io System and method for efficient compilation and invocation of function type calls By www.freepatentsonline.com Published On :: Tue, 26 May 2015 08:00:00 EDT A system and method for efficient compilation and invocation of function type calls in a virtual machine (VM), or other runtime environment, and particularly for use in a system that includes a Java Virtual Machine (JVM). In accordance with an embodiment, the system comprises a virtual machine for executing a software application; a memory space for the application byte code comprising callsites generated using a function type carrier; a bytecode to machine code compiler which performs MethodHandle invocation optimizations; a memory space for the compiled machine code; and a memory space for storing software objects as part of the software application. The system enables carrying the function type from the original MethodHandle to a callsite in the generated bytecode, including maintaining generics information for a function type acquired from a target function, and generating a callsite based on the generics information for the function object invocation. Full Article
io Optimization of loops and data flow sections in multi-core processor environment By www.freepatentsonline.com Published On :: Tue, 26 May 2015 08:00:00 EDT The present invention relates to a method for compiling code for a multi-core processor, comprising: detecting and optimizing a loop, partitioning the loop into partitions executable and mappable on physical hardware with optimal instruction level parallelism, optimizing the loop iterations and/or loop counter for ideal mapping on hardware, chaining the loop partitions generating a list representing the execution sequence of the partitions. Full Article
io Software modification methods to provide master-slave execution for multi-processing and/or distributed parallel processing By www.freepatentsonline.com Published On :: Tue, 26 May 2015 08:00:00 EDT In one embodiment of the invention, a method is disclosed for modifying a pre-existing application program for multi-processing and/or distributed parallel processing. The method includes searching an application program for a computational loop; analyzing the computational loop to determine independence of the computational transactions of the computational loop; and replacing the computational loop with master code and slave code to provide master-slave execution of the computational loop in response to analyzing the computational loop to determine independence of the computational transactions of the computational loop. Multiple instances of the modified application program are executed to provide multi-processing and/or distributed parallel processing. Full Article
io Optimization hints for a business process flow By www.freepatentsonline.com Published On :: Tue, 26 May 2015 08:00:00 EDT In one embodiment, an optimization hint may be included in a business process flow. An executable process may be generated from the business process flow where the optimization hint is included in the executable process. While executing the executable process, the runtime engine encounters an optimization hint and determines an optimization to perform. The optimization hint may be related to an aspect of a business process being orchestrated by the business process flow. The optimization is then performed while executing the executable process. For example, the runtime engine may start pre-processing the branch while the condition is being evaluated. If the condition evaluates such that the pre-processed branch should be executed, then the runtime engine has already started processing of that branch. The processing is thus optimized in that the runtime engine is not sitting idle while waiting for the condition to be evaluated. Full Article
io Systems and methods for information flow analysis By www.freepatentsonline.com Published On :: Tue, 26 May 2015 08:00:00 EDT Computer-implemented methods for analyzing computer programs written in semi-structured languages are disclosed. The method is based on unification of the two classic forms of program flow analysis, control flow and data flow analysis. As such, it is capable of substantially increased precision, which increases the effectiveness of applications such as automated parallelization and software testing. Certain implementations of the method are based on a process of converting source code to a decision graph and transforming that into one or more alpha graphs which support various applications in software development. The method is designed for a wide variety of digital processing platforms, including highly parallel machines. The method may also be adapted to the analysis of (semi-structured) flows in other contexts including water systems and electrical grids. Full Article
