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Detection of Nutrition and Toxic Elements in Pakistani Pepper Powders Using Laser Induced Breakdown Spectroscopy

Anal. Methods, 2020, Accepted Manuscript
DOI: 10.1039/D0AY00630K, Paper
Imran Rehan, Kamran Rehan, Muhammad Zubair Khan, Sabiha Sultana, Riaz Khan, Hamdullah Khan
In the current paper, we applied laser induced breakdown spectroscopy (LIBS) to determine the elemental distribution of nutritional and trace heavy metals in pepper powders available in Pakistan using standard...
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Detection of prostate-specific antigen in semen using DNA aptamers: an application of nucleic acid aptamers in forensic body fluid identification

Anal. Methods, 2020, Accepted Manuscript
DOI: 10.1039/D0AY00371A, Paper
Tetsuya Satoh, Seiya Kouroki, Yusuke Kitamura, Toshihiro Ihara, Kazutoshi Matsumura, Susumu Iwase
In forensics, body fluid identification plays an important role because it aids in reconstructing the crime scene. Therefore, it is essential to develop simple and reliable techniques for body fluid...
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Direct measurement of Cu and Pb isotopic ratios without column chemistry for bronzes using MC-ICP-MS

Anal. Methods, 2020, Accepted Manuscript
DOI: 10.1039/D0AY00561D, Paper
Zhian Bao, Chunlei Zong, Peng Liang, Yan Zhang, Kaiyun Chen, Honglin Yuan
This study presents a practical method for high-precision Cu and Pb isotope determination without column chemistry for bronzes using MC-ICP-MS. The standard-sample bracketing method combined with Ga internal normalization (SSBIN)...
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Rapid detection of quality of Japanese fermented soy sauce using near-infrared spectroscopy

Anal. Methods, 2020, Advance Article
DOI: 10.1039/D0AY00521E, Paper
Shuo Wang, Takehiro Tamura, Nobuyuki Kyouno, Xiaofang Liu, Han Zhang, Yoshinobu Akiyama, Jie Yu Chen
The application of NIR spectroscopy has great potential as an alternative quality control method, which provides a robust model for routinely estimating the final quality of soy sauce production rapidly and economically.
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Shenling Baizhu San improves functional dyspepsia in rats as revealed by 1H-NMR based metabolomics

Anal. Methods, 2020, Advance Article
DOI: 10.1039/D0AY00580K, Paper
Shaobao Zhang, Zengmei Xu, Xueqing Cao, Yuzhen Xie, Lei Lin, Xiao Zhang, Baorong Zou, Deliang Liu, Ying Cai, Qiongfeng Liao, Zhiyong Xie
Functional dyspepsia (FD), a common gastrointestinal disorder around the world, is driven by multiple factors, making prevention and treatment a major challenge.
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Targeted profiling of amino acid metabolome in serum by a liquid chromatography-mass spectrometry method: application to identify potential markers for diet-induced hyperlipidemia

Anal. Methods, 2020, Advance Article
DOI: 10.1039/D0AY00305K, Paper
Xiao-fan Wang, You-xi Zhang, Hai-ying Ma
Targeted profiling of amino acid metabolome in serum by LC-MS: application to identify potential markers for diet-induced hyperlipidemia.
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Fast magnetic solid-phase extraction using Fe3O4-NH2@MOF material for monohydroxy polycyclic aromatic hydrocarbons in urine of coke-oven workers

Anal. Methods, 2020, Accepted Manuscript
DOI: 10.1039/D0AY00449A, Paper
Yahui Wang, Meng Yan, Qianqian Ji, Manman Wang, Qian Wang, Xue-Sheng Wang, Yulan Hao
In this work, magnetic material (Fe3O4-NH2@MIL-101) was successfully prepared, and the material was used as a sorbent for the magnetic solid-phase extraction (MSPE) of trace level monohydroxy polycyclic aromatic hydrocarbons...
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Derivatization and rapid GC—MS screening of chlorides relevant to the Chemical Weapons Convention in organic liquid samples

