Esters of 4,5-disubstituted-oxy-2-methyl-3,6-dioxo-cyclohexa-1,4-dienyl alkyl acids were prepared chemically and/or enzymatically. Depending upon the ester, improved melanocyte cytotoxicity was achieved. Improved cytotoxicity characteristics are consistent with ester analogs being more physiologically compatible and less irritating to skin than their corresponding acids.

A multi-legged apparatus enables a multi-legged robot to provide a natural motion, and includes a body portion comprising a body, a front leg portion comprising a front fixing portion fixed to the body, and a front rotating portion rotatably connected to the front fixing portion, a rear leg portion connected to the body and a rear leg portion comprising a rear rotating portion rotatably connected to the rear fixing portion, and a first link rotatably connected, at both ends, to the front and rear rotating portions, respectively. The body portion additionally includes a driving portion which rotates one of the front and rear rotating portions. By employing the first link and the driving portion, the body of the multi-legged robot is moved to and fro and left and right naturally in accordance with the movement of the legs, in a similar pattern as that generally shown in actual multi-legged animals.

A walking robot having joints which move using a torque servo, a posture of the robot being stably controlled, and a method of controlling a posture of the robot. It is possible to maintain a stable angle of the upper body while keeping an erect posture and balance using the COG of the robot and the inclination and the direction of the upper body and the pelvis of the robot, even in an external variation including external force or an inclination angle of the ground. Even in a state in which terrain information is not known in advance, the robot may keep an erect posture in a direction of gravity. Even when a plane where the robot stands is gradually inclined, the postures of the upper body and the legs of the robot may be kept while actively changing the angle of the ankle joint.

Methods and compositions for the deposition of a film on a substrate. In general, the disclosed compositions and methods utilize a precursor containing calcium or strontium.

The present invention relates to an (amide amino alkane) metal compound represented by the formula (1): wherein M represents a metal atom;R1 represents a linear, branched or cyclic alkyl group having 1 to 6 carbon atoms;R2 and R3 may be the same as, or different from each other, and each independently represents a linear or branched alkyl group having 1 to 3 carbon atoms, or R2 and R3 may form a substituted or unsubstituted 5- or 6-membered ring together with the nitrogen atom to which they are bound;Z represents a linear or branched alkylene group having 1 to 10 carbon atoms (a part of which may optionally form a ring); andn represents a number of the ligands, which is equal to the valence of the metal (M), and represents an integer of from 1 to 3; with the proviso that the metal compounds in which M is Li (Lithium), Be (Beryllium), Ge (Germanium) or Nd (Neodymium) are excluded;the metal compounds in which M is Mg (Magnesium) and R1 is methyl group are excluded;the metal compounds in which M is Zn (Zinc) and R1 is methyl group are excluded;the metal compounds in which M is Bi (Bismuth) and R1 is t-butyl group are excluded; andin cases where n is two or greater, two or more ligands may be the same as, or different from each other; and a method of producing a metal-containing thin film using the metal compound.

A cycloalkyl triamine pentacarboxylate compound coordinating to a metal ion to form a high stability metal complex in serum is provided. The metal complex of the present invention can be used as a contrast agent for magnetic resonance imaging (MRI).

Acylated insulins wherein an acyl moiety is attached to the parent insulin and wherein the acyl moiety comprises repeating units of alkylene glycol containing amino acids and wherein there is only one lysine residue (K & Lys) in the parent insulin, having satisfactory properties when administered pulmonary.

The present invention provides processes for the manufacturing of polypeptide conjugates. In particular, the invention provides methods for the purification of polypeptide conjugates, which include at least one polymeric modifying groups, such as a poly(alkylene oxide) moiety. Exemplary poly(alkylene oxide) moieties include poly(ethylene glycol) (PEG) and poly(propylene glycol). In an exemplary process, hydrophobic interaction chromatography (HIC) is used to resolve different glycoforms of glycoPEGylated polypeptides.