io Method for identifying problematic loops in an application and devices thereof By www.freepatentsonline.com Published On :: Tue, 26 May 2015 08:00:00 EDT This invention relates to a method, computer readable medium, and apparatus for identifying one or more problematic loops in an application. This invention provides a Directed Acyclic Graph or DAG representation of structure of one or more loops in the application by performing a static and a dynamic analysis of the application source code and depicts the loop information as LoopID, loop weight, total loop iteration, average loop iteration, total loop iteration time, average loop iteration time and embedded vector size. This aids a programmer to concentrate on problematic loops in the application and analyze them further for potential parallelism. Full Article
io Electronic system with system modification control mechanism and method of operation thereof By www.freepatentsonline.com Published On :: Tue, 26 May 2015 08:00:00 EDT An electronic system and method of operation thereof includes: a control unit for receiving a patterned signal; a recognizer module, coupled to the control unit, for recognizing an unique trigger from the patterned signal; an operation module, coupled to the recognizer module, for detecting an operational mode from the unique trigger; and a change module, coupled to the operation module, for configuring a system state change of a memory sub-system based on the operational mode. Full Article
io Generic download and upload functionality in a client/server web application architecture By www.freepatentsonline.com Published On :: Tue, 26 May 2015 08:00:00 EDT The present invention relates generally to client-server architectures for allowing generic upload and download functionality between a web application at a server and a client. One exemplary method includes sending a download/upload request to a web application at the server, where the download/upload request specifies at least one file to download/upload; receiving a transmission from the server; parsing the transmission to identify a download/upload command and an associated download/upload manifest, where the download/upload manifest includes executable code that, when executed on the client, will perform the download/upload of the at least one file. Full Article
io Blueprint-driven environment template creation in a virtual infrastructure By www.freepatentsonline.com Published On :: Tue, 26 May 2015 08:00:00 EDT A system for blueprint-driven environment template creation in a virtual infrastructure comprises a processor and a memory. The processor is configured to receive a blueprint, receive an environment template configuration, and build an environment template using the blueprint and the environment template configuration. The environment template is for provisioning an environment. The environment is for deploying an application. The memory is coupled to the processor and is configured to provide the processor with instructions. Full Article
io Adjustment of threads for execution based on over-utilization of a domain in a multi-processor system by destroying parallizable group of threads in sub-domains By www.freepatentsonline.com Published On :: Tue, 26 May 2015 08:00:00 EDT Embodiments provide various techniques for dynamic adjustment of a number of threads for execution in any domain based on domain utilizations. In a multiprocessor system, the utilization for each domain is monitored. If a utilization of any of these domains changes, then the number of threads for each of the domains determined for execution may also be adjusted to adapt to the change. Full Article
io Methods and systems to identify and reproduce concurrency violations in multi-threaded programs using expressions By www.freepatentsonline.com Published On :: Tue, 15 Sep 2015 08:00:00 EDT Methods and systems to identify and reproduce concurrency bugs in multi-threaded programs are disclosed. An example method disclosed herein includes defining a data type. The data type includes a first predicate associated with a first thread of a multi-threaded program that is associated with a first condition, a second predicate that is associated with a second thread of the multi-threaded program, the second predicate being associated with a second condition, and an expression that defines a relationship between the first predicate and the second predicate. The relationship, when satisfied, causes the concurrency bug to be detected. A concurrency bug detector conforming to the data type is used to detect the concurrency bug in the multi-threaded program. Full Article
io Malodor counteracting compositions and method for their use By www.freepatentsonline.com Published On :: Tue, 08 Jul 2014 08:00:00 EDT The present invention relates to the field of perfumery and more particularly to the field of malodor counteractancy. In particular, it relates to a method for application of malodor counteracting (MOC) compositions capable of neutralizing in an efficient manner, through chemical reactions, malodors of a large variety of origins and which can be encountered in the air, on textiles, bathroom or kitchen surfaces, and the like. The composition may be applied as is or in the form of a perfuming composition or in a consumer product or article containing the compound or perfume composition. Full Article