Anal. Methods, 2020, Accepted Manuscript
DOI: 10.1039/D0AY00263A, Paper
Open Access
Marja-Leena Kuitunen, Jorgelina Cecilia Altamirano, Peter Siegenthaler, Terhi Hannele Taure, Vesa Mauri Antero Häkkinen, Paula Vanninen
A simple derivatization technique was developed for the analysis of seven Schedule 3 chemicals and one Schedule 2 chemical listed in the Chemical Weapons Conventions (CWC). Phosgene, phosphorus oxychloride, phosphorus...
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Ultrasensitive immunochromatographic strips for fast screening of the nicarbazin marker in chicken breast and liver samples based on monoclonal antibodies

Anal. Methods, 2020, 12,2143-2151
DOI: 10.1039/D0AY00414F, Paper
Xiaoxin Xu, Liqiang Liu, Xiaoling Wu, Hua Kuang, Chuanlai Xu
Nicarbazin is an anticoccidial drug with a residue limit in animal husbandry.
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Improving the determination of celecoxib in body fluids and pharmaceuticals using a new selective and thermosensitive molecularly imprinted poly(vinylidene fluoride) membrane

Anal. Methods, 2020, 12,2185-2195
DOI: 10.1039/D0AY00237B, Paper
Negin Yazdanian, Behrouz Akbari-Adergani, Maryam Kazemipour, Homayon Ahmad Panahi, Mehran Javanbakht
Molecularly imprinted membranes that demonstrated high selectivity for celecoxib were synthesized using N-vinylcaprolactam and 2-hydroxyethyl methacrylate.
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Multi-residue determination of micropollutants in Nigerian fish from Lagos lagoon using ultrasound assisted extraction, solid phase extraction and ultra-high-performance liquid chromatography tandem mass spectrometry

Anal. Methods, 2020, 12,2114-2122
DOI: 10.1039/D0AY00411A, Paper
Idera Fabunmi, Natalie Sims, Kathryn Proctor, Aderonke Oyeyiola, Temilola Oluseyi, Kehinde Olayinka, Barbara Kasprzyk-Hordern
This reports for the first time a simple and robust approach in determining pharmaceuticals in different fish species in Nigeria.
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Development of a paper-immobilized yeast biosensor for the detection of physiological concentrations of doxycycline in technology-limited settings

Anal. Methods, 2020, 12,2123-2132
DOI: 10.1039/D0AY00001A, Paper
Rachel A. Miller, Galen Brown, Elsa Barron, Jamie L. Luther, Marya Lieberman, Holly V. Goodson
To combat pharmaceutical counterfeiting in low- and middle-income countries (LMIC), there is a need for improved low-cost, portable methods that monitor pharmaceutical concentrations relevant to dosage forms and physiological fluids.
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Aptamer-based fluorometric determination of chloramphenicol by controlling the activity of hemin as a peroxidase mimetic

Anal. Methods, 2020, Advance Article
DOI: 10.1039/D0AY00389A, Paper
Ling-Chen Wang, Cheng-Yi Hong, Zheng-Zhong Lin, Xiao-Mei Chen, Zhi-Yong Huang
A method for the aptamer-based determination of chloramphenicol (CAP) was developed by exploiting the peroxidase mimicking activity of hemin.
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In situ imaging of intracellular human telomerase RNA with molecular beacon-functionalized gold nanoparticles

Anal. Methods, 2020, Advance Article
DOI: 10.1039/D0AY00461H, Paper
Tao Xie, Ziyan Fan, Ruilong Zhang, Xiaohe Tian, Guangmei Han, Zhengjie Liu, Zhongping Zhang
We develop molecular beacon-functionalized gold nanoparticles for in situ human telomerase RNA imaging in live cells.
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Correction: Towards simultaneous quantification of protease inhibitors and inflammatory biomarkers in serum for people living with HIV

Anal. Methods, 2020, 12,2196-2196
DOI: 10.1039/D0AY90050H, Correction
Open Access
  This article is licensed under a Creative Commons Attribution 3.0 Unported Licence.
Pengyi Wang, Charles S. Venuto, Raymond Cha, Benjamin L. Miller
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Determination of polychlorinated biphenyls and organochlorine pesticides in Chinese mitten crabs (Eriocheir sinensis) using modified QuEChERS followed by GC-MS

Anal. Methods, 2020, Advance Article
DOI: 10.1039/D0AY00519C, Paper
Ting Liu, Jianguang Zhou, Li He, Jinhua Gan
A new QuEChERS method followed by GC-MS was developed for the simultaneous analysis of polychlorinated biphenyls (PCBs) and organochlorine pesticides (OCPs) in Chinese mitten crabs.
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Rh(III) hydroxocomplexes speciation using HPLC-ESI-MS