A machine which provides for both leaf stripping and grading can be used to process plants, such as burley tobacco plants, by continuously moving the plants in a first direction while simultaneously varying the position of the plants in a second direction relative to a defoliating apparatus. The plants may be moved horizontally through a machine by a transporter engaging the plant stalks while the vertical distance between the transporter (and thus the plants) is varied relative to the defoliating apparatus. The transporter and defoliating apparatus may be positioned at an angle to one another. Due to the changing amount of vertical distance, leaves from different sections of the plants, such as leaves at different stalk heights, can be contacted and removed at different corresponding horizontal locations in the machine. Accordingly, leaves can be graded based on the location(s) from which they are retrieved after removal.

An alkaline primary battery includes: a positive electrode 2 containing manganese dioxide; an alkaline electrolyte containing zinc oxide; a gelled negative electrode 3 containing zinc alloy particles, the alkaline electrolyte, and a gelling agent; and a negative electrode current collector 6 inserted in the gelled negative electrode. The gelled negative electrode 3 has a predetermined malleability such that when 4.0 g of the gelled negative electrode 3 formed into a cylindrical shape with a diameter of 15 mm is extended with 200 g of a load through 10 g of a flat plate, and then an upper surface of the extended gelled negative electrode 3 is approximated to a circle, this circle has a diameter ranging from 24 mm to 36 mm, both inclusive.

A system according to one embodiment includes at least two write transducers for writing to a magnetic medium; and a low reluctance path from a first pole of a first of the write transducers to a second pole of a second of the write transducers. In another embodiment, either 1) the first pole of the first write transducer and the second pole of the second write transducer are positioned close enough to each other that a low reluctance path is present from the first pole of the first write transducer to the second pole of the second write transducer, or 2) a magnetic strap extends between the first pole of the first write transducer and the second pole of the second write transducer thereby creating a low reluctance path therebetween.

Process for the preparation of vinyl aromatic (co) polymers grafted on an elastomer in a controlled manner, comprising: dissolving an elastomer functionalized with bromoalkanes and nitroxy radicals, soluble in non-polar solvents, in a liquid phase consisting of a mixture of vinyl aromatic monomer(s)/polymerization solvent; feeding at least one radical initiator to the mixture, containing the functionalized elastomer in solution, and polymerizing the mixture thus obtained at a temperature higher than or equal to 1200 C; recovering the vinyl aromatic (co) polymer obtained after devolatization; and recycling the solvent/monomer(s) mixture, coming from the devolatization, to step (a).

A telescopic chalk holder for drawing upon a drawing surface and including an outer cylinder having a tip at one end, a chalk stick received within the outer cylinder, the tip in radial receipt of the chalk stick, a push rod received by a second end of the outer cylinder and extending at least a portion of the chalk stick through the tip, and a push rod providing pressure to the chalk stick as the tip is manipulated over the drawing surface.

An improved polymerization and process method allows the production of special nitrile rubbers which are characterized by a specific anion content and an excellent storage stability and allow a particularly good vulcanization rate and moreover result in vulcanized materials that have advantageous properties, especially with regard to the contact with metal components of molded parts based on said vulcanized materials.

A combine harvester grain bulk tank and grain unloading system includes opposed bulk tank augers and an unloading auger formed in a grain bulk tank of a combine harvester. The bulk tank augers are for receiving and conveying grain through the bulk tank to the unloading auger, and the unloading auger is for receiving grain from the bulk tank augers and conveying grain to a grain unloading spout for grain unloading. A primary drive gear is coupled to the unloading auger and to an input, a secondary drive gear is drivingly coupled to the bulk tank augers, and a clutch is coupled between the primary drive gear and the secondary drive gear, which is movable between an engaged position for transferring power from the input to the unloading auger and to the bulk tank augers, and a disengaged position for isolating the bulk tank augers from the primary drive gear.

Volatile liquid precursors are provided for use in the formation of alkali metal-containing materials. The compound includes an alkali metal and an amide ligand and is a liquid at a temperature of less than about 70° C.

A process for preparing alkyllithium compounds by reacting a sodium-lithium alloy with alkyl halides at temperatures of about 50 to 125° C.

