rre Michigan man arrested for alleged threats to kill 'conservative Christian filth' over Trump election win By www.christianpost.com Published On :: Thu, 07 Nov 2024 10:00:29 -0500 A 25-year-old Michigan man is facing federal charges after he allegedly threatened violence against conservative Christians over former President Donald Trump winning the presidential election. Full Article
rre Pastor John-Paul Miller arrested months after suicide of wife Mica Miller By www.christianpost.com Published On :: Thu, 07 Nov 2024 12:55:30 -0500 Pastor John-Paul Miller is expected to appear in a Myrtle Beach court Thursday for a bond hearing after he was arrested and charged a day earlier with third-degree assault months after the suicide of his wife, Mica Miller. Full Article
rre Church reels after murdered missionary’s wife arrested in connection with his death By www.christianpost.com Published On :: Mon, 04 Nov 2024 17:21:51 -0500 Members of the Lakes Area Vineyard Church in Detroit Lakes, Minnesota, where the late Beau Shroyer and his family were longtime members before moving to Lubango, Angola, to serve as missionaries in 2021, are now reeling in a complex web of emotions after learning that Beau’s wife, Jackie Shroyer, was arrested in connection with his murder in the southern African country just over a week ago. Full Article
rre Deputy Defence Minister Timur Ivanon arrested on charges of large bribery By english.pravda.ru Published On :: Wed, 24 Apr 2024 14:02:00 +0300 Timur Ivanov, Russian Deputy Defence Minister, was arrested on April 23 in the case of bribery. He will remain in custody before June 2024. A Moscow court sent Deputy Defence Minister Timur Ivanov to a pre-trial detention centre. He was arrested for two months, until June 23. Ivanov was charged under Part 6 of Art. 290 of the Criminal Code (receiving a bribe on an especially large scale). According to investigators, Ivanov entered into a "criminal conspiracy with third parties to commit a crime and received a large bribe in the form of property services provided during contracting and subcontracting works for the needs of the Defence Ministry.” Full Article Russia
rre Putin proposes new Defence Minister amid notorious arrest of Shoigu's deputy By english.pravda.ru Published On :: Mon, 13 May 2024 14:04:00 +0300 Andrei Belousov, who held the position of First Deputy Head of the Cabinet of Ministers, will now become Russia's new Defence Minister. The Federation Council will discuss his candidacy on May 13 and 14. Kremlin spokesman Dmitry Peskov said that it was important to integrate the economy of the power bloc into the country's economy so that it meets the dynamics of the current moment. "The one who is more open to innovation wins on the battlefield," Peskov said. "The Ministry of Defence must be absolutely open to innovation, to all advanced ideas the purpose of economic competitiveness. Apparently, this is why the president picked the candidacy of Andrei Removich Belousov," he noted. Full Article Russia
rre Suspected serial arsonist arrested in Snyder By www.tdi.texas.gov Published On :: Tue, 23 Apr 2024 00:00:00 CDT Snyder law enforcement officials last week arrested Daniel Allen Jr. Full Article
rre Yars nuclear deterrent missile designed to cool Western hot heads By english.pravda.ru Published On :: Tue, 01 Oct 2024 20:14:00 +0300 Not that long ago, the Teikovo missile unit (Guards Order of Kutuzov missile division) took mobile ground-based Yars missile systems for exercises. The manoeuvres included marches at a distance of up to 100 kilometers, dispersal and change of positions, organization of combat security and camouflage. The goal of the exercises was to improve the training and coherence of personnel of the Strategic Missile Forces. Full Article World
rre Moscow Patriot Park director and high-ranking defense official arrested for fraud By english.pravda.ru Published On :: Mon, 05 Aug 2024 16:29:00 +0300 Vyacheslav Akhmedov, director of Moscow's Patriot Park, was arrested as part of the investigation into fraudulent activities. Deputy head of the Main Directorate for Innovative Development of the Russian Ministry of Defense, Major General Vladimir Shesterov, was detained as well, the Investigative Committee of Russia said on its Telegram channel. The arrested individuals, together with their accomplices, are responsible for the theft of funds allocated for the operation of the Patriot Park. Army-2024 international military and technical forum was supposed to be held in the Patriot Park in August 2024. Now the event has been put into question. Full Article Russia
rre Why do people use cryptocurrency despite all the fraud and complexity? By english.pravda.ru Published On :: Tue, 08 Sep 2020 11:33:00 +0300 With the continuous and rapid evolution of the technological era, digital currencies are gaining popularity daily. They have been gaining traction from the past half-decade. Despite the fluctuations in bitcoin and other cryptocurrencies' value, more and more people start seeing cryptocurrency as a profitable investment. For instance, if we talk about Bitcoin, one of the most popular types of cryptocurrency, it has taken over the digital currency market. If we further discuss its fame, you'll see that it is being used in some of the biggest business names around the globe, including Microsoft, Overstock, and AT&T, now accept it as a method of payment. Here, you might be thinking, why do people use cryptocurrency and cryptocurrency wallets? What are their pros and cons? Is it worth investing in cryptocurrency wallets in 2020? If you have such questions, get them answered here. But first, let us tell you about the MOST USEFUL cryptocurrency wallets. A lot of wallets are designed solely for the storage of cryptocurrencies. At a time when there was a peak in online currency exchanges and thefts, there was a need to create a wallet that will provide ultimate protection. OWNR Wallet is one of the safest bitcoin wallets to buy crypto in 2020. It helps people in keeping their digital money safe from external threats. Along with security, OWNR Wallet offers a variety of useful features for both holders and traders. Full Article Business