io Fragrance compositions By www.freepatentsonline.com Published On :: Tue, 29 Jul 2014 08:00:00 EDT A rose-like fragrance composition including methyl epijasmonate, provided that a natural jasmine fragrance containing methyl epijasmonate is excluded. The rose-like fragrance composition can also include 2-isopropyl-4-methyl thiazole. Full Article
io Perfume compositions By www.freepatentsonline.com Published On :: Tue, 02 Sep 2014 08:00:00 EDT Perfume compositions effective against urine malodor and having a low odor, comprise between 20% and 50% of perfume ingredients comprising at least 15% by-weight of N-ethyl-N-(3-methylphenyl) propanamide. Full Article
io Perfuming compositions and uses thereof By www.freepatentsonline.com Published On :: Tue, 02 Sep 2014 08:00:00 EDT A perfuming composition capable of prolonging the release of a perfuming component into the surrounding environment when applied on a body surface. The composition includes isocetyl alcohol as a fragrance evaporation modulator in the presence of high amounts of ethanol. Also, consumer articles containing such compositions and methods for the perfuming of a body surface and for increasing the long-lastingness of a perfuming component using these compositions. Full Article
io Lipid composition having excellent shape retention property and product By www.freepatentsonline.com Published On :: Tue, 30 Sep 2014 08:00:00 EDT It is to provide a technique for preventing aggregation or caking of menthol at the time of its keeping. In addition, it is to provide a lipid composition, which can show excellent thermal stability even in the case of high temperature at the time of keeping menthol and at the time of blending in a product, does not cause mutual aggregation of powders, particles, flakes, pellets, sticks and the like of menthol, and can maintain its shape retention property. From 10 to 50% by mass of sterols are added to and mixed with from 50 to 90% by mass of menthol, and the resultant is melted with heating. Paraffins may be further added and mixed in an amount of 20% by mass or less, based on the lipid composition. Full Article
io 3-methyl-6-cyclohexadecen-1-one and its use in perfume compositions By www.freepatentsonline.com Published On :: Tue, 14 Oct 2014 08:00:00 EDT The present invention is directed to a novel fragrance compound, 3-methyl-cyclohexadec-6-enone. Full Article
io Compressed gas aerosol compositions By www.freepatentsonline.com Published On :: Tue, 21 Oct 2014 08:00:00 EDT Certain surfactants suitable for use alone to dissolve a water-insoluble component in compositions is described for providing VOC-free compressed gas aerosol compositions. The compositions include water-insoluble component(s), a surfactant and water. The water-insoluble component(s) can be active agent(s), such as fragrance(s) and/or an insecticide(s). The surfactant is present as a single surfactant which, in the absence of a solvent, dissolves or disperses the water-insoluble component(s) and provides a homogenous blend in water which provides a stable compressed gas emulsion. The surfactant is an anionic surfactant or a nonionic surfactant, in particular nonionic alkylpolyglycosides; nonionic cocoglucoside; nonionic alkylene oxide extended chain alkylpolyglycosides; anionic sodium lauryl ether sulfate (SLES), nonionic C13-C15 oxoalcohol ethoxylate with 8 ethylene oxides (EO), nonionic C12-C14 secondary alcohol ethoxylate with 7EO or 12EO, polyethylene glycol (PEG) hydrogenated castor oil wherein the PEG is PEG-60 or PEG-40, polyglyceryl-10 laurate and polyglyceryl-6 caprylate. Full Article
io Functional fragrance precursor By www.freepatentsonline.com Published On :: Tue, 25 Nov 2014 08:00:00 EST The present invention relates to a class of fragrance precursor compounds comprising one or more of the compounds derived from the reaction of X—OH and an aldehyde or ketone, the fragrance precursor compounds being of the formula X—O—C(R)(R*)(OR**) wherein R is a C6-24 alkyl group, a C6-24 aralkyl group or a C6-24 alkaryl group; R* is H or a C6-24 alkyl group, a C6-24 aralkyl group or a C6-24 alkaryl group; R** is H or X; X—O representing a moiety derived from X—OH, and wherein X—OH is a compound selected from the group consisting of surfactants, fabric softeners, softener precursor ester amines, softener precursor amido amines, hair conditioners, skin conditions, saccharides and polymers. In a second aspect it relates to a method of preparing such precusors. Further the invention relates to compositions, comprising the precursor of the invention. Full Article
