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Rhodium(III)-catalyzed synthesis of 3-trifluoromethylindanones from N-Methoxybenzamides via C-H activation and Claisen/Retro-Claisen reaction

By pubs.rsc.org
Published On ::

Org. Chem. Front., 2020, Accepted Manuscript
DOI: 10.1039/D0QO00330A, Research Article
Satyasheel Sharma, Bharatkumar Chaudhary, Neeraj Kulkarni
The Rhodium(III)-catalyzed reaction of N-methoxybenzamides as a directing group with β-trifluoromethyl-α,β-unsaturated ketones is reported. The reaction involved sp2 C−H activation, followed by Claisen condensation involving C-N bond cleavage to form...
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[ASAP] Contrasting Efficiency of Electron-Induced Reaction at Cu(110) in Aliphatic and Aromatic Bromides

By feedproxy.google.com
Published On :: Tue, 05 May 2020 04:00:00 GMT

Journal of the American Chemical Society
DOI: 10.1021/jacs.0c02851


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[ASAP] Speciation of Cu Surfaces During the Electrochemical CO Reduction Reaction

By feedproxy.google.com
Published On :: Wed, 06 May 2020 04:00:00 GMT

Journal of the American Chemical Society
DOI: 10.1021/jacs.0c02354


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[ASAP] Rapid Route-Finding for Bifurcating Organic Reactions

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Published On :: Thu, 07 May 2020 04:00:00 GMT

Journal of the American Chemical Society
DOI: 10.1021/jacs.9b13449


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Maillard reaction in foods: mitigation strategies and positive properties / Salvatore Parisi, Sara M. Ameem, Shana Montalto and Anna Santangelo

By library.mit.edu
Published On :: Sun, 14 Jul 2019 06:40:38 EDT

Online Resource


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Palladium supported on triazolyl-functionalized hypercrosslinked polymers as a recyclable catalyst for Suzuki–Miyaura coupling reactions

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RSC Adv., 2020, 10,17123-17128
DOI: 10.1039/D0RA01190H, Paper
Open Access
Cijie Liu, Lijuan Zheng, Dexuan Xiang, Shasha Liu, Wei Xu, Qionglin Luo, You Shu, Yuejun Ouyang, Hongwei Lin
A novel hypercrosslinked polymer-palladium catalyst was prepared via external cross-linking reactions and applied in Suzuki–Miyaura reactions as a recyclable catalyst, resulting in TON numbers up to 1.66 × 104 and yields reaching 99%.
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Simple organocatalyst component system for asymmetric hetero Diels–Alder reaction of isatins with enones

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RSC Adv., 2020, 10,17486-17491
DOI: 10.1039/D0RA03006F, Paper
Open Access
Perumalsamy Parasuraman, Zubeda Begum, Madhu Chennapuram, Chigusa Seki, Yuko Okuyama, Eunsang Kwon, Koji Uwai, Michio Tokiwa, Suguru Tokiwa, Mitsuhiro Takeshita, Hiroto Nakano
A simple two catalysts component system of β-amino alcohols (catalyst) and amino acids (co-catalyst) works as an efficient organocatalysts in hetero Diels–Alder reaction of isatins with enones to afford chiral spirooxindole-tetrahydropyranones.
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Alkaline water-splitting reactions over Pd/Co-MOF-derived carbon obtained via microwave-assisted synthesis

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Published On ::

RSC Adv., 2020, 10,17359-17368
DOI: 10.1039/D0RA02307H, Paper
Open Access
  This article is licensed under a Creative Commons Attribution 3.0 Unported Licence.
Adewale K. Ipadeola, Kenneth I. Ozoemena
Palladium nanoparticles supported on MOF-derived carbon serve as an efficient bifunctional electrocatalyst for alkaline water-splitting reactions.
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Borohydride catalyzed redistribution reaction of hydrosilane and chlorosilane: a potential system for facile preparation of hydrochlorosilanes

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Published On ::