rre Court orders arrest of Volkswagen's Russian assets By english.pravda.ru Published On :: Mon, 20 Mar 2023 12:42:00 +0300 The Arbitration Court of the Nizhny Novgorod region arrested all assets of German automaker Volkswagen in Russia, Interfax reports. Since March 17, Volkswagen has been banned from conducting any registration actions, such as actions to liquidate, reorganise or change the composition of participants, increase and decrease the authorized capital of the Russian subsidiary of Volkswagen and its legal entities. Volkswagen's assets in Russia ere banned following a court appeal from Russia's GAZ automobile group from March 14. The document was published in the file of arbitration cases. Full Article Business
rre The Importance of Buying The Correct Barcode Scanner By www.retailtechnologyreview.com Published On :: By Bryan Luna, freelance writer.Read on to learn the different types and features present in various barcode scanners to make the right decision for your business and employee needs. Full Article Data Capture Mobile Computers RFID
rre September 2006 Post of the Month: Irreducible Complexity as an Evolutionary Prediction By www.talkorigins.org Published On :: Added October 19, 2006: Full Article
rre Police Seek Arrest Warrants for 6 Anti-Yoon Protesters By world.kbs.co.kr Published On :: Mon, 11 Nov 2024 18:51:53 +0900 [Domestic] : Police have requested arrest warrants for six members of the Korean Confederation of Trade Unions(KCTU) who took part in a large protest in downtown Seoul on Saturday urging President Yoon Suk Yeol to step down. The police said Monday that they detained eleven people on Saturday and asked the Central ...[more...] Full Article Domestic
rre Labor, Civic Groups Hold Major Rallies in Seoul, 11 Arrested By world.kbs.co.kr Published On :: Sun, 10 Nov 2024 12:43:14 +0900 [Politics] : Labor and civic groups held massive anti-government rallies in Seoul on Saturday afternoon. The Korean Confederation of Trade Unions (KCTU), one of the nation's two umbrella groups, staged a rally along with civic groups starting at 4 p.m. near Deoksu Palace and some of the protesters clashed with ...[more...] Full Article Politics
rre JCS Warns N. Korea Will Face Corresponding Steps if It Infiltrates Drones By world.kbs.co.kr Published On :: Mon, 28 Oct 2024 17:41:20 +0900 [Inter-Korea] : The Joint Chiefs of Staff(JCS) has warned that North Korea will face corresponding countermeasures if it infiltrates drones into South Korean territory. JCS spokesperson Lee Sung-joon unveiled such a stance to reporters on Monday when asked to comment on Kim Yo-jong, the sister of North Korean leader Kim ...[more...] Full Article Inter-Korea
rre What Is the Strongest Currency in the World? By money.howstuffworks.com Published On :: Fri, 27 Sep 2024 10:20:02 -0400 If you found a bag full of cash, which currency would you prefer it to be? The quick answer might not be the best one; while a suitcase full of U.S. dollars would mean you could start spending immediately (provided you were in the U.S., or in a country that accepted the U.S. dollar as an official currency), there are actually more valuable currencies out there. Full Article
rre S. Korea Posts Current Account Surplus in September for Fifth Straight Month By world.kbs.co.kr Published On :: Thu, 07 Nov 2024 08:29:44 +0900 [Economy] : The nation posted a current account surplus for the fifth consecutive month in September, on the back of robust exports of semiconductors and other IT products. According to tentative data from the Bank of Korea on Thursday, the current account surplus came to eleven-point-12 billion dollars in ...[more...] Full Article Economy
rre Assessment of the exchange-hole dipole moment dispersion correction for the energy ranking stage of the seventh crystal structure prediction blind test By journals.iucr.org Published On :: 2024-10-15 The seventh blind test of crystal structure prediction (CSP) methods substantially increased the level of complexity of the target compounds relative to the previous tests organized by the Cambridge Crystallographic Data Centre. In this work, the performance of density-functional methods is assessed using numerical atomic orbitals and the exchange-hole dipole moment dispersion correction (XDM) for the energy-ranking phase of the seventh blind test. Overall, excellent performance was seen for the two rigid molecules (XXVII, XXVIII) and for the organic salt (XXXIII). However, for the agrochemical (XXXI) and pharmaceutical (XXXII) targets, the experimental polymorphs were ranked fairly high in energy amongst the provided candidate structures and inclusion of thermal free-energy corrections from the lattice vibrations was found to be essential for compound XXXI. Based on these results, it is proposed that the importance of vibrational free-energy corrections increases with the number of rotatable bonds. Full Article text