Disclosed is a method for producing Alkyllithium compounds by reacting metallic lithium with an Alkyl halide in a solvent. The reaction is performed at a reduced pressure at the boiling point of the solvent.

In the process of synthesizing alkylborazine compound represented by the chemical formula 2, by a reaction of a halogenated borazine compound represented by the chemical formula 1 with a Grignard reagent, thus synthesized alkylborazine compound is washed with water, or subjected to sublimation purification or distillation purification at least three times, and/or subjected to distillation purification at least twice. In the formulas, R1 independently represents alkyl group; R2 independently represents alkyl group; and X represents halogen atom.

A method for the production of alkyl lithium compounds is disclosed, in which metallic lithium is reacted with an alkyl halide in a solvent, whereby the metallic lithium is introduced in the form of lithium particles, generated by spraying molten lithium into an inert atmosphere or into a vacuum.

Pulverulent solid which consists essentially of at least one metal alkyl compound bound chemically and/or physically to a finely divided, porous, mechanically stable and chemically inert support, has a proportion by weight of metal alkyl compound of at least 5% by weight, based on the support, and has an angle of repose, determined in accordance with ISO 4324, of up to 48°. The solid allows trouble-free metering as active component into a reactor.

The present invention relates to a synthesis method of metal cyclopentadienide by direct reaction of dicyclopentadiene with a group 1 metal in the presence of an aprotic solvent. Unlike the conventional method depending on retro Diels-Alder reaction of dicyclopentadiene to generate indirectly cyclopentadiene, the method of the present invention favors generation of cyclopentadiene and metal cyclopentadienide as well by adding dicyclopentadiene directly when the reaction temperature reaches to the boiling point of a reaction solvent.

[Problem] To provide a preparation process by which an organic alkali metal compound is obtained in a high yield and a process for preparing an organic transition metal compound using the organic alkali metal compound. [Means to solve the problem] A process for preparing an organic alkali metal compound, which is characterized by adding a compound represented by the following formula (2) in the reaction of an active proton-containing compound represented by the following formula (1) with an alkali metal compound. RHp (1) In the formula (1), R is a hydrocarbon group or an amino group and may contain a halogen atom, a silicon atom, an oxygen atom or a nitrogen atom, H is an active proton, and p is the number of hydrogen atoms abstracted in the reaction with the alkali metal compound. In the formula (2), Ra to Rc are each an atom or a group selected from a hydrogen atom, a hydrocarbon group, a heteroatom-containing group and a silicon-containing group and may be the same as or different from each other, and the neighboring substituents may be bonded to each other to form a ring.

An apparatus and method are provided, for alternatively producing either small or bulk packs of napkins from a stack of folded napkins produced by one folding machine, through use of a pack dispatching arrangement having an inlet, a small pack transfer station and a bulk pack transfer station, and configured for operation in a small pack mode for dispatching a stream of spaced apart small packs of folded sheets separated from the stack of folded sheets, and received at an inlet of the pack dispatching arrangement, to the small pack transfer station, and alternatively operable in a bulk pack mode for dispatching a stream of spaced apart bulk packs of folded sheets separated from the stack of folded sheets, and received at an inlet of the pack dispatching arrangement, to the bulk pack transfer station.

A CO2 amine scrubbing process uses an absorbent mixture consisting of an alkanolamine CO2 sorbent in combination with a non-nucleophilic base. The alkanolamine has oxygen and nitrogen sites capable of nucleophilic attack at the CO2 carbon atom. The nucleophilic addition is promoted in the presence of the non-nucleophilic, relatively stronger base, acting as a proton acceptor. The non-nucleophilic base promoter, which may also act as a solvent for the alkanolamine, can promote reaction with the CO2 at each of the reactive hydroxyl and nucleophilic amine group(s) of the alkanolamines. In the case of primary amino alkanolamines the CO2 may be taken up by a double carboxylation reaction in which two moles of CO2 are taken up by the reacting primary amine groups.