RSC Adv., 2020, 10,17404-17407
DOI: 10.1039/D0RA03536J, Paper
Open Access
Yi Chen, Liqing Ai, Yongming Li, Caihong Xu
A borohydride catalyzed Si–H/Si–Cl redistribution system was established to prepare hydrochlorosilanes facilely and efficiently.
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Position-locking of volatile reaction products by atmosphere and capping layers slows down photodecomposition of methylammonium lead triiodide perovskite

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RSC Adv., 2020, 10,17534-17542
DOI: 10.1039/D0RA03572F, Paper
Open Access
  This article is licensed under a Creative Commons Attribution 3.0 Unported Licence.
Fengshuo Zu, Thorsten Schultz, Christian M. Wolff, Dongguen Shin, Lennart Frohloff, Dieter Neher, Patrick Amsalem, Norbert Koch
Gas pressure and capping layers under ultrahigh vacuum prevent methylammonium lead triiodide photo-degradation due to efficient back-reaction of volatile compounds.
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Computational study on the polymerization reaction of D-aminopeptidase for the synthesis of D-peptides

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RSC Adv., 2020, 10,17582-17592
DOI: 10.1039/D0RA01138J, Paper
Open Access
  This article is licensed under a Creative Commons Attribution 3.0 Unported Licence.
Joan Gimenez-Dejoz, Kousuke Tsuchiya, Ayaka Tateishi, Yoko Motoda, Takanori Kigawa, Yasuhisa Asano, Keiji Numata
We studied the molecular mechanism of D-aminopeptidase for the synthesis of polypeptides incorporating D-amino acids.
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Dependence on co-adsorbed water in the reforming reaction of ethanol on a Rh(111) surface

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RSC Adv., 2020, 10,17787-17794
DOI: 10.1039/D0RA02015J, Paper
Open Access
Yu-Yao Hsia, Po-Cheng Chien, Lu-Hsin Lee, Yu-Ling Lai, Li-Chung Yu, Yao-Jane Hsu, Jeng-Han Wang, Meng-Fan Luo
Adsorbed ethanol molecules penetrated readily through pre-adsorbed water to react at the Rh surface; they decomposed at a promoted probability.
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Photo-reduction enables catalyst regeneration in Fenton reaction on an Fe2O3-decorated TiO2 nanotube-based photocatalyst

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Published On ::

Dalton Trans., 2020, Advance Article
DOI: 10.1039/D0DT00670J, Paper
Quanming Peng, Guiming Peng, Liangpeng Wu, Yaqian Chen, Bin Han, Qiucheng Su, Shijun Liu, Xinjun Li
Active Fe2+ sites of TNT(Pd)/Fe2O3 with a unique electronic structure for the Fenton reaction can be self-generated.
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1,2-Insertion Reactions of Alkynes into Ge–C Bonds of Arylbromogermylene

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Published On ::

Dalton Trans., 2020, Accepted Manuscript
DOI: 10.1039/D0DT01223H, Paper
Tomohiro Sugahara, Arturo Espinosa Ferao, Alicia Rey, Jing-Dong Guo, Shin Aoyama, Kazunobu Igawa, Katsuhiko Tomooka, Takahiro Sasamori, Daisuke Hashizume, Shigeru Nagase, Norihiro Tokitoh
1,2-insertion reactions of alkynes into the Ge–C bonds in dibromodigermenes afford stable crystalline bromovinylgermylenes. In contrast to previously reported Lewis-base-supported vinylgermylenes, the bromovinylgermylene obtained from reaction of the bromogermylene with...
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Selenotungstates incorporating organophosphonate ligands and metal ions: synthesis, characterization, magnetism and catalytic efficiency in Knoevenagel condensation reaction

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Published On ::

Dalton Trans., 2020, Accepted Manuscript
DOI: 10.1039/D0DT00444H, Paper
Jingyang Niu, Hui Kong, Peipei He, Zongfei Yang, Qiaofei Xu, Jiawei Wang, Ran Ban, Pengtao Ma, Jingping Wang
Three sandwich-type TM-containing (TM = transition metal) organophosphonate-based polyoxotungstate clusters, [TM(H2O)4(SeW6O21)2{Co(OOCCH2NCH2PO3)2}3]12– (TM = Co, Ni), have been successfully synthesized, which is the first reported TMs-containing organophosphonate-based selenotungstates. They were structurally...
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Simulations unveil Grignard reactions' complex mechanism