io Functional fragrance precursor By www.freepatentsonline.com Published On :: Tue, 25 Nov 2014 08:00:00 EST The present invention relates to a class of fragrance precursor compounds comprising one or more of the compounds derived from the reaction of X—OH and an aldehyde or ketone, the fragrance precursor compounds being of the formula X—O—C(R)(R*)(OR**) wherein R is a C6-24 alkyl group, a C6-24 aralkyl group or a C6-24 alkaryl group; R* is H or a C6-24 alkyl group, a C6-24 aralkyl group or a C6-24 alkaryl group; R** is H or X; X—O representing a moiety derived from X—OH, and wherein X—OH is a compound selected from the group consisting of surfactants, fabric softeners, softener precursor ester amines, softener precursor amido amines, hair conditioners, skin conditions, saccharides and polymers. In a second aspect it relates to a method of preparing such precusors. Further the invention relates to compositions, comprising the precursor of the invention. Full Article
io Fragrance composition By www.freepatentsonline.com Published On :: Tue, 02 Dec 2014 08:00:00 EST A topical salve to mask unpleasant smells is disclosed that consists of a composition having beeswax, eucalyptus oil, and menthol. The composition is placed under the nose of a user. The salve masks unpleasant strong odors, thereby allowing the user to perform the task at hand. Full Article
io Functional fragrance precursor By www.freepatentsonline.com Published On :: Tue, 02 Dec 2014 08:00:00 EST The present invention relates to a class of fragrance precursor compounds comprising one or more of the compounds derived from the reaction of X—OH and an aldehyde or ketone, the fragrance precursor compounds being of the formula X—O—C(R)(R*)(OR**) wherein R is a C6-24 alkyl group, a C6-24 aralkyl group or a C6-24 alkaryl group; R* is H or a C6-24 alkyl group, a C6-24 aralkyl group or a C6-24 alkaryl group; R** is H or X; X—O representing a moiety derived from X—OH, and wherein X—OH is a compound selected from the group consisting of surfactants, fabric softeners, softener precursor ester amines, softener precursor amido amines, hair conditioners, skin conditions, saccharides and polymers. In a second aspect it relates to a method of preparing such precusors. Further the invention relates to compositions, comprising the precursor of the invention. Full Article
io Functional fragrance precursor By www.freepatentsonline.com Published On :: Tue, 09 Dec 2014 08:00:00 EST The present invention relates to a class of fragrance precursor compounds comprising one or more of the compounds derived from the reaction of X—OH and an aldehyde or ketone, the fragrance precursor compounds being of the formula X—O—C(R)(R*)(OR**) wherein R is a C6-24 alkyl group, a C6-24 aralkyl group or a C6-24 alkaryl group; R* is H or a C6-24 alkyl group, a C6-24 aralkyl group or a C6-24 alkaryl group; R** is H or X; X—O representing a moiety derived from X—OH, and wherein X—OH is a compound selected from the group consisting of surfactants, fabric softeners, softener precursor ester amines, softener precursor amido amines, hair conditioners, skin conditions, saccharides and polymers. In a second aspect it relates to a method of preparing such precursors. Further the invention relates to compositions, comprising the precursor of the invention. Full Article
io Extended release fragrance compositions By www.freepatentsonline.com Published On :: Tue, 30 Dec 2014 08:00:00 EST Compositions are provided that provide release of fragrance over an extended period of time. The compositions comprise a hydrophilically-modified cross-linked silicone elastomer and an acrylic rheology modifier. Full Article
io Benzodioxole derivatives as watery odorants By www.freepatentsonline.com Published On :: Tue, 24 Mar 2015 08:00:00 EDT The present invention relates to compounds of formula (I) in the form of any one of its stereoisomers or a mixture thereof, and wherein R1 represents a substituent of the benzene ring and is a bromine atom or a linear, branched or cyclic C1-8 alkyl, alkenyl, alkoxy or alkenyloxy group; R2 represents a C1-3 alkyl group; and R3 represents a hydrogen atom or a methyl or ethyl group; and their use as perfuming ingredients, for instance to impart odor notes of the watery/ozone type. Full Article
io Odorant composition containing allyl ethers as odorant precursors By www.freepatentsonline.com Published On :: Tue, 14 Apr 2015 08:00:00 EDT The deliberate release of odorants or aroma substances is desirable in many fields of application, and in particular in the field of washing and cleaning agents. Said deliberate release is achieved by using an odorant composition that comprises an odorant precursor, which is an allyl ether of the formula (I), R1R2C═CR3—CR4R5—O—CHR6R7, in which the residues R1, R2, R3, R4, R5, R6 and R7 mutually independently denote H or a hydrocarbon residue that can be acyclic or cyclic, substituted or unsubstituted, branched or unbranched, as well as saturated or unsaturated. Thus, in particular odorants in the form of an alkene having an allylic hydrogen atom, such as α-pinene, can be released in a deliberate manner. Full Article