The present invention provides an alkali metal salt of fluorosulfonyl imide having favorable heat resistance and a reduced content of specific impurities and a water content, and provides a method for producing an alkali metal salt of fluorosulfonyl imide, which is capable of easily removing a solvent from a reaction solution. An alkali metal salt of fluorosulfonyl imide of the present invention is represented by the following general formula (I) and has a mass loss rate of 2% or less when the alkali metal salt of fluorosulfonyl imide is kept at 100° C. for 8 hours under an air current. A method for producing an alkali metal salt of fluorosulfonyl imide of the present invention comprises a step of concentrating a solution of the alkali metal salt of fluorosulfonyl imide by bubbling a gas into a reaction solution containing the alkali metal salt of fluorosulfonyl imide, and/or concentrating a solution of the alkali metal salt of fluorosulfonyl imide by thin layer distillation.

A bulk material product bag has an adhesive closure strip fixedly secured thereon. As a result of the adhesive closure strip being oriented transversely across the normally open end region of the bulk material product bag so as to be adhesively bonded to both the back and front sides of the bulk material product bag, the adhesive closure strip effectively closes and seals the open end region of the bulk material product bag. Handle structure can also be integrally incorporated within the adhesive closure strip.

A robotic tubesheet walker having two rails connected by a central hinge, wherein the central hinge can be opened or closed by an actuation device. Upon each rail is mounted a carriage, wherein each carriage can move along its respective rail toward or away from the central hinge by means of a drive mechanism. Each carriage further contains at least two “gripper” attachment mechanisms, such as camlocks, to grip the tubesheet. The grippers either insert into tube holes within the tubesheet to fasten the respective carriage to the tubesheet, or retract to disengage. Further attached to the central hinge is a tool support fixture, and attached to the tool support fixture is a coupler that holds maintenance or inspection tools.

The invention relates to a method for producing alkaline amides or imides of ethylenically unsaturated C3 to C6 carboxylic acids by reacting amines that contain at least one primary and/or secondary amino group and at least one tertiary amino group with ethylenically unsaturated C3 to C6 carboxlic acids to form an ammonium salt and said ammonium salt is subsequently converted into the alkaline amide or imide by means of microwave radiation, with the proviso that the primary and/or secondary amino group is devoid of alkoxy groups.

An apparatus and method are provided for filling multi-chamber containers with different loose bulk materials. The apparatus and method may be particularly well-suited to packaging at least one bulk material, which is susceptible to water, chemicals, or other contaminants, with at least one other bulk material. The apparatus is a machine that includes separate hoppers for handling the separate bulk materials, and directs the separate bulk materials into different chambers of a multi-chamber container, which is then transported away from the machine for storage or use. The machine may include one or more movable hoppers supported on tracks, for moving the bulk materials to the hoppers that direct the bulk materials into different chambers of the multi-chamber container. A controller and data logger may be provided to control the apparatus and record the quantity and/or weight of the contents of each multi-chamber container.

A flexible and resilient tool for use with a conventional half barrel, parallel frame caulking gun or enclosed “sausage” style caulking gun, aiding the user in finishing and shaping after the caulking material has been applied. One function of the tool is to collect excess caulk from his finger(s) or from various shaping tools and spatulas. Also provided can be cap, rag and sponge holders. Additional embodiments include adaptations to existing prior art disposable caulking cartridges and caulking guns to include components of the disclosed tool.

A movable discharge device for use in a particle/bulk material storage silo includes: a travel body configured to travel along a groove provided at a lower portion of a storage silo; a scrape-out unit configured to move integrally with the travel body and including a blade configured to rotate above the groove to rake coals in the storage silo and scrape out the coals to the groove; and a groove closing mechanism configured to close a predetermined region of the groove within a rotation trajectory region of the blade. The discharge device is configured to be able to suppress the change in the discharge amount of coals discharged by the blade from the particle/bulk material storage silo.

A teat cup has a nozzle in a head portion of a flexible liner of the teat cup for delivering fluid internally of the teat cup. The nozzle is directed so as to discharge fluid towards the discharge end of the teat cup. When milking is terminated, treatment fluid is injected through the nozzle into the head portion of the liner just prior to and/or as the teat cup is being withdrawn from the teat and, the teat cup wipes the fluid down the teat so as substantially to coat the teat. When the teat cup falls into an inverted rest position, after take-off, the interior of the liner may be flushed and dried with disinfectant, water and compressed air discharged upwardly into the liner by the nozzle. The discharge end of the teat cup may be fitted with a shut-off valve which can be actuated to prevent ingress of treatment and cleansing fluids into the milk tubes during the treatment and cleansing cycle.