rre AnACor2.0: a GPU-accelerated open-source software package for analytical absorption corrections in X-ray crystallography By journals.iucr.org Published On :: AnACor2.0 significantly accelerates the calculation of analytical absorption corrections in long-wavelength crystallography, achieving up to 175× speed improvements. This enhancement is achieved through innovative sampling techniques, bisection and gridding methods, and optimized CUDA implementations, ensuring efficient and accurate results. Full Article text
rre Effect of thickness and noise on angular correlation analysis from scanning electron nanobeam diffraction of disordered carbon By journals.iucr.org Published On :: The impact of sample thickness and experimental noise on angular correlation analysis from scanning electron nanobeam diffraction patterns of disordered carbon are investigated and analyzed regarding the interpretability of the analysis results. Full Article text
rre AnACor2.0: a GPU-accelerated open-source software package for analytical absorption corrections in X-ray crystallography By journals.iucr.org Published On :: 2024-11-04 Analytical absorption corrections are employed in scaling diffraction data for highly absorbing samples, such as those used in long-wavelength crystallography, where empirical corrections pose a challenge. AnACor2.0 is an accelerated software package developed to calculate analytical absorption corrections. It accomplishes this by ray-tracing the paths of diffracted X-rays through a voxelized 3D model of the sample. Due to the computationally intensive nature of ray-tracing, the calculation of analytical absorption corrections for a given sample can be time consuming. Three experimental datasets (insulin at λ = 3.10 Å, thermolysin at λ = 3.53 Å and thaumatin at λ = 4.13 Å) were processed to investigate the effectiveness of the accelerated methods in AnACor2.0. These methods demonstrated a maximum reduction in execution time of up to 175× compared with previous methods. As a result, the absorption factor calculation for the insulin dataset can now be completed in less than 10 s. These acceleration methods combine sampling, which evaluates subsets of crystal voxels, with modifications to standard ray-tracing. The bisection method is used to find path lengths, reducing the complexity from O(n) to O(log2 n). The gridding method involves calculating a regular grid of diffraction paths and using interpolation to find an absorption correction for a specific reflection. Additionally, optimized and specifically designed CUDA implementations for NVIDIA GPUs are utilized to enhance performance. Evaluation of these methods using simulated and real datasets demonstrates that systematic sampling of the 3D model provides consistently accurate results with minimal variance across different sampling ratios. The mean difference of absorption factors from the full calculation (without sampling) is at most 2%. Additionally, the anomalous peak heights of sulfur atoms in the Fourier map show a mean difference of only 1% compared with the full calculation. This research refines and accelerates the process of analytical absorption corrections, introducing innovative sampling and computational techniques that significantly enhance efficiency while maintaining accurate results. Full Article text
rre Correlation of refractive index based and THz streaking arrival time tools for a hard X-ray free-electron laser By journals.iucr.org Published On :: 2024-01-22 To fully exploit ultra-short X-ray pulse durations routinely available at X-ray free-electron lasers to follow out-of-equilibrium dynamics, inherent arrival time fluctuations of the X-ray pulse with an external perturbing laser pulse need to be measured. In this work, two methods of arrival time measurement were compared to measure the arrival time jitter of hard X-ray pulses. The methods were photoelectron streaking by a THz field and a transient refractive index change of a semiconductor. The methods were validated by shot-to-shot correction of a pump–probe transient reflectivity measurement. An ultimate shot-to-shot full width at half-maximum error between the devices of 19.2 ± 0.1 fs was measured. Full Article text
rre Novel correction procedure for compensating thermal contraction errors in the measurement of the magnetic field of superconducting undulator coils in a liquid helium cryostat By journals.iucr.org Published On :: 2024-02-22 Superconducting undulators (SCUs) can offer a much higher on-axis undulator field than state-of-the-art cryogenic permanent-magnet undulators with the same period and vacuum gap. The development of shorter-period and high-field SCUs would allow the free-electron laser and synchrotron radiation source community to reduce both the length of undulators and the dimensions of the accelerator. Magnetic measurements are essential for characterizing the magnetic field quality of undulators for operation in a modern light source. Hall probe scanning is so far the most mature technique for local field characterization of undulators. This article focuses on the systematic error caused by thermal contraction that influences Hall probe measurements carried out in a liquid helium cryostat. A novel procedure, based on the redundant measurement of the magnetic field using multiple Hall probes at known relative distance, is introduced for the correction of such systematic error. Full Article text