By feedproxy.google.com
Published On :: 19 Feb 2020 22:00:00 +0000

Detailed models highlight a key role for solvents


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New mapping method reveals reactions galore

By feedproxy.google.com
Published On :: 01 Apr 2020 15:01:33 +0000

System combines compounds in unfamiliar ways


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Nudging reaction in reverse repurposes polyurethane foam

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Published On :: 29 Apr 2020 13:44:12 +0000

New polymer processing method offers a path to recycle a huge class of consumer goods


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[ASAP] Hydrothermal Liquefaction of Polycarbonate (PC) Plastics in Sub-/Supercritical Water and Reaction Pathway Exploration

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Published On :: Tue, 28 Apr 2020 04:00:00 GMT

ACS Sustainable Chemistry & Engineering
DOI: 10.1021/acssuschemeng.0c00700


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[ASAP] Design and Synthesis of Highly Performing Bifunctional Ni-NiO-MoNi Hybrid Catalysts for Enhanced Urea Oxidation and Hydrogen Evolution Reactions

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Published On :: Thu, 30 Apr 2020 04:00:00 GMT

ACS Sustainable Chemistry & Engineering
DOI: 10.1021/acssuschemeng.0c01637


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[ASAP] Two-Dimensional Metal Hexahydroxybenzene Frameworks as Promising Electrocatalysts for an Oxygen Reduction Reaction

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Published On :: Tue, 05 May 2020 04:00:00 GMT

ACS Sustainable Chemistry & Engineering
DOI: 10.1021/acssuschemeng.0c01908


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Computational fluid dynamics (CFD) and reaction modelling study of bio-oil catalytic hydrodeoxygenation in microreactors

By pubs.rsc.org
Published On ::

React. Chem. Eng., 2020, Advance Article
DOI: 10.1039/D0RE00102C, Paper
Sanaa Hafeez, Elsa Aristodemou, George Manos, S. M. Al-Salem, Achilleas Constantinou
A computational fluid dynamics (CFD) model was derived and validated in order to investigate the hydrodeoxygenation reaction of 4-propylguaiacol, which is a lignin-derived compound present in bio-oil.
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Elementary reaction pathway study and a deduced macrokinetic model for the unified understanding of Ni-catalyzed steam methane reforming

By pubs.rsc.org
Published On ::

React. Chem. Eng., 2020, 5,873-885
DOI: 10.1039/C9RE00460B, Paper
Changming Ke, Zijing Lin
DFT based microkinetics and macrokinetics that give quantitative explanations of the Ni-catalyzed steam methane reforming reactions.
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New insights into catalysis for Heck reactions with fine supported Pd particles

By pubs.rsc.org
Published On ::

React. Chem. Eng., 2020, 5,921-934
DOI: 10.1039/C9RE00480G, Paper
Lin Huang, Zhan Wang, Jozel Tan
The catalytic activity over supported Pd particles is dependent on the concentration of soluble active Pd species. The correlation that the smaller the size of supported Pd particles, the higher the catalytic activity is confirmed.
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Automated generation of photochemical reaction data by transient flow experiments coupled with online HPLC analysis

By pubs.rsc.org
Published On ::

React. Chem. Eng., 2020, 5,912-920
DOI: 10.1039/D0RE00066C, Paper
Christian P. Haas, Simon Biesenroth, Stephan Buckenmaier, Tom van de Goor, Ulrich Tallarek
Competing homo- and crossdimerization reactions between coumarin and 1-methyl-2-quinolinone are investigated by transient continuous-flow experiments combined with online HPLC, enabling the generation and acquisition of large reaction data sets.
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Synthesis of 3-trifluoromethylated 1,3-butadienes via a Pd(0)-catalyzed fluorinated Heck reaction

By pubs.rsc.org
Published On ::

