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[ASAP] Optimized Synthesis of 7-Azaindazole by a Diels–Alder Cascade and Associated Process Safety

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Published On :: Fri, 01 May 2020 04:00:00 GMT

Organic Process Research & Development
DOI: 10.1021/acs.oprd.0c00184


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[ASAP] Enzymatic Preparation of the Chiral (<italic toggle="yes">S</italic>)-Sulfoxide Drug Esomeprazole at Pilot-Scale Levels

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Published On :: Sun, 03 May 2020 04:00:00 GMT

Organic Process Research & Development
DOI: 10.1021/acs.oprd.0c00115


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[ASAP] Continuous Process for Preparing the Difluoromethylating Reagent [(DMPU)<sub>2</sub>Zn(CF<sub>2</sub>H)<sub>2</sub>] and Improved Synthesis of the ICHF<sub>2</sub> Precursor

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Published On :: Tue, 05 May 2020 04:00:00 GMT

Organic Process Research & Development
DOI: 10.1021/acs.oprd.0c00089


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[ASAP] <sc>d</sc>-Serine as a Key Building Block: Enzymatic Process Development and Smart Applications within the Cascade Enzymatic Concept

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Published On :: Thu, 07 May 2020 04:00:00 GMT

Organic Process Research & Development
DOI: 10.1021/acs.oprd.0c00024


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[ASAP] Correction to “Application of Crabtree/Pfaltz-type Iridium Complexes for the Catalyzed Asymmetric Hydrogenation of an Agrochemical Building Block”

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Published On :: Fri, 08 May 2020 04:00:00 GMT

Organic Process Research & Development
DOI: 10.1021/acs.oprd.0c00206


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[ASAP] Catalyst-Free Cyclization- and Curtius Rearrangement-Induced Functional Group Transformation: An Improved Synthetic Strategy of First-in-Class ATX Inhibitor Ziritaxestat (GLPG-1690)

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Published On :: Fri, 08 May 2020 04:00:00 GMT

Organic Process Research & Development
DOI: 10.1021/acs.oprd.9b00511


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The effect of crystallite size on low-temperature hydrothermal stability of Cu-SAPO-34

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Catal. Sci. Technol., 2020, Advance Article
DOI: 10.1039/D0CY00414F, Paper
Jinpeng Du, Xiaoyan Shi, Yulong Shan, Yingjie Wang, Wenshuo Zhang, Yunbo Yu, Wenpo Shan, Hong He
Two Cu-SAPO-34 catalysts with different crystallite sizes were obtained, and catalyst with smaller crystallite size had better low-temperature hydrothermal stability because of less Cu2+ species on the surface.
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Synthesis and characterization of a supported Pd complex on carbon nanofibers for the selective decarbonylation of stearic acid to 1-heptadecene: the importance of subnanometric Pd dispersion

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Catal. Sci. Technol., 2020, Advance Article
DOI: 10.1039/D0CY00322K, Paper
Open Access
Elba Ochoa, Wilson Henao, Sara Fuertes, Daniel Torres, Tomas van Haasterecht, Elinor Scott, Harry Bitter, Isabel Suelves, Jose Luis Pinilla
Evaluation of the dispersion of Pd active sites on the catalyst performance during fatty acids decarbonylation to α-olefins was explored in this work. Pd subnanometric particles, clusters and aggregates were found to modulate the catalyst activity.
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Enhancing aqueous pollutants photodegradation via Fermi level matched Z-scheme BiOI/Pt/g-C3N4 photocatalyst: unobstructed photogenerated charge behavior and degradation pathway exploration

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Catal. Sci. Technol., 2020, Accepted Manuscript
DOI: 10.1039/D0CY00429D, Paper
Jingjing Jiang, Yueyu Song, Xingyue Wang, Tianren Li, Mingyu Li, Yanhong Lin, Tengfeng Xie, Shuangshi Dong
Z-scheme photocatalytic system was widely requisited to solve water pollution problem. However, the degradation mechanism for pollutants with Z-scheme photocatalyst has been ambiguous. In this work, an efficient all solid-state...
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Domino lignin depolymerization and reconnection to complex molecules mediated by boryl radicals