rre High-pressure X-ray photon correlation spectroscopy at fourth-generation synchrotron sources By journals.iucr.org Published On :: 2024-04-10 A new experimental setup combining X-ray photon correlation spectroscopy (XPCS) in the hard X-ray regime and a high-pressure sample environment has been developed to monitor the pressure dependence of the internal motion of complex systems down to the atomic scale in the multi-gigapascal range, from room temperature to 600 K. The high flux of coherent high-energy X-rays at fourth-generation synchrotron sources solves the problems caused by the absorption of diamond anvil cells used to generate high pressure, enabling the measurement of the intermediate scattering function over six orders of magnitude in time, from 10−3 s to 103 s. The constraints posed by the high-pressure generation such as the preservation of X-ray coherence, as well as the sample, pressure and temperature stability, are discussed, and the feasibility of high-pressure XPCS is demonstrated through results obtained on metallic glasses. Full Article text
rre Iterative Bragg peak removal on X-ray absorption spectra with automatic intensity correction By journals.iucr.org Published On :: 2024-04-09 This study introduces a novel iterative Bragg peak removal with automatic intensity correction (IBR-AIC) methodology for X-ray absorption spectroscopy (XAS), specifically addressing the challenge of Bragg peak interference in the analysis of crystalline materials. The approach integrates experimental adjustments and sophisticated post-processing, including an iterative algorithm for robust calculation of the scaling factor of the absorption coefficients and efficient elimination of the Bragg peaks, a common obstacle in accurately interpreting XAS data, particularly in crystalline samples. The method was thoroughly evaluated on dilute catalysts and thin films, with fluorescence mode and large-angle rotation. The results underscore the technique's effectiveness, adaptability and substantial potential in improving the precision of XAS data analysis. While demonstrating significant promise, the method does have limitations related to signal-to-noise ratio sensitivity and the necessity for meticulous angle selection during experimentation. Overall, IBR-AIC represents a significant advancement in XAS, offering a pragmatic solution to Bragg peak contamination challenges, thereby expanding the applications of XAS in understanding complex materials under diverse experimental conditions. Full Article text
rre A new experimental setup for combined fast differential scanning calorimetry and X-ray photon correlation spectroscopy By journals.iucr.org Published On :: 2024-04-24 Synchrotron-radiation-based techniques are a powerful tool for the investigation of materials. In particular, the availability of highly brilliant sources has opened the possibility to develop techniques sensitive to dynamics at the atomic scale such as X-ray photon correlation spectroscopy (XPCS). XPCS is particularly relevant in the study of glasses, which have been often investigated at the macroscopic scale by, for example, differential scanning calorimetry. Here, we show how to adapt a Flash calorimeter to combine XPCS and calorimetric scans. This setup paves the way to novel experiments requiring dynamical and thermodynamic information, ranging from the study of the crystallization kinetics to the study of the glass transition in systems that can be vitrified thanks to the high cooling rates reachable with an ultrafast calorimeter. Full Article text
rre Wavefront analysis and phase correctors design using SHADOW By journals.iucr.org Published On :: 2024-04-23 Knife-edge imaging is a successful method for determining the wavefront distortion of focusing optics such as Kirkpatrick–Baez mirrors or compound refractive lenses. In this study, the wavefront error of an imperfect elliptical mirror is predicted by developing a knife-edge program using the SHADOW/OASYS platform. It is shown that the focusing optics can be aligned perfectly by minimizing the parabolic and cubic coefficients of the wavefront error. The residual wavefront error provides precise information about the figure/height errors of the focusing optics suggesting it as an accurate method for in situ optical metrology. A Python program is developed to design a customized wavefront refractive corrector to minimize the residual wavefront error. Uniform beam at and out of focus and higher peak intensity are achieved by the wavefront correction in comparison with ideal focusing. The developed code provides a quick way for wavefront error analysis and corrector design for non-ideal optics especially for the new-generation diffraction-limited sources, and saves considerable experimental time and effort. Full Article text
rre Mapping of lithium ion concentrations in 3D structures through development of in situ correlative imaging of X-ray Compton scattering-computed tomography By journals.iucr.org Published On :: 2024-06-05 Understanding the correlation between chemical and microstructural properties is critical for unraveling the fundamental relationship between materials chemistry and physical structures that can benefit materials science and engineering. Here, we demonstrate novel in situ correlative imaging of the X-ray Compton scattering computed tomography (XCS-CT) technique for studying this fundamental relationship. XCS-CT can image light elements that do not usually exhibit strong signals using other X-ray characterization techniques. This paper describes the XCS-CT setup and data analysis method for calculating the valence electron momentum density and lithium-ion concentration, and provides two examples of spatially and temporally resolved chemical properties inside batteries in 3D. XCS-CT was applied to study two types of rechargeable lithium batteries in standard coin cell casings: (1) a lithium-ion battery containing a cathode of bespoke microstructure and liquid electrolyte, and (2) a solid-state battery containing a solid-polymer electrolyte. The XCS-CT technique is beneficial to a wide variety of materials and systems to map chemical composition changes in 3D structures. Full Article text