React. Chem. Eng., 2020, 5,961-966
DOI: 10.1039/D0RE00093K, Paper
Yang Li, Meng Hao, Ming Xia, Ning Sun, Cai-Lin Zhang, Wen-Qing Zhu
1,3-Butadienes play a key role in modern synthetic chemistry and biochemistry because they are well-known precursors for the synthesis of retinoids.
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Multitask prediction of site selectivity in aromatic C–H functionalization reactions

By pubs.rsc.org
Published On ::

React. Chem. Eng., 2020, 5,896-902
DOI: 10.1039/D0RE00071J, Paper
Open Access
Thomas J. Struble, Connor W. Coley, Klavs F. Jensen
Aromatic C–H functionalization reactions are an important part of the synthetic chemistry toolbox.
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Sustainable chemo-enzymatic preparation of enantiopure (R)-β-hydroxy-1,2,3-triazoles via lactic acid bacteria-mediated bioreduction of aromatic ketones and a heterogeneous “click” cycloaddition reaction in deep eutectic solvents

By pubs.rsc.org
Published On ::

React. Chem. Eng., 2020, 5,859-864
DOI: 10.1039/D0RE00067A, Communication
Paola Vitale, Francesco Lavolpe, Francesca Valerio, Mariaelena Di Biase, Filippo Maria Perna, Eugenia Messina, Gennaro Agrimi, Isabella Pisano, Vito Capriati
A chemo-enzymatic strategy for the preparation of enantiopure (R)-β-hydroxy-1,2,3-triazoles using a lactic acid bacterium as a whole-cell biocatalyst and a heterogeneous “click” cycloaddition reaction in deep eutectic solvents is disclosed.
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Outstanding Reviewers for Reaction Chemistry & Engineering in 2019

By pubs.rsc.org
Published On ::

React. Chem. Eng., 2020, 5,813-813
DOI: 10.1039/D0RE90016H, Editorial

We would like to take this opportunity to highlight the Outstanding Reviewers for Reaction Chemistry & Engineering in 2019, as selected by the editorial team for their significant contribution to the journal.
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An automated flow chemistry platform to decouple mixing and reaction times

By pubs.rsc.org
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React. Chem. Eng., 2020, Advance Article
DOI: 10.1039/D0RE00129E, Communication
Robert W. Epps, Amanda A. Volk, Kameel Abdel-Latif, Milad Abolhasani
We present a flow chemistry platform that decouples precursor mixing rates from reaction time using solely off-the-shelf components. We then utilize this platform towards material-efficient studies of mass transfer-controlled synthesis of inorganic perovskite quantum dots.
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Correction: Efficacy of proprietary Lactobacillus casei for anti-tuberculosis associated gastrointestinal adverse reactions in adult patients: a randomized, open-label, dose–response trial

By feeds.rsc.org
Published On ::

Food Funct., 2020, 11,3751-3751
DOI: 10.1039/D0FO90017F, Correction
Open Access
  This article is licensed under a Creative Commons Attribution 3.0 Unported Licence.
Song Lin, Shanliang Zhao, Jiahong Liu, Jianwen Zhang, Chao Zhang, Haibo Hao, Yuxia Sun, Jing Cai, Yang Yang, Yan Ma, Yuanyuan Li, Jinyu Wang, Aiguo Ma
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Enzyme reaction-guided identification of active components from the flowers of Sophora japonica var. violacea

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Food Funct., 2020, Advance Article
DOI: 10.1039/D0FO00625D, Paper
Yunci Zhang, Dongyu Gu, Shuai He, Jing Meng, Jifeng Wang, Yunxiao Wang, Yi Wang, Jing Tian, Yi Yang
The flower of S. japonica is a favorite food and used as traditional medicine.
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[ASAP] Total Synthesis of Isohericenone J via a Stille Coupling Reaction

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Published On :: Thu, 30 Apr 2020 04:00:00 GMT

Journal of Natural Products
DOI: 10.1021/acs.jnatprod.9b01251


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[ASAP] Upscaling Photoredox Cross-Coupling Reactions in Batch Using Immersion-Well Reactors

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Published On :: Thu, 30 Apr 2020 04:00:00 GMT