Anal. Methods, 2020, Accepted Manuscript
DOI: 10.1039/D0AY00363H, Paper
Victoria V Volchek, Semen Nikolaevich Berdyugin, Olga Vasil`evna Shuvaeva, Dmitriy Sheven, Danila Vasilchenko, Sergey Korenev
A mixture of rhodium(III) hydroxocomplexes formed during the polycondensation process in alkaline media has been fully characterized by the hyphenated high performance liquid chromatography with electrospray ionization mass spectrometry (HPLC-ESI-MS)....
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Au nanoparticle preconcentration coupled with CE-electrochemiluminescence detection for sensitive analysis of fluoroquinolones in European eel (Anguilla anguilla)

Anal. Methods, 2020, Accepted Manuscript
DOI: 10.1039/D0AY00264J, Paper
Longhua Guo, Meihua Liu, Yuechun Yin, Lifen Chen, Zhitao Chen, Jing-Jing Liu, Bin Qiu
In this work, a novel method based on gold nanoparticle preconcentration coupled with CE for electrochemiluminescent detection of ciprofloxacin, enrofloxacin, ofloxacin, and norfloxacin in European eels was developed. The addition...
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Colorimetric speciation analysis of chromium using 2-thiobarbituric acid capped silver nanoparticles

Anal. Methods, 2020, Advance Article
DOI: 10.1039/D0AY00160K, Paper
Kamal Mousapour, Salahaddin Hajizadeh, Khalil Farhadi
Colorimetric determination of Cr(III) and Cr(VI) based on 2-thiobarbituric acid capped silver nanoparticles.
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Confirmation of brand identification in infant formulas by using near-infrared spectroscopy fingerprints

Anal. Methods, 2020, Advance Article
DOI: 10.1039/D0AY00375A, Paper
Shuyi Chang, Chengcheng Yin, Sha Liang, Mei Lu, Ping Wang, Zhicheng Li
The NIR spectra of 12 batches of each stage of Brand A infant formulas.
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Solid-phase microextraction using a β-ketoenamine-linked covalent organic framework coating for efficient enrichment of synthetic musks in water samples

Anal. Methods, 2020, Advance Article
DOI: 10.1039/C9AY02755F, Paper
Lian Wen, Peng Wu, Lei-Lei Wang, Li-Zong Chen, Ming-Lin Wang, Xia Wang, Jin-Ming Lin, Ru-Song Zhao
This study indicated the promising applicability of the TpPa-1 as a solid-phase microextraction fiber coating for reliably detecting synthetic musks at trace levels from environmental samples.
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A high-throughput plasmonic tongue using an aggregation assay and nonspecific interactions: classification of taste profiles in maple syrup

Anal. Methods, 2020, Advance Article
DOI: 10.1039/C9AY01942A, Paper
Simon Forest, Trevor Théorêt, Julien Coutu, Jean-Francois Masson
A simple colorimetric test detects off-flavour profiles of maple syrups in minutes, which are detectable by the naked eye.
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Effects of harvesting and extraction methods on metabolite recovery from adherently growing mammalian cells

Anal. Methods, 2020, Advance Article
DOI: 10.1039/C9AY02753J, Paper
Yun Luo, Ningbo Geng, Baoqin Zhang, Jiping Chen, Haijun Zhang
We compare the efficiencies of different cell harvesting methods and metabolite extraction methods in sample preparation procedures and provide a cell sample processing protocol which focuses on maximizing metabolite recovery ranging from polar to lipidic ones.
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A rapid and colorimetric biosensor based on GR-5 DNAzyme and self-replicating catalyzed hairpin assembly for lead detection

Anal. Methods, 2020, 12,2215-2220
DOI: 10.1039/D0AY00091D, Paper
Fang Wang, Jianyuan Dai, Hongli Shi, Xiaoqian Luo, Lan Xiao, Cuisong Zhou, Yong Guo, Dan Xiao
A rapid and colorimetric biosensor for Pb2+ detection has been constructed on the basis of Pb2+-dependent GR-5 DNAzyme and the self-replicating catalyzed hairpin assembly (SRCHA) reaction.
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Detection of organophosphorus compounds using a surface acoustic wave array sensor based on supramolecular self-assembling imprinted films