rre Correcting angular distortions in Bragg coherent X-ray diffraction imaging By journals.iucr.org Published On :: 2024-08-08 Bragg coherent X-ray diffraction imaging (BCDI) has emerged as a powerful technique for strain imaging and morphology reconstruction of nanometre-scale crystals. However, BCDI often suffers from angular distortions that appear during data acquisition, caused by radiation pressure, heating or imperfect scanning stages. This limits the applicability of BCDI, in particular for small crystals and high-flux X-ray beams. Here, we present a pre-processing algorithm that recovers the 3D datasets from the BCDI dataset measured under the impact of large angular distortions. We systematically investigate the performance of this method for different levels of distortion and find that the algorithm recovers the correct angles for distortions up to 16.4× (1640%) the angular step size dθ = 0.004°. We also show that the angles in a continuous scan can be recovered with high accuracy. As expected, the correction provides marked improvements in the subsequent phase retrieval. Full Article text
rre Structure determination using high-order spatial correlations in single-particle X-ray scattering By journals.iucr.org Published On :: 2024-01-01 Single-particle imaging using X-ray free-electron lasers (XFELs) is a promising technique for observing nanoscale biological samples under near-physiological conditions. However, as the sample's orientation in each diffraction pattern is unknown, advanced algorithms are required to reconstruct the 3D diffraction intensity volume and subsequently the sample's density model. While most approaches perform 3D reconstruction via determining the orientation of each diffraction pattern, a correlation-based approach utilizes the averaged spatial correlations of diffraction intensities over all patterns, making it well suited for processing experimental data with a poor signal-to-noise ratio of individual patterns. Here, a method is proposed to determine the 3D structure of a sample by analyzing the double, triple and quadruple spatial correlations in diffraction patterns. This ab initio method can reconstruct the basic shape of an irregular unsymmetric 3D sample without requiring any prior knowledge of the sample. The impact of background and noise on correlations is investigated and corrected to ensure the success of reconstruction under simulated experimental conditions. Additionally, the feasibility of using the correlation-based approach to process incomplete partial diffraction patterns is demonstrated. The proposed method is a variable addition to existing algorithms for 3D reconstruction and will further promote the development and adoption of XFEL single-particle imaging techniques. Full Article text
rre Orientational analysis of atomic pair correlations in nanocrystalline indium oxide thin films By journals.iucr.org Published On :: 2024-01-01 The application of grazing-incidence total X-ray scattering (GITXS) for pair distribution function (PDF) analysis using >50 keV X-rays from synchrotron light sources has created new opportunities for structural characterization of supported thin films with high resolution. Compared with grazing-incidence wide-angle X-ray scattering, which is only useful for highly ordered materials, GITXS/PDFs expand such analysis to largely disordered or nanostructured materials by examining the atomic pair correlations dependent on the direction relative to the surface of the supporting substrate. A characterization of nanocrystalline In2O3-derived thin films is presented here with in-plane-isotropic and out-of-plane-anisotropic orientational ordering of the atomic structure, each synthesized using different techniques. The atomic orientations of such films are known to vary based on the synthetic conditions. Here, an azimuthal orientational analysis of these films using GITXS with a single incident angle is shown to resolve the markedly different orientations of the atomic structures with respect to the planar support and the different degrees of long-range order, and hence, the terminal surface chemistries. It is anticipated that orientational analysis of GITXS/PDF data will offer opportunities to extend structural analyses of thin films by providing a means to qualitatively determine the major atomic orientation within nanocrystalline and, eventually, non-crystalline films. Full Article text