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Catal. Sci. Technol., 2020, Advance Article
DOI: 10.1039/D0CY00558D, Paper
Longcheng Hong, Astrid Spielmeyer, Janin Pfeiffer, Hermann A. Wegner
Lignin has been demonstrated as a source of complex molecules via a boryl-mediated domino degradation/reconnection process.
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Hydrodeoxygenation of anisole to benzene over an Fe2P catalyst by a direct deoxygenation pathway

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Catal. Sci. Technol., 2020, Advance Article
DOI: 10.1039/D0CY00046A, Paper
Shuyuan Wang, Dan Xu, Yunlei Chen, Song Zhou, Di Zhu, Xiaodong Wen, Yong Yang, Yongwang Li
Fe2P catalyst was highly selective for the cleavage of C–O bond of anisole via direct deoxygenation pathway.
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Water-soluble NHC-stabilized platinum nanoparticles as recoverable catalysts for hydrogenation in water

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Catal. Sci. Technol., 2020, Advance Article
DOI: 10.1039/D0CY00481B, Paper
Andrea M. Ruiz-Varilla, Edwin A. Baquero, Bruno Chaudret, Ernesto de Jesús, Camino Gonzalez-Arellano, Juan C. Flores
Aromatic compounds have been hydrogenated in water using recoverable catalysts based on water-soluble platinum nanoparticles capped with NHC ligands.
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Enhancing the methane low-temperature conversion on the Zn/ZSM-5 in the presence of methanol by regulating methanol-to-aromatics reaction pathway

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Catal. Sci. Technol., 2020, Accepted Manuscript
DOI: 10.1039/D0CY00449A, Paper
Zhixiang Xi, Bingjie Zhou, Yue Yu, Binbo Jiang, Zhengliang Huang, Zuwei Liao, Jingdai Wang, Yao Yang, Jingyuan Sun, Yongrong Yang
Co-reaction method provides efficient strategy for methane conversion in mild condition, which is of urgent importance of direct valorization of natural gas to liquid hydrocarbons. However, vague mechanism and neglect...
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Seaweed bio-inspired ZnO piezoelectric cilia array applied in microreactors for enhanced photocatalytic performance

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Catal. Sci. Technol., 2020, 10,2337-2342
DOI: 10.1039/C9CY02509J, Paper
Yukai Chen, Jiaojiao Fang, Baoying Dai, Huimin Wei, Jiahui Kou, Chunhua Lu
A piezoelectric built-in electric field is believed to be an effective way to separate photoinduced carriers and enhance photocatalytic performance.
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Microemulsion solventing-out co-precipitation strategy for fabricating highly active Cu–ZnO/Al2O3 dual site catalysts for reverse water gas shift

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Catal. Sci. Technol., 2020, 10,2343-2352
DOI: 10.1039/C9CY02608H, Paper
Ziheng Zhen, Wenxiang Tang, Wei (Willy) Chu, Tao Zhang, Li Lv, Shengwei Tang
A new strategy for the preparation of dual site catalysts is introduced, which combines microemulsion technology and anti-solvent extraction technology.
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Pd–Au bimetallic catalysts supported on ZnO for selective 1,3-butadiene hydrogenation

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Catal. Sci. Technol., 2020, 10,2503-2512
DOI: 10.1039/C9CY02395J, Paper
Open Access
Belén Bachiller-Baeza, Ana Iglesias-Juez, Giovanni Agostini, Eva Castillejos-López
The effect of the ZnO morphology on the properties of Pd–Au bimetallic catalysts has been discussed.
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Path of electron transfer created in S-doped NH2-UiO-66 bridged ZnIn2S4/MoS2 nanosheet heterostructure for boosting photocatalytic hydrogen evolution

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Catal. Sci. Technol., 2020, 10,2531-2539
DOI: 10.1039/D0CY00127A, Paper
Qi Ran, Zebin Yu, Ronghua Jiang, Lun Qian, Yanping Hou, Fei Yang, Fengyuan Li, Mingjie Li, Qianqian Sun, Heqing Zhang
This work introduces the synthesis of ZnIn2S4/NH2-UiO-66/MoS2 sheet heterostructure photocatalysts and their application to photocatalytic hydrogen evolution.
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Trace amounts of Cu(OAc)2 boost the efficiency of cumene oxidation catalyzed by carbon nanotubes washed with HCl