Anal. Methods, 2020, 12,2206-2214
DOI: 10.1039/D0AY00211A, Paper
Yong Pan, Tengxiao Guo, Genwei Zhang, Junchao Yang, Liu Yang, Bingqing Cao
In this study, diisopropyl methylphosphonate (DIMP), tributyl phosphate (TBP), and dimethyl methylphosphonate (DMMP) were selected as organophosphorus chemical warfare agent (CWA) simulants.
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Hydrothermal synthesis of Auricularia auricula derived nitrogen, phosphorus-doped carbon dots and application in Ag(I) and 4-nitrophenol detection and bioimaging

Anal. Methods, 2020, 12,2237-2243
DOI: 10.1039/D0AY00316F, Paper
Yujiao Tu, Suping Wang, Xiaotian Yuan, Pengfei Song, Yunlin Wei, Kunhao Qin, Qi Zhang, Xiuling Ji
Schematic of the synthetic route for fluorescent Aa N,P-CDs and their application in the detection of 4-NP and Ag(I) and bioimaging.
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Adsorptive removal of Hg2+ from environmental water samples using thioglycerol-intercalated magnetic layered double hydroxides

Anal. Methods, 2020, 12,2279-2286
DOI: 10.1039/D0AY00448K, Paper
Ali Esrafili, Mahnaz Ghambarian, Mohammad Tajik, Mahroo Baharfar
Herein, the removal of Hg2+ from environmental water samples was carried out using a novel nanoadsorbent based on magnetite nanoparticles coated by a thioglycerol-intercalated layered double hydroxide.
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Identification of Gentiana rigescens from different geographical origins based on HPLC and FTIR fingerprints

Anal. Methods, 2020, 12,2260-2271
DOI: 10.1039/D0AY00309C, Paper
Yanli Zhao, Tianjun Yuan, Lihua Wu, Ji Zhang, Zhitian Zuo, Yuanzhong Wang
Gentiana rigescens is a traditional Chinese medicine with efficacy in liver protection, as a cholagogic, anti-hyperglycemic, and anti-hypertension agent, and in relieving spasms and pain.
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Selection and optimization of protein and carbohydrate assays for the characterization of marine biofouling

Anal. Methods, 2020, 12,2228-2236
DOI: 10.1039/D0AY00272K, Paper
Chloe Richards, Nicole O'Connor, Diveena Jose, Alan Barrett, Fiona Regan
Biofilms comprise a set of microorganisms attached to a surface through extracellular polymeric substances (EPS). Development of reliable analytical assays are valuable in determining the rate of biofilm attachment on surfaces.
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Ion chromatography for monitoring [NTf2]− anion contaminants in pure and saline water

Anal. Methods, 2020, 12,2244-2252
DOI: 10.1039/D0AY00337A, Paper
Coby J. Clarke, Liem Bui-Le, Jason Hallett
An optimized ion chromatography method for quantifying highly polarizable [NTf2] anions in high salinity wastewater is presented.
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Detection of radium at the attogram per gram level in copper by inductively coupled plasma mass spectrometry after cation-exchange chromatography

Anal. Methods, 2020, 12,2272-2278
DOI: 10.1039/D0AY00512F, Paper
Mélodie Bonin, Dominic Larivière, Pavel P. Povinec
In this study, a new method was developed for the separation and isolation of radium from metallic copper.
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What’s novel in the new Eurachem guide on uncertainty from sampling?

Anal. Methods, 2020, 12,2295-2297
DOI: 10.1039/D0AY90051F, AMC Technical Brief
Analytical Methods Committee, AMCTB No. 96
This Technical Brief aims to explain how the new second edition of the Eurachem guide, Measurement uncertainty arising from sampling, differs significantly from the first edition that was published in 2007.
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Development and validation of a real-time microelectrochemical sensor for clinical monitoring of tissue oxygenation/perfusion

Anal. Methods, 2020, Advance Article
DOI: 10.1039/D0AY00206B, Paper
Gama Theophile Gnahoré, Jack L. Kelly, Saidhbhe L. O'Riordan, Fiachra B. Bolger, Michelle M. Doran, Michelle Sands, John P. Lowry
Oxygen is critically important to tissue viability and there is increasing demand for its reliable real-time clinical monitoring in order to prevent, diagnose and treat several pathological disorders, including hypoxia, stroke and reperfusion injury.
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A simple paper-based approach for arsenic determination in water using hydride generation coupled with mercaptosuccinic-acid capped CdTe quantum dots