rre Current developments and trends in quantum crystallography By journals.iucr.org Published On :: 2024-06-18 Quantum crystallography is an emerging research field of science that has its origin in the early days of quantum physics and modern crystallography when it was almost immediately envisaged that X-ray radiation could be somehow exploited to determine the electron distribution of atoms and molecules. Today it can be seen as a composite research area at the intersection of crystallography, quantum chemistry, solid-state physics, applied mathematics and computer science, with the goal of investigating quantum problems, phenomena and features of the crystalline state. In this article, the state-of-the-art of quantum crystallography will be described by presenting developments and applications of novel techniques that have been introduced in the last 15 years. The focus will be on advances in the framework of multipole model strategies, wavefunction-/density matrix-based approaches and quantum chemical topological techniques. Finally, possible future improvements and expansions in the field will be discussed, also considering new emerging experimental and computational technologies. Full Article text
rre A short note on the use of irreducible representations for tilted octahedra in perovskites By journals.iucr.org Published On :: 2024-08-08 It is pointed out that many authors are unaware that the particular choice of unit-cell origin determines the irreducible representations to which octahedral tilts in perovskites belong. Furthermore, a recommendation is made that the preferred option is with the origin at the B-cation site rather than that of the A site. Full Article text
rre A correction procedure for secondary scattering contributions from windows in small-angle X-ray scattering and ultra-small-angle X-ray scattering By journals.iucr.org Published On :: 2024-03-29 This article describes a correction procedure for the removal of indirect background contributions to measured small-angle X-ray scattering patterns. The high scattering power of a sample in the ultra-small-angle region may serve as a secondary source for a window placed in front of the detector. The resulting secondary scattering appears as a sample-dependent background in the measured pattern that cannot be directly subtracted. This is an intricate problem in measurements at ultra-low angles, which can significantly reduce the useful dynamic range of detection. Two different procedures are presented to retrieve the real scattering profile of the sample. Full Article text
rre Ray-tracing analytical absorption correction for X-ray crystallography based on tomographic reconstructions By journals.iucr.org Published On :: 2024-04-15 Processing of single-crystal X-ray diffraction data from area detectors can be separated into two steps. First, raw intensities are obtained by integration of the diffraction images, and then data correction and reduction are performed to determine structure-factor amplitudes and their uncertainties. The second step considers the diffraction geometry, sample illumination, decay, absorption and other effects. While absorption is only a minor effect in standard macromolecular crystallography (MX), it can become the largest source of uncertainty for experiments performed at long wavelengths. Current software packages for MX typically employ empirical models to correct for the effects of absorption, with the corrections determined through the procedure of minimizing the differences in intensities between symmetry-equivalent reflections; these models are well suited to capturing smoothly varying experimental effects. However, for very long wavelengths, empirical methods become an unreliable approach to model strong absorption effects with high fidelity. This problem is particularly acute when data multiplicity is low. This paper presents an analytical absorption correction strategy (implemented in new software AnACor) based on a volumetric model of the sample derived from X-ray tomography. Individual path lengths through the different sample materials for all reflections are determined by a ray-tracing method. Several approaches for absorption corrections (spherical harmonics correction, analytical absorption correction and a combination of the two) are compared for two samples, the membrane protein OmpK36 GD, measured at a wavelength of λ = 3.54 Å, and chlorite dismutase, measured at λ = 4.13 Å. Data set statistics, the peak heights in the anomalous difference Fourier maps and the success of experimental phasing are used to compare the results from the different absorption correction approaches. The strategies using the new analytical absorption correction are shown to be superior to the standard spherical harmonics corrections. While the improvements are modest in the 3.54 Å data, the analytical absorption correction outperforms spherical harmonics in the longer-wavelength data (λ = 4.13 Å), which is also reflected in the reduced amount of data being required for successful experimental phasing. Full Article text
rre On the analysis of two-time correlation functions: equilibrium versus non-equilibrium systems By journals.iucr.org Published On :: 2024-07-04 X-ray photon correlation spectroscopy (XPCS) is a powerful tool for the investigation of dynamics covering a broad range of timescales and length scales. The two-time correlation function (TTC) is commonly used to track non-equilibrium dynamical evolution in XPCS measurements, with subsequent extraction of one-time correlations. While the theoretical foundation for the quantitative analysis of TTCs is primarily established for equilibrium systems, where key parameters such as the diffusion coefficient remain constant, non-equilibrium systems pose a unique challenge. In such systems, different projections (`cuts') of the TTC may lead to divergent results if the underlying fundamental parameters themselves are subject to temporal variations. This article explores widely used approaches for TTC calculations and common methods for extracting relevant information from correlation functions, particularly in the light of comparing dynamics in equilibrium and non-equilibrium systems. Full Article text