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Catal. Sci. Technol., 2020, 10,2523-2530
DOI: 10.1039/C9CY02536G, Paper
Jie Deng, Yuhang Li, Yonghai Cao, Hongjuan Wang, Hao Yu, Qiao Zhang, Jiangliang Zuo, Feng Peng
Trace amounts of Cu(OAc)2 significantly improve the activity and selectivity of cumene oxidation catalyzed by HCl-washed carbon nanotubes.
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Mechanism of selective and complete oxidation in La2O3-catalyzed oxidative coupling of methane

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Catal. Sci. Technol., 2020, 10,2602-2614
DOI: 10.1039/D0CY00141D, Paper
Shibin Wang, Shenggang Li, David A. Dixon
The catalytic mechanism and reaction network of oxidative coupling of methane over La2O3 are thoroughly investigated by density functional theory calculations.
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Single-step benzene hydroxylation by cobalt(II) catalysts via a cobalt(III)-hydroperoxo intermediate

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Catal. Sci. Technol., 2020, 10,2540-2548
DOI: 10.1039/C9CY02601K, Paper
Karunanithi Anandababu, Sethuraman Muthuramalingam, Marappan Velusamy, Ramasamy Mayilmurugan
Cobalt(II) complexes reported as efficient and selective catalysts for single-step phenol formation from benzene using H2O2. The catalysis proceeds likely via cobalt(III)-hydroperoxo species.
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Alumina grafted SBA-15 sustainable bifunctional catalysts for direct cross-coupling of benzylic alcohols to diarylmethanes

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Catal. Sci. Technol., 2020, 10,2583-2592
DOI: 10.1039/D0CY00471E, Paper
Chandran Rajendran, Govindaswamy Satishkumar, Charlotte Lang, Eric M. Gaigneaux
AlSBA-15 catalysts possessing Brønsted acid and Lewis acid–base bifunctionalities catalyze the direct arylation of benzyl alcohols to diarylmethanes with an 85% product yield through C–O bond activation.
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Gold-catalyzed domino cyclization enabling construction of diverse fused azaspiro tetracyclic scaffolds: a cascade catalysis mechanism due to a substrate and counterion

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Catal. Sci. Technol., 2020, 10,2415-2426
DOI: 10.1039/D0CY00120A, Paper
Yunhe Li, Xiang Zhao
The detailed mechanism and origins of gold-catalyzed domino cyclization to diverse fused azaspiro tetracyclic scaffolds by cooperative dual catalysis and cascade catalysis are systematically studied.
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Acetate-catalyzed hydroboration of CO2 for the selective formation of methanol-equivalent products

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Catal. Sci. Technol., 2020, 10,2407-2414
DOI: 10.1039/D0CY00118J, Paper
Yuri C. A. Sokolovicz, Olalla Nieto Faza, David Specklin, Béatrice Jacques, Carlos Silva López, João H. Z. dos Santos, Henri S. Schrekker, Samuel Dagorne
The acetate anion is a highly robust and effective catalyst for the selective hydroboration of CO2 to methanol-equivalent products.
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Carbon nanotube-supported Cu-based catalysts for oxidative carbonylation of methanol to methyl carbonate: effect of nanotube pore size

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Catal. Sci. Technol., 2020, 10,2615-2626
DOI: 10.1039/C9CY02407G, Paper
Dan Zhao, Guoqiang Zhang, Lifei Yan, Lingqi Kong, Huayan Zheng, Jie Mi, Zhong Li
The inner diameter of CNTs significantly affected the location, dispersion, autoreduction and stability of Cu species and thus the catalytic activity and stability for oxidative carbonylation of methanol to dimethyl carbonate.
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Adjustable anchoring of Ni/Co cations by oxygen-containing functional groups on functionalized graphite paper and accelerated mass/electron transfer for overall water splitting

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Catal. Sci. Technol., 2020, 10,2627-2643
DOI: 10.1039/D0CY00181C, Paper
Yiyi Huang, Lei Sun, Zebin Yu, Ronghua Jiang, Jun Huang, Yanping Hou, Fei Yang, Boge Zhang, Runzhi Zhang, Yalan Zhang
NCS–NCO/FGP0.44 with a cellular network of porous nanosheets and close-contact heterointerface reveals accelerated interfacial mass/electron transportation for overall water splitting.
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Mechanistic insights into photocatalysis and over two days of stable H2 generation in electrocatalysis by a molecular cobalt catalyst immobilized on TiO2