Organic Process Research & Development
DOI: 10.1021/acs.oprd.0c00070


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Enhancing the methane low-temperature conversion on the Zn/ZSM-5 in the presence of methanol by regulating methanol-to-aromatics reaction pathway

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Published On ::

Catal. Sci. Technol., 2020, Accepted Manuscript
DOI: 10.1039/D0CY00449A, Paper
Zhixiang Xi, Bingjie Zhou, Yue Yu, Binbo Jiang, Zhengliang Huang, Zuwei Liao, Jingdai Wang, Yao Yang, Jingyuan Sun, Yongrong Yang
Co-reaction method provides efficient strategy for methane conversion in mild condition, which is of urgent importance of direct valorization of natural gas to liquid hydrocarbons. However, vague mechanism and neglect...
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Synergistic photocatalysis–Fenton reaction for selective conversion of methane to methanol at room temperature

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Catal. Sci. Technol., 2020, 10,2329-2332
DOI: 10.1039/D0CY00028K, Communication
Yi Zeng, Hang Chen Liu, Jing Sheng Wang, Xing Yang Wu, Song Ling Wang
Combining the photocatalysis and Fenton reaction highly promote the yield and selectivity of CH3OH from CH4 with solar light at room temperature, up to 471 μmol g−1 h−1 and 83%, respectively.
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New findings and current controversies in the reaction of ruthenium red and ammonium cerium(IV) nitrate: focus on the precipitated compound

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Catal. Sci. Technol., 2020, 10,2491-2502
DOI: 10.1039/C9CY02499A, Paper
Bahram Sarvi, Seyedeh Maedeh Hosseini, Bahareh Deljoo, Abdelhamid El-Sawy, Alireza Shirazi Amin, Mark Aindow, Steven L. Suib, Mohammad Mahdi Najafpour
During water-oxidation reaction in the presence of RuR and CAN, a heterogeneous nano-sized Ru-Ce compound is detected, which is formed by the interaction of [(NH3)5RuORu(NH3)4ORu(NH3)5],6+/7+ nitrate ions, and the products of the reduction of CAN.
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Kinetic study of the methane dry (CO2) reforming reaction over the Ce0.70La0.20Ni0.10O2−δ catalyst

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Catal. Sci. Technol., 2020, 10,2652-2662
DOI: 10.1039/C9CY02192B, Paper
Lidia Pino, Cristina Italiano, Massimo Laganà, Antonio Vita, Vincenzo Recupero
The kinetic behaviour of the Ce0.70La0.20Ni0.10O2−δ catalyst during the methane dry reforming reaction was investigated in a fixed bed reactor in the temperature range of 923–1023 K with the partial pressure of CH4 and CO2 ranging between 5 and 50 kPa.
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Integrated adsorption and photocatalytic degradation of VOCs using a TiO2/diatomite composite: effects of relative humidity and reaction atmosphere

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Catal. Sci. Technol., 2020, 10,2378-2388
DOI: 10.1039/D0CY00168F, Paper
Guangxin Zhang, Arman Peyravi, Zaher Hashisho, Zhiming Sun, Yangyu Liu, Shuilin Zheng, Lexuan Zhong
The optimal relative humidity condition for VOC degradation is related to the length of the carbon chain of VOCs.
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Enhancing hydrogen evolution reaction through modulating electronic structure of self-supported NiFe LDH

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Catal. Sci. Technol., 2020, Advance Article
DOI: 10.1039/D0CY00315H, Paper
Xiao-Peng Li, Wen-Kai Han, Kang Xiao, Ting Ouyang, Nan Li, Feng Peng, Zhao-Qing Liu
NiFe-layered double hydroxide (NiFe LDH), as an efficient oxygen evolution reaction (OER) electrocatalyst, has emerged as a promising electrocatalyst for catalyzing overall water splitting in alkaline electrolyte.
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Development of BiOI as an effective photocatalyst for oxygen evolution reaction under simulated solar irradiation