An apparatus for milking an animal and provides a milking parlor includes first and second robotic manipulation devices and a plurality of milking stalls provided on a platform moveable relative to the robotic manipulation devices. The robotic manipulation devices are positioned so that each of the robotic manipulation devices is able to simultaneously service two neighboring milking stalls on the platform.

The invention relates to a device for and method of milking dairy animals, in particular cows. The device and method have been improved in order to enhance the efficiency of use. In one embodiment, for the milking, teat cups are connected by means of a robot arm to respective teats of the dairy animal. This makes it possible to start the milking of the teats of the dairy animal. A milk flow from the respective teat can be measured. The milking can be ended by means of a control unit in dependence on a comparison value which is calculated on the basis of a milking parameter representative of a milk flow from the respective teat and in dependence on a deactivation threshold. According to the invention, the milking of the last teat is ended in dependence on a last-teat period to be calculated.

A mammalian quadruped walking system for providing visibility in dimly lit conditions features a body harness having a first side top shoulder strap, a second side top shoulder strap, a bottom strap, an upper body strap, a lower body strap, and a breast shield. The breast shield features a powerful bicycle's strength planar reflector that is only red or blue. The system features a harness extension having an extension first end located at an intersection of a first side top shoulder strap second end, a second side top shoulder strap second end and an upper body strap midpoint. A powerful bicycle's strength spherical red bead reflector is located adjacent to a spherical blue bead reflector close to a harness extension second end. The system features an external light source emitting light in a horizontal beam between 22 inches and 54 inches from a ground surface.

A device (1) for printing an impression by silk screen printing on at least one object (3), comprising of: a chassis (27); an object holder module (5) being movable relative to the chassis along a direction of pressing (Oz); a print head (7) including a screen holder module (29) and a squeegee holder module (31), the print head being movable relative to the chassis between an operating position close to the object holder module, and a maintenance position away from the object holder module, and an actuator (8) having a first part (125) and a second part (127) that is movable relative to the first part (125), the actuator (8) being adapted, in a first mode of operation, to be supported on the chassis by the first part and capable of moving the print head from the operating position to the maintenance position by a movement of the second part. The actuator is adapted, in a second mode of operation, to be supported on the chassis by the second part and is capable of moving the object holder module along the direction of pressing relative to the chassis by a movement of the first part.

Latent dispersants were made by the hydrogenation of an alkyl ketene dimer, alkenyl ketene dimer, or ketene multimer. Adding the latent dispersant to paper or paperboard increased its resistance to water and water vapor while maintaining recyclability and repulpability. Additionally, provided is a method for increasing the repulpability of a wax coated paper or paperboard. Dispersants made by the hydrolysis of the alkyl ketene dimer, alkenyl ketene dimer, and ketene multimer are also described.

Absorbent members, especially bulked absorbent members, and methods of making the same are disclosed. The absorbent member may be in the form of a unitary absorbent fibrous layer comprising at least some cellulose fibers. The unitary absorbent fibrous layer is at least partially stratified through its thickness. The absorbent member may also have a plurality of discrete deformations, such as depressions and/or apertures in its surfaces. The method involves subjecting a precursor web to at least one cycle (or pass) through a mechanical deformation process. The mechanical deformation process utilizes a first forming member and a second forming member that form a nip therebetween through which the precursor web is passed. The first and second forming members are moving at different speeds relative to each other when they come together to form the nip.