rre Correlative X-ray micro-nanotomography with scanning electron microscopy at the Advanced Light Source By journals.iucr.org Published On :: 2024-10-29 Geological samples are inherently multi-scale. Understanding their bulk physical and chemical properties requires characterization down to the nano-scale. A powerful technique to study the three-dimensional microstructure is X-ray tomography, but it lacks information about the chemistry of samples. To develop a methodology for measuring the multi-scale 3D microstructure of geological samples, correlative X-ray micro- and nanotomography were performed on two rocks followed by scanning electron microscopy with energy-dispersive spectroscopy (SEM-EDS) analysis. The study was performed in five steps: (i) micro X-ray tomography was performed on rock sample cores, (ii) samples for nanotomography were prepared using laser milling, (iii) nanotomography was performed on the milled sub-samples, (iv) samples were mounted and polished for SEM analysis and (v) SEM imaging and compositional mapping was performed on micro and nanotomography samples for complimentary information. Correlative study performed on samples of serpentine and basalt revealed multiscale 3D structures involving both solid mineral phases and pore networks. Significant differences in the volume fraction of pores and mineral phases were also observed dependent on the imaging spatial resolution employed. This highlights the necessity for the application of such a multiscale approach for the characterization of complex aggregates such as rocks. Information acquired from the chemical mapping of different phases was also helpful in segmentation of phases that did not exhibit significant contrast in X-ray imaging. Adoption of the protocol used in this study can be broadly applied to 3D imaging studies being performed at the Advanced Light Source and other user facilities. Full Article text
rre Keyshia Cole arrested on suspicion of battery By www.scpr.org Published On :: Fri, 19 Sep 2014 17:34:44 -0700 Keyshia Cole performs during the 4th annual BET Honors at the Warner Theatre on Jan. 15, 2011 in Washington, DC.; Credit: Kris Connor/Getty Images Police say Grammy-nominated R&B singer Keyshia Cole has been arrested on suspicion of battery after an altercation early Friday morning in Los Angeles. Los Angeles police officer Nuria Vanegas says Cole was arrested around 5 a.m. after someone initiated a private person's arrest. The 32-year-old was booked on suspicion of battery and released from custody Friday afternoon. Police did not release any further details about the incident. An email message sent to Cole's publicist was not immediately returned. Cole's second album, 2007's "Just Like You," produced the songs "Let It Go," ''I Remember" and "Heaven Sent." Full Article
rre Warren, Sanders Call For Expanding Food Aid To College Students By www.scpr.org Published On :: Tue, 11 May 2021 08:20:07 -0700 Sen. Elizabeth Warren holds a news conference in March. She and Sen. Bernie Sanders are leading the push to introduce a bill Tuesday that would make pandemic-related food benefits for college students permanent, and create grants for colleges to address hunger.; Credit: Chip Somodevilla/Getty Images Elissa Nadworny | NPRDemocrats in the House and Senate are introducing legislation Tuesday that would make pandemic-related food benefits for college students permanent. The push is being led by Senators Elizabeth Warren, Democrat of Massachusetts and Bernie Sanders, a Vermont Independent, In the December relief package, Congress increased the number of low-income college students eligible for Supplemental Nutrition Assistance Program (or SNAP) benefits for the duration of the pandemic. That included students who are eligible for work study, have an Expected Family Contribution of zero dollars, or qualify for a maximum Pell Grant on their federal financial aid form. According to The Century Foundation, this expansion affects about 3 million college students. The legislation proposed Tuesday would make these changes permanent, including requiring the U.S. Education Department to notify students they may be eligible for SNAP when they fill out their student aid applications. The bill would also require the Department to collect data on hunger and food insecurity, and would create a $1 billion-a-year grant program for institutions to address hunger on campus. "Far too many college students struggle to meet their basic needs while they get their education and the pandemic has made this problem even worse," Warren said in a statement to NPR. "As students take on a mountain of student loan debt, they shouldn't have to choose between paying tuition and eating." The push comes amid new research that shows 39% of two-year college students are facing food insecurity; for students at 4-year schools the number affected is 29%, according to Temple University's Hope Center for College, Community and Justice. Before the pandemic, in 2019, the U.S. Government Accountability Office issued a report on humger among college students, concluding that over a third of students don't always have enough to eat, and that federal systems already in place, including SNAP, could do a better job of helping them. Many colleges have increased food benefits for their students, creating or expanding emergency grants, food pantries and other forms of assistance. State legislatures in several places including Virginia and Massachusetts have also moved to address issues of hunger on campus. Copyright 2021 NPR. To see more, visit https://www.npr.org. This content is from Southern California Public Radio. View the original story at SCPR.org. Full Article