io Pyrimidine derivatives and their use in perfume compositions By www.freepatentsonline.com Published On :: Tue, 12 May 2015 08:00:00 EDT The present invention relates to novel pyrimidine derivatives and their use in perfume compositions. The novel pyrimidine derivatives of the present invention are represented by the following formula: wherein m and n are integers of 0 or 1, with the proviso that when m is 0, n is 1 and when m is 1, n is 0; andwherein the dashed circle represents either single or double bonds. Full Article
io Separation of isomeric menthol compounds By www.freepatentsonline.com Published On :: Tue, 05 May 2015 08:00:00 EDT The invention relates to a process for rectificative separation of compositions of matter containing diastereomers of 2-isopropyl-5-methylcyclohexanol by using ionic liquids as extractants. Full Article
io Process for isolating crystallized 2,2,4,4 tetramethyl-1,3-cyclobutanediol (TMCD) particles utilizing pressure filtration By www.freepatentsonline.com Published On :: Tue, 05 May 2015 08:00:00 EDT A method for isolating 2,2,4,4-tetramethyl-1,3-cyclobutanediol (TMCD) solids from an isolated feed slurry formed in a TMCD process comprising TMCD, a liquid phase, and impurities by (a) treating the isolated feed slurry in a product isolation zone to produce an isolated TMCD product wet cake, a mother liquor, and impurities; wherein the product isolation zone can comprise at least one rotary pressure drum filter. Full Article
io Purification of crude glycerol By www.freepatentsonline.com Published On :: Tue, 05 May 2015 08:00:00 EDT Crude glycerol obtained from raw materials, such as the glycerol obtained during the production of biodiesel or glycerol obtained during the conversion of fats or oils, is purified by forming a dioxolane therefrom by reacting the crude glycerol with a ketone or aldehyde, separating the dioxolane thus formed, converting the dioxolane into purified glycerol and ketone/aldehyde, and recovering the glycerol thus purified. Full Article
io Process for the production of ethanol from an acetic acid feed and a recycled ethyl acetate feed By www.freepatentsonline.com Published On :: Tue, 05 May 2015 08:00:00 EDT The present invention produces ethanol in a reactor that comprises a catalyst composition and a feed stream comprising acetic acid and a recycled liquid stream comprising ethyl acetate. The catalyst composition comprises a first catalyst comprising platinum, cobalt, and/or tin and a second catalyst comprising copper. The crude ethanol product may be separated and ethanol recovered. Full Article
io Reduced energy alcohol separation process having controlled pressure By www.freepatentsonline.com Published On :: Tue, 05 May 2015 08:00:00 EDT The present invention is directed to processes for the recovery of ethanol from a crude ethanol product obtained from the hydrogenation of acetic acid using a low energy process. The crude ethanol product is separated in one or more columns. At least one of the columns is operated at a controlled pressure to enhance separation of ethanol and organics. In one embodiment, there are at least two columns that operate at controlled pressures. Full Article
io Process to reduce ethanol recycled to hydrogenation reactor By www.freepatentsonline.com Published On :: Tue, 05 May 2015 08:00:00 EDT The present invention is directed to processes for recovering ethanol obtained from the hydrogenation of acetic acid. Acetic acid is hydrogenated in the presence of a catalyst in a hydrogenation reactor to form a crude ethanol product. The crude ethanol product is separated in one or more columns to recover ethanol. In some embodiments, less than 10 wt. % ethanol is recycled to the hydrogenation reactor. Full Article
io Hydrogenation catalysts with acidic sites By www.freepatentsonline.com Published On :: Tue, 05 May 2015 08:00:00 EDT The present invention relates to catalysts and to chemical processes employing such catalysts. The catalysts are preferably used for converting acetic acid to ethanol. The catalyst comprises acidic sites and two or more metals. The catalyst has acidic sites on the surface and the balance favors Lewis acid sites. Full Article
io Hydrogenation catalysts comprising a mixed oxide comprising nickel By www.freepatentsonline.com Published On :: Tue, 05 May 2015 08:00:00 EDT A process is disclosed for producing ethanol comprising contacting acetic acid and hydrogen in a reactor in the presence of a catalyst comprising a binder and a mixed oxide comprising nickel and tin. Full Article
io Esterification process using extractive separation to produce feed for hydrogenolysis By www.freepatentsonline.com Published On :: Tue, 05 May 2015 08:00:00 EDT Disclosed herein are processes for alcohol production by reducing an esterification product, such as ethyl acetate. The processes comprise esterifying acetic acid and an alcohol such as ethanol to produce an esterification product. The esterification product may be recovered using an extractive separation. The esterification product is reduced with hydrogen in the presence of a catalyst to obtain a crude reaction mixture comprising the alcohol, in particular ethanol, which may be separated from the crude reaction mixture. Full Article