The present invention is directed to a mobile platform for the delivery of bulk explosives to a blast hole. One embodiment of the platform provides the ability to obtain weight information relating to the contents of a tank that is associated with the platform and that, in operation, contains either the bulk explosive or a constituent of the explosive. The platform comprises a vehicle with a frame, a tank, a load cell structure for connecting the frame and the tank and providing weight data relating to the contents of the tank, and a suspension system that prevents relative movement of the frame and the tank that could compromise the load cell structure. Another embodiment of the platform provides a tank for holding an explosive composition and a rotary shaft that supports a mixing blade that mixes the explosive composition within the tank. The platform further comprises bearing structure for supporting the rotary shaft that is located to deter any of the explosive composition from entering the bearing. A further embodiment of the platform comprises a conduit structure for discharging a bulk explosive into a blast hole that includes a substantially rigid tube with an outlet port for discharging a bulk explosive into the blast hole. The tube is adapted to rotate about a vertical axis such that the outlet port can be moved towards and away from the vehicle along an arc of less than 180°. In one embodiment, the outlet port can be positioned substantially adjacent to an operator's station to allow an operator to readily view the loading of the explosive into the blast hole.

A set of vertically stackable interacting cartridges for improving the delivery of biocide of a bulk feeder by positioning the stackable cartridges in a stacked condition within a chamber in the bulk feeder wherein the stackable cartridges are maintained in vertical interacting flow alignment with each other to provide enhanced control of the delivery of the biocide carried within each of the stackable cartridges without replacing the control valves of the bulk feeder.

Provided in one embodiment is a method of forming a connection mechanism in or on a bulk-solidifying amorphous alloy by casting in or on, or forming with the bulk-solidifying amorphous alloy, a machinable metal. The connection mechanism can be formed by machining the machinable metal.

Provided in one embodiment is a method of making use of foams as a processing aid or to improve the properties of bulk-solidifying amorphous alloy materials. Other embodiments include the bulk-solidifying amorphous alloy/foam composite materials made in accordance with the methods.

A coffee machine comprises a frothing device, wherein an internal milk channel leading to a frothing chamber is provided into which opens a bypass air inlet for operable air supply to the frothing device. A flexible milk suction line connects the frothing device with a milk supply container. Means are provided for cleaning the frothing device and the milk suction line with rinsing water from a continuous-flow water heater of the coffee machine. A controlled valve arrangement is provided which feeds rinsing water from the continuous-flow water heater to the bypass air inlet of the frothing device. A milk suction end of the milk suction line is directly or indirectly, fluid-conductively connectable with a residual water pan of the coffee machine prior to feeding rinsing water to the bypass air inlet.

The invention comprises using a fabric cut into several pieces which are further assembled together by stitches, the stitches being made using a sewing machine comprising at least two needles (A', B') operating in-line one behind the other so that the sewing stitch of the second needle (B') is made on the threads of the sewing stitch made by the first needle (A') in order to cover the perforation made by the first needle and so that the perforation made by the second needle (B') is made through said thread (11), thereby filling said perforation with said thread (11).

A method for fabricating a repair laminate for a composite part having an exposed surface includes applying a bonding material to the exposed surface and forming an uncured ply stack assembly on the bonding material. The uncured ply stack assembly is formed by forming and compacting a series of uncured ply stacks. The ply stack assembly and bonding material are then cured.

A freeze dryer processes bulk powder products. The freeze dryer freezes the product by mixing an atomized spray of product with sterile liquid nitrogen. The resultant powder is freeze dried in a vessel, and the vessel contents is agitated to maintain product contact with heated vessel wall and to prevent agglomeration.

A panel for tensioning fabric such as a silkscreen mesh is described. The panel includes locking strips secured to the edges using stitching through the mesh and locking strips. A method for fabricating the panel and tensioning the panel on a frame is also described. Locking strips may be stitched to edges of the fabric or mesh.

A system and method for changing a flow rate and direction of dry bulk material supplied from an elevated source, via an angled spout to an adjustable spout end having no internal baffles therein and having readily interchangeable wear pads therein which are accessible through an access door.

A system and method for causing a differential flow rate to exist in a downspout so as to reduce abrasion of a bottom side of said downspout and to sort dry bulk material flowing therethrough. The present invention reduces the velocity of the mass of the dry bulk material, such as corn, thus preserving grain quality and reducing the exit velocity at the lower end of the spout.