 18,3022-3026
DOI: 10.1039/D0OB00357C, Communication
Ryosuke Agata, Siming Lu, Hiroshi Matsuda, Katsuhiro Isozaki, Masaharu Nakamura
The first iron-catalysed cross coupling of propargyl electrophiles with lithium alkenylborates has been developed.
The content of this RSS Feed (c) The Royal Society of Chemistry




synthesis

Photochemical rearrangement of diarylethenes: synthesis of functionalized phenanthrenes

Org. Biomol. Chem., 2020, 18,3098-3103
DOI: 10.1039/D0OB00296H, Paper
A. V. Zakharov, A. V. Yadykov, A. G. Lvov, E. A. Mitina, V. Z. Shirinian
The photocyclization of diarylethenes bearing naphthalene units was explored and a convenient protocol for the synthesis of functionalized phenanthrenes was proposed.
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