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Catal. Sci. Technol., 2020, 10,2549-2560
DOI: 10.1039/D0CY00330A, Paper
Open Access
Nicola Weder, Benjamin Probst, Laurent Sévery, Ricardo J. Fernández-Terán, Jan Beckord, Olivier Blacque, S. David Tilley, Peter Hamm, Jürg Osterwalder, Roger Alberto
Molecular and heterogeneous water reduction combined: Over 2 days of electrocatalysis of a cobalt polypyridyl catalyst immobilized on TiO2.
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Optimized preparation and regeneration of MFI type base catalysts for D-glucose isomerization in water

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Catal. Sci. Technol., 2020, Advance Article
DOI: 10.1039/D0CY00188K, Paper
Margarida M. Antunes, Auguste Fernandes, Diogo Falcão, Martyn Pillinger, Filipa Ribeiro, Anabela A. Valente
Eco-friendly solid bases possessing hierarchical MFI structure for D-glucose isomerization to D-fructose. Optimizing catalyst synthesis and composition for enhanced stability.
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Mechanistic insights into the oxidation of copper(I) species during NH3–SCR over Cu-CHA zeolites: A DFT study

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Catal. Sci. Technol., 2020, Accepted Manuscript
DOI: 10.1039/D0CY00379D, Paper
Chong Liu, Hiroe Kubota, Takashi Toyao, Zen Maeno, Ken-ichi Shimizu
Selective catalytic reduction of nitrogen oxides using ammonia (NH3–SCR) over Cu-exchanged zeolites proceeds via reduction of Cu(II) to Cu(I) and subsequent reoxidation of Cu(I) to Cu(II). Although the mechanism of...
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Selenium-catalyzed oxidation of alkenes: insight into the mechanisms and developing trend

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Catal. Sci. Technol., 2020, Advance Article
DOI: 10.1039/D0CY00400F, Perspective
Hongen Cao, Rongrong Qian, Lei Yu
Recent progresses of the selenium-catalyzed oxidation of alkenes are summarized at the mechanism level. It may be beneficial for designing novel selenium-containing catalysts and alkene oxidation protocols for the next phase of studies.
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Insights into isothiourea-catalyzed asymmetric [3 + 3] annulation of α,β-unsaturated aryl esters with 2-acylbenzazoles：Mechani-sm, origin of stereoselectivity and switchable chemoselectivity

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Catal. Sci. Technol., 2020, Accepted Manuscript
DOI: 10.1039/D0CY00295J, Paper
Congcong Wang, Shi-Jun Li, Qiao-Chu Zhang, Donghui Wei, Lina Ding
Recently, isothiourea-catalyzed asymmetric [3 + 3] annulation reactions of α,β-unsaturated aryl esters with 2-acylbenzothiazole (or 2-acylbenzoxazole) were reported with switchable chemoselectivity to form either dihydropyridone or dihydropyrone, but predicting the...
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Two-way desorption coupling to enhance the conversion of syngas into aromatics by MnO/H-ZSM-5

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Catal. Sci. Technol., 2020, Advance Article
DOI: 10.1039/D0CY00275E, Paper
Syed Zulfiqar Ali Gilani, Le Lu, Muhammad Tahir Arslan, Babar Ali, Qi Wang, Fei Wei
We herein report a composite catalyst containing partially reducible and highly active manganese oxide and nano-size H-ZSM-5 with short b-axis, prepared for the direct conversion of syngas into aromatics.
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Ru nanoparticles supported on amorphous ZrO2 for CO2 methanation

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Catal. Sci. Technol., 2020, Accepted Manuscript
DOI: 10.1039/D0CY00233J, Paper
Hironori Nagase, Rei Naito, Shohei Tada, Ryuji Kikuchi, Kakeru Fujiwara, Masahiko Nishijima, Tetsuo Honma
The influence of support materials and preparation methods on CO2 methanation activity was investigated using Ru nanoparticles supported on amorphous ZrO2 (am-ZrO2), crystalline ZrO2 (cr-ZrO2), and SiO2. Among them, Ru/am-ZrO2...
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Effective N-methylation of nitroarenes with methanol catalyzed by a functionalized NHC-based iridium catalyst: a green approach to N-methyl amines