io Method for producing 2-chloromethylbenzaldehyde, 2-chloromethylbenzaldehyde-containing composition, and method for storing same By www.freepatentsonline.com Published On :: Tue, 12 May 2015 08:00:00 EDT A process for obtaining an industrially useful 2-chloromethylbenzaldehyde-containing liquid composition at a high yield is provided. More specifically, a process for producing 2-chloromethylbenzaldehyde comprising step (A) of mixing 1-dichloromethyl-2-chloromethylbenzene and sulfuric acid having a concentration of 84.5% by weight or more; and step (B) of mixing a mixture obtained in step (A) and water is provided. Full Article
io Protected aldehydes for use as intermediates in chemical syntheses, and processes for their preparation By www.freepatentsonline.com Published On :: Tue, 12 May 2015 08:00:00 EDT A para-methoxy protected benzaldehyde useful in preparation of treprostinil, and of formula: (Formula (1)) is prepared by subjecting to Claisen re-arrangement a substituted benzaldehyde of formula (1a): (Formula (Ia)) to form the m-hydroxy-substituted benzaldehyde of formula (1b): (Formula (Ib)) and then reacting compound (1b) with a p-methoxybenzyl (PMB) compound to form a PMB-substituted benzaldehyde of formula (1). Full Article
io Apparatus for coproducting ISO type reaction products and alcohols from olefins, and method for coproducting them using the apparatus By www.freepatentsonline.com Published On :: Tue, 12 May 2015 08:00:00 EDT The present invention relates to an apparatus for coproducting iso-type reaction product and alcohol from olefin, and a method for coproducting using the apparatus, in which the hydroformylation reactor provides a sufficient reaction area due to the broad contact surface area between the olefin and the synthesis gases that are the raw materials by a distributor plate installed in the reactor, and the raw materials can be sufficiently mixed with the reaction mixture due to the circulation of the reaction mixture so that the efficiency of the production of the aldehyde is excellent; and also the hydrogenation reactor suppresses the side reaction so that the efficiency for producing aldehyde and alcohol are all increased, and also iso-type reaction product and alcohol can be efficiently co-produced. Full Article
io Phenol purification process By www.freepatentsonline.com Published On :: Tue, 12 May 2015 08:00:00 EDT The present invention provides an easy process for purifying phenol by separating carbonyl compounds through selective hydrogenation of the compounds to the corresponding alcohols then distillation. The phenol purification process of the present invention comprises bringing phenol into contact with a copper-based catalyst in the presence of hydrogen to convert carbonyl compounds contained in the phenol to the corresponding alcohol compounds, and separating the alcohol compounds and phenol by distillation. Full Article
io Method for cultivation of Monarda fistulosa By www.freepatentsonline.com Published On :: Tue, 12 May 2015 08:00:00 EDT A method for cultivating Monarda fistulosaincludes planting seeds at rates between about 2.5 and about 5 pounds per acre, preferably about 4 pounds per acre. Fuel costs are reduced because seeding, mowing the first season, and harvesting in seasons thereafter are all that is required. Reduction in herbicide use results from the heavy rate of planting, improved germination attributed to rolling, and the plant's natural herbicides which are more highly effective when seeded at the higher rate. The method includes seeding, mowing during a first growing season, and harvesting each season thereafter. This method results in oil without weed contamination and carvacrol levels are high. Full Article
io Dehydrogenation of cyclohexanone to produce phenol By www.freepatentsonline.com Published On :: Tue, 12 May 2015 08:00:00 EDT In a process for the dehydrogenation of cyclohexanone to produce phenol, a feed comprising cyclohexanone is contacted with a dehydrogenation catalyst under dehydrogenation conditions comprising a temperature of less than 400° C. and a pressure of less than 690 kPa, gauge, such 0.1 to 50 wt % of the cyclohexanone in said feed is converted to phenol and the dehydrogenation product contains less than 100 ppm by weight of alkylbenzenes. Full Article
io Energy efficient method and apparatus for the extraction of lower alcohols from dilute aqueous solution By www.freepatentsonline.com Published On :: Tue, 12 May 2015 08:00:00 EDT The present invention relates to the energy efficient and selective extraction of dilute concentrations of C2-C6 alcohols from an aqueous solution using liquid phase dimethyl ether. Full Article