Anal. Methods, 2020, Accepted Manuscript
DOI: 10.1039/D0AY00273A, Paper
Oraphan Thepmanee, Kanlaya Prapainop Katewongsa, Obnithi Nooppha, Nuanlaor Ratanawimarnwong, Weena Siangproh, Orawon Chailapakul, Kriangsak Songsrirote
This research aims to develop a simple paper-based device for arsenic detection in water samples where a hydride generation technique coupled with mercaptosuccinic acid-capped CdTe quantum dots (MSA-CdTe QDs) as...
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ELISA as an effective tool to determine spatial and seasonal occurrence of emerging contaminants in the aquatic environment

Anal. Methods, 2020, Advance Article
DOI: 10.1039/D0AY00426J, Paper
Carla Patrícia Silva, Tânia Carvalho, Rudolf J. Schneider, Valdemar I. Esteves, Diana L. D. Lima
Monitoring emerging contaminants is essential as they represent a risk to the aquatic environment. ELISA is a promising method for their quantification mostly because it allows controlling their concentration levels through large screening campaigns.
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A flower-like Ag coated with molecularly imprinted polymers as surface-enhanced Raman scattering substrate for sensitive and selective detection of glibenclamide

Anal. Methods, 2020, Accepted Manuscript
DOI: 10.1039/D0AY00575D, Paper
Xiaohui Ren, Xin Li
The flower-like Ag, was formed by nanosheets self-assembly, as SERS active substrate was utilized for preparation of flower-like Ag@molecularly imprinted polymers (MIPs) surface-enhanced Raman scattering (SERS) sensor. Based on the...
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Fabrication of an electrochemical sensor based on metal-organic framework ZIF-8 for quantitation of silver ion: optimizing experimental conditions by central composite design (CCD)

Anal. Methods, 2020, Accepted Manuscript
DOI: 10.1039/D0AY00843E, Paper
Farzaneh Hashemi , Ali Reza Zanganeh, Farid Naeimi , Maryam Tayebani
The ZIF-8 was synthesized and carbon paste electrode (CPE) modified with this metal-organic framework utilized for quantitation of silver(Ι) by differential pulse anodic stripping voltammetry (DPASV) technique. The prepared ZIF-8...
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Digital Reference Section (DRS) Virtual Programs: New blog post invites readers to "Sample a Taste of History This Thanksgiving"

Find a new and historic recipe for a dish to put on your Thanksgiving table in What Mrs. Fisher Knows About Old Southern Cooking. This cookbook, published in 1881, is highlighted in a recent post on the Library of Congress Blog. Abby Fisher perfected her culinary skills as an enslaved cook on a South Carolina plantation but went on to establish a successful catering business in San Francisco and publish a compilation of her recipes—one of the first by an African-American. Learn more about this remarkable woman and, this Thanksgiving, sample a taste of history!

Click here to go to the Library of Congress Blog post, "Sample a Taste of History This Thanksgiving!"




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The Oxford handbook of Anglo-Saxon archaeology [electronic resource] / edited by Helena Hamerow, David A. Hinton and Sally Crawford.

Oxford : Oxford University Press, 2011.




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Recharting the Black Atlantic [electronic resource] : modern cultures, local communities, global connections / edited by Annalisa Oboe and Anna Scacchi

New York : Routledge, 2008




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Asian-European relations [electronic resource] : building blocks for global governance? / edited by Jürgen Rüland [and others]

London ; New York : Routledge, 2008




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Covid-19 Factoid: Over 3,000 dying daily, and three other data trends

The US, Italy and Spain together share almost half the total Covid-19 cases across the globe




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Covid-19 Factoid: Gap between daily new cases and recoveries widening

The world is adding over 70,000 cases everyday while the daily recoveries are still sub-15,000 on an average in the last three days.




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Covid-19 Factoid: Counting the dead - from the US to Punjab and Iran

The US remains the most affected country with over 340,000 cases and the death toll at over 11,000




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Covid-19 factoid: Alarm bells ring as India adds 1,500 cases in a day

Country's death toll consistently rising too, taking just two days to add the last 50 fatalities to the total.




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I-T dept, GSTN, CBIC caution people against phishing emails promising refunds

Separately