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Catal. Sci. Technol., 2020, Accepted Manuscript
DOI: 10.1039/D0CY00707B, Paper
Miguel González-Lainez, M. Victoria Jiménez, Vincenzo Passarelli, Jesús J. Pérez-Torrente
Compound [IrBr(CO)2(κC-tBuImCH2PyCH2OMe)] featuring a flexible pyridine/OMe functionalized NHC ligand κ1C coordinated efficiently catalyzes the selective N-monomethylation of nitroarenes using methanol as both the reducing agent and the C1 source. A...
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Mesoporous Ce-doped ZnO hollow microspheres for oxidation of 1,2-dichlorobenzene

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Catal. Sci. Technol., 2020, Accepted Manuscript
DOI: 10.1039/D0CY00272K, Paper
Xiaodong Ma, Jiaxin Wen, Haiwei Guo, Zizhang Wei, Xu He, Longlong Zhang, BODONG LI, tao wang, YANHU CHENG
Mesoporous Ce-doped ZnO hollow microspheres were synthesized for the oxidative decomposition of 1,2-dichlorobenzene (o-DCB) as a model compound of polychlorinated aromatic hydrocarbons (PCAHs). The results showed that the molar ratios...
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Ligand photodissociation in Ru(II)–1,4,7-triazacyclononane complexes enhances water oxidation and enables electrochemical generation of surface active species

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Catal. Sci. Technol., 2020, Advance Article
DOI: 10.1039/C9CY02575H, Paper
Hussein A. Younus, Nazir Ahmad, Ibrahim Yildiz, Serge Zhuiykov, Shiguo Zhang, Francis Verpoort
Ligand transformations involved in metal complexes during water oxidation (WO), such as ligand decomposition, partial oxidation, or complete dissociation have been reported, however, ligand photodissociation has not been reported yet.
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Homogeneous vs. Heterogeneous: Mechanistic Insights into Iron Group Metal-Catalyzed Reductions from Poisoning Experiments

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Catal. Sci. Technol., 2020, Accepted Manuscript
DOI: 10.1039/D0CY00644K, Minireview
Axel Jacobi von Wangelin, Sebastian Sandl, Dominik Gärtner
Iron group metal catalysts constitute a promising alternative to well-established noble metal catalysts in reduction reactions. However, the development of effective 3d metal catalysts has largely been hampered by their...
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Heterogenization for polyoxometalates as solid catalysts in aerobic oxidation of glycerol

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Catal. Sci. Technol., 2020, Accepted Manuscript
DOI: 10.1039/D0CY00403K, Paper
Meilin Tao, yue li, Yiming Li, Xueyan Zhang, Yurii Geletii, Xiaohong Wang, Craig L Hill
A series of heterogeneous catalysts based on phosphomolybdic salts with different Lewis metals in counter or substituent places LnPMo12O40 (L = Al3+, Fe3+, Cr3+, Ti4+, Zr4+ and Zn2+, abbreviated as...
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Stability of the ketyl radical as a descriptor in the electrochemical coupling of benzaldehyde

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Catal. Sci. Technol., 2020, Advance Article
DOI: 10.1039/D0CY00282H, Paper
Jacob Anibal, Arnav Malkani, Bingjun Xu
Electroreductive coupling is an emerging pathway for the renewable upgrading of biomass derived oxygenates. This work investigates electrochemical benzaldehyde reduction on Au, Cu, Pt and Pd using reactivity testing and in situ spectroscopy.
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From cellulose to 1,2,4-benzenetriol via catalytic degradation over a wood-based activated carbon catalyst

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Catal. Sci. Technol., 2020, Advance Article
DOI: 10.1039/D0CY00424C, Paper
Qiong Wu, Baozheng Zhao, Shiwei Liu, Shitao Yu, Lang Huang, Arthur J. Ragauskas
1,2,4-Benzenetriol was obtained from cellulose hydrothermal degradation using phosphoric acid-activated wood-based AC as the catalyst.
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Does the structure of CuZn hydroxycarbonate precursors affect the intrinsic hydrogenolysis activity of CuZn catalysts?