rre Current Test-Based Incentive Programs Have Not Consistently Raised Student Achievement in U.S. - Improved Approaches Should Be Developed and Evaluated By Published On :: Thu, 26 May 2011 04:00:00 GMT Despite being used for several decades, test-based incentives have not consistently generated positive effects on student achievement, says a new report from the National Research Council. Full Article
rre Current Research Not Sufficient to Assess Deterrent Effect of the Death Penalty By Published On :: Wed, 18 Apr 2012 05:00:00 GMT Research to date on the effect of capital punishment on homicide rates is not useful in determining whether the death penalty increases, decreases, or has no effect on these rates, says a new report from the National Research Council. Full Article
rre Examining U.S. Interregional Travel and Policies – New Report By Published On :: Thu, 07 Jan 2016 06:00:00 GMT A new report from the National Academies of Sciences, Engineering, and Medicine reviews the demand for interregional travel in the U.S. by automobile, airplane, bus, and train and examines the uncertainties that arise in supplying transportation services and infrastructure to accommodate it. Full Article
rre General Support for Science Does Not Always Correlate With Attitudes Toward Specific Science Issues, Says New Report By Published On :: Tue, 09 Aug 2016 05:00:00 GMT U.S. adults perform comparably to adults in other economically developed countries on most measures of science knowledge and support science in general, says a new report from the National Academies of Sciences, Engineering, and Medicine. Full Article
rre New Report Calls for Eliminating Correctable and Avoidable Vision Impairments by 2030 By Published On :: Thu, 15 Sep 2016 05:00:00 GMT Despite the importance of eyesight, millions of people grapple with undiagnosed or untreated vision impairments — ranging from mild conditions to total blindness — and eye and vision health remain relatively absent from national health priority lists, says a new report from the National Academies of Sciences, Engineering, and Medicine. Full Article
rre New Report Calls for Comprehensive Research Campaign to Better Understand, Predict Gulf of Mexico’s Loop Current System By Published On :: Wed, 03 Jan 2018 06:00:00 GMT A new report from the National Academies of Sciences, Engineering, and Medicine calls for an international, multi-institutional comprehensive campaign of research, observation, and analysis activities that would help improve understanding and prediction of the Gulf of Mexico’s Loop Current System (LCS). Full Article
rre To Prevent Sexual Harassment, Academic Institutions Should Go Beyond Legal Compliance to Promote a Change in Culture - Current Approaches Have Not Led to Decline in Harassment By Published On :: Tue, 12 Jun 2018 05:00:00 GMT A systemwide change to the culture and climate in higher education is needed to prevent and effectively respond to sexual harassment, says a new report from the National Academies of Sciences, Engineering, and Medicine. Full Article
rre Research Campaign to Advance Understanding of Gulf of Mexico Loop Current Moves Forward By Awarding $10.3 Million in Initial Grants By Published On :: Wed, 19 Dec 2018 06:00:00 GMT Following recommendations from a National Academies of Sciences, Engineering, and Medicine report released earlier this year, the National Academies’ Gulf Research Program (GRP) is developing a long-term research campaign to improve understanding and prediction of the Gulf of Mexico Loop Current System (LCS). Full Article
rre New Investments Are Needed to Sustain NASA’s Instrumentation and Facilities for Future Extraterrestrial Sample Analyses, Says New Report By Published On :: Thu, 20 Dec 2018 06:00:00 GMT NASA’s investment in new instruments to analyze extraterrestrial samples is insufficient to provide for replacement of existing instruments, says a new report from the National Academies of Sciences, Engineering, and Medicine. Full Article
rre $2.5 Million in Grants Available to Advance Understanding and Prediction of Gulf of Mexico Loop Current By Published On :: Wed, 06 Mar 2019 06:00:00 GMT The Gulf Research Program (GRP) of the National Academies of Sciences, Engineering, and Medicine today announced a new funding opportunity to provide up to $2.5 million in grants to foster innovative approaches that support its ongoing efforts to improve understanding and prediction of the Gulf of Mexico Loop Current System (LCS). Full Article
rre Current Evidence Supports Classification of Red Wolf as a Distinct Species, Report Says, Mexican Gray Wolf Is a Valid Subspecies of Gray Wolf By Published On :: Thu, 28 Mar 2019 05:00:00 GMT Current evidence supports the classification of the contemporary red wolf as a distinct species of wolf, although additional genomic evidence from historic wolf specimens could change that assessment, says Evaluating the Taxonomic Status of the Mexican Gray Wolf and the Red Wolf, a new report from the National Academies of Sciences, Engineering, and Medicine. Full Article