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Catal. Sci. Technol., 2020, Advance Article
DOI: 10.1039/D0CY00266F, Paper
Tzu-Hsin Chen, Masaaki Yoshida, Shun Tsunekawa, Jia-Hao Wu, Kun-Yi Andrew Lin, Chechia Hu
In this study, crystalline BiOI powders were prepared for photocatalytic O2 evolution in the presence of NaIO3 as the electron mediator.
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Facet-Dependent Activity of Hematite Nanocrystals toward Oxygen Evolution Reaction

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Catal. Sci. Technol., 2020, Accepted Manuscript
DOI: 10.1039/D0CY00655F, Paper
Toshihiro Takashima, Shota Hemmi, Qingyu Liu, Hiroshi Irie
Electrocatalytic activity of hematite exposed with different facets toward the oxygen evolution reaction (OER) was investigated. Hematite nanoparticles with pseudo cubic, hexagonal bipyramid, and plate morphologies were prepared, which predominantly...
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Hybrid Phase 1T/2H-MoS2 with Controllable 1T Concentration and Its Promoted Hydrogen Evolution Reaction

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Published On ::

Nanoscale, 2020, Accepted Manuscript
DOI: 10.1039/D0NR02525A, Paper
Yuxiao Zhang, Yasutaka Kuwahara, Kohsuke Mori, Catherine Louis, Hiromi Yamashita
MoS2 has been investigated as a low-cost alternative to Pt in electrochemical hydrogen evolution reaction. One of the promising method to further activate MoS2 is phase engineering. MoS2 generally exhibit...
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Enhanced type I photoreaction of indocyanine green via electrostatic-force-driven aggregation

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Published On ::

Nanoscale, 2020, 12,9517-9523
DOI: 10.1039/D0NR01208D, Paper
Huizhen Fan, Yu Fan, Wenna Du, Rui Cai, Xinshuang Gao, Xinfeng Liu, Hao Wang, Lei Wang, Xiaochun Wu
ICG forms aggregates in positively charged mesoporous silica, which show an enhanced type I photoreaction pathway.
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2D molybdenum disulphide nanosheets incorporated with single heteroatoms for the electrochemical hydrogen evolution reaction

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Nanoscale, 2020, Advance Article
DOI: 10.1039/D0NR01295E, Minireview
Thomas H. M. Lau, John S. Foord, S. C. Edman Tsang
2D nanosheets give enhanced surface area to volume ratios in particle morphology and they can also provide defined surface sites to disperse foreign atoms.
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Single-wavelength phototheranostics for colon cancer via thiolytic reaction

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Nanoscale, 2020, Accepted Manuscript
DOI: 10.1039/D0NR02393K, Paper
Yucheng Zhu, Chao Chen, Qinghua Wu, Guoliang Yang, Zhiyong Liu, Erhong Hao, Hongliang Cao, Yun Gao, Weian Zhang
It’s a huge challenge to develop effective nanosystems combined the capabilities of diagnoses and therapies together for colon cancer in clinic. Herein, we constructed a far-red absorbing phototheranostic nanosystem (FR-H2S)...
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MnV2O6/Graphene Nanocomposite as an Efficient Electrocatalyst for the Oxygen Evolution Reaction

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Published On ::

Nanoscale, 2020, Accepted Manuscript
DOI: 10.1039/D0NR02325F, Communication
Kyeong-Ho Kim, Yun-Hyuk Choi, Seong-Hyeon Hong
MnV2O6/graphene nanocomposite was fabricated through hydrothermal synthesis and high energy mechanical milling as an electrocatalyst for oxygen evolution reaction (OER). MnV2O6/graphene (20 wt%) nanocomposite deposited on carbon fiber paper (CFP)...
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Reactions to natural and man-made radioactive threat

By digital.lib.usf.edu
Published On :: Sun, 26 Jan 2014 14:09:46 -0400


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Inhibitory effects of food matrices on inhibition real-time reverse transcription polymerase chain reaction detection of foodborne viruses

By digital.lib.usf.edu
Published On :: Sat, 15 Feb 2014 18:07:42 -0400


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A comparison of centrifugal forces to reduce the inhibitory effects of food matrixes on reverse transciptase polymerase chain reaction for the detection of food borne viruses

By digital.lib.usf.edu
Published On :: Sat, 15 Feb 2014 18:11:44 -0400


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