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Catal. Sci. Technol., 2020, Advance Article
DOI: 10.1039/D0CY00143K, Paper
Violetta Pospelova, Jaroslav Aubrecht, Kateřina Pacultová, Miloslav Lhotka, Oleg Kikhtyanin, David Kubička
A comparative study of the properties and activity of catalysts derived from single-phase CuZn precursors to elucidate the effect of the precursor structure on the catalyst activity in DMA hydrogenolysis and to examine replacement of CuCr catalysts.
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Phosphine-catalyzed [3 + 2] annulation of 2-aminoacrylates with allenoates and mechanistic studies

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Catal. Sci. Technol., 2020, Accepted Manuscript
DOI: 10.1039/D0CY00092B, Paper
Xiao-Yun Wu, Hou-Ze Gui, Harish Jangra, Yin Wei, Min Shi, Hendrik Zipse
A convenient and efficient strategy for the synthesis of 3-pyrrolines containing an amino quaternary stereogenic center via phosphine-catalyzed formal [3 + 2] annulation of allenoates with 2-aminoacrylates is disclosed. A...
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Hierarchical Z-scheme 1D/2D architecture with TiO2 nanowires decorated by MnO2 nanosheets for efficient adsorption and full spectrum photocatalytic degradation of organic pollutants

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Catal. Sci. Technol., 2020, Accepted Manuscript
DOI: 10.1039/D0CY00419G, Paper
Jiejing Zhang, Yajie Hu, Hong Zheng, Pengyi Zhang
Constructing composite photocatalysts with efficient photocatalytic activity, wide optical response range and excellent stability has great significance for the removal of organic pollutants in water. Herein, we report a novel...
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Horizontal Scroll in Firefox

By css-tricks.com
Published On :: Wed, 22 Jan 2020 06:50:20 +0000

Hi,

I’m playing with this horizontal scroll, but having trouble getting it to work with Firefox. Chrome and Safari handle it fine. I have no way to test IE. Any tips or ideas?

codepen https://codepen.io/sarcodes/pen/XWJoBGy


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UTI MF files draft papers for IPO; issue size likely to be up to Rs 4000 cr

By www.business-standard.com
Published On :: Thu, 19 Dec 2019 22:32:00 +0530

The issue size is expected to be Rs 3,000-4,000 crore, valuing the AMC at Rs 10,000-11,000 crore


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New containment zones come up in south Kolkata

By timesofindia.indiatimes.com
Published On :: Sat, 09 May 2020 04:00:00 IST

Several south Kolkata neighbourhoods, which had managed to stave off coronavirus for the past 40 days, are now on the city’s containment-zone map with fresh cases being reported from them. The affected portions include added areas — both sides of the Tolly canal, EM Bypass and Behala — and some upscale south Kolkata locations, like Lord Sinha Road and Hindustan Park.


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Sara / Garth Ennis, writer; Steve Epting, art; Elizabeth Breitweiser, color art

By library.mit.edu
Published On :: Sun, 17 Nov 2019 06:50:01 EST

Barker Library - PN6728.S27 2018


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The 7 deadly sins / written by Tze Chun; drawn by Artyom Trakhanov; and colored by Giulia Brusco

By library.mit.edu
Published On :: Sun, 17 Nov 2019 06:50:01 EST

Barker Library - PN6728.A17 2018


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Comics and sacred texts: reimagining religion & graphic narratives / edited by Assaf Gamzou, Ken Koltun-Fromm

By library.mit.edu
Published On :: Sun, 2 Feb 2020 06:51:59 EST

Dewey Library - PN6712.C53 2018


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Women's manga in Asia and beyond: uniting different cultures and identities / Fusami Ogi, Rebecca Suter, Kazumi Nagaike, John A. Lent, editors

By library.mit.edu
Published On :: Sun, 23 Feb 2020 07:00:06 EST

Rotch Library - PN6714.W664 2019


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Ricanstruction: reminiscing & rebuilding Puerto Rico / publisher, executive producer, editor, title design, book design, writer, Edgardo Miranda-Rodriguez ; cover artists Tony Daniel, Danny Miki, Tomeu Morey ; inside cover artist Nicole Virella ; back

By library.mit.edu
Published On :: Sun, 23 Feb 2020 07:00:06 EST

Barker Library - PN6726.R53 2018


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