io Method for producing phenylphosphonic acid metal salt composition, and crystal nucleating agent therefrom By www.freepatentsonline.com Published On :: Tue, 19 May 2015 08:00:00 EDT A method for producing a phenylphosphonic acid metal salt composition, including reacting a phenylphosphonic acid compound (a) with a metal salt, metal oxide or metal hydroxide (b) that is present in an amount beyond the equivalent, the phenylphosphonic acid metal salt composition containing phenylphosphonic acid metal salt, and a surplus amount of the metal salt, the metal oxide or the surplus metal hydroxide (b). A crystal nucleating agent comprises the phenylphosphonic acid metal salt composition produced by the method. Full Article
io Hydrolysis of the residues obtained in the production of isophorone to recover isophorone and acetone By www.freepatentsonline.com Published On :: Tue, 19 May 2015 08:00:00 EDT A process for preparing isophorone (3,5,5-trimethyl-2-cyclohexen-1-one) is provided wherein distillation vapors from the work-up of product fractions are recycled to earlier stages of operation of the process. Full Article
io Optical resolution methods for bicyclic compounds using asymmetric catalysts By www.freepatentsonline.com Published On :: Tue, 19 May 2015 08:00:00 EDT An optically active bicyclic compound is efficiently produced by optical resolution using an optically active amine. Full Article
io Process for the in situ production of polyether polyols based on renewable materials and their use in the production of flexible polyurethane foams By www.freepatentsonline.com Published On :: Tue, 19 May 2015 08:00:00 EDT A polyether polyol based on renewable materials is obtained by the in situ production of a polyether from a hydroxyl group-containing vegetable oil, at least one alkylene oxide and a low molecular weight polyol having at least 2 hydroxyl groups. The polyol is produced by introducing the hydroxyl group-containing vegetable oil, a catalyst and an alkylene oxide to a reactor and initiating the alkoxylation reaction. After the alkoxylation reaction has begun but before the reaction has been 20% completed, the low molecular weight polyol having at least 2 hydroxyl groups is continuously introduced into the reactor. After the in situ made polyether polyol product having the desired molecular weight has been formed, the in situ made polyether polyol is removed from the reactor. These polyether polyols are particularly suitable for the production of flexible polyurethane foams. Full Article
io Method for the hydroxylation of phenols and phenol ethers By www.freepatentsonline.com Published On :: Tue, 19 May 2015 08:00:00 EDT The present invention relates to a method for the hydroxylation of phenols and phenol ethers by means of hydrogen peroxide. The invention specifically relates to a method for the hydroxylation of phenol by means of the hydrogen peroxide. The method of the invention for the hydroxylation of a phenol or phenol ether by means of reacting said phenol or phenol ether with the hydrogen peroxide in the presence of an acid catalyst is characterized in that it includes mixing a phenol or phenol ether with a hydrogen peroxide solution in a mixing device under conditions enabling the conversion rate of the hydrogen peroxide to be minimized, and in that said reaction mixture is then placed in a piston flow reactor where the reaction leading to the production of the hydroxylated material takes place, the acid catalyst being fed into the mixing device and/or into the piston flow reactor. Full Article
io Dehydrogenation process By www.freepatentsonline.com Published On :: Tue, 19 May 2015 08:00:00 EDT In a process for the dehydrogenation of dehydrogenatable hydrocarbons, a feed comprising dehydrogenatable hydrocarbons is contacted with a catalyst comprising a support and a dehydrogenation component under dehydrogenation conditions effective to convert at least a portion of the dehydrogenatable hydrocarbons in the feed. The catalyst is produced by a method comprising treating the support with a liquid composition comprising the dehydrogenation component or a precursor thereof and at least one organic dispersant selected from an amino alcohol and an amino acid. Full Article
io Process for production of hexamethylenediamine from carbohydrate-containing materials and intermediates therefor By www.freepatentsonline.com Published On :: Tue, 19 May 2015 08:00:00 EDT Processes are disclosed for the conversion of a carbohydrate source to hexamethylenediamine (HMDA) and to intermediates useful for the production of hexamethylenediamine and other industrial chemicals. HMDA is produced by direct reduction of a furfural substrate to 1,6-hexanediol in the presence of hydrogen and a heterogeneous reduction catalyst comprising Pt or by indirect reduction of a furfural substrate to 1,6-hexanediol wherein 1,2,6-hexanetriol is produced by reduction of the furfural substrate in the presence of hydrogen and a catalyst comprising Pt and 1,2,6-hexanediol is then converted by hydrogenation in the presence of a catalyst comprising Pt to 1,6 hexanediol, each process then proceeding to the production of HMDA by known routes, such as amination of the 1,6 hexanediol. Catalysts useful for the direct and indirect production of 1,6-hexanediol are also disclosed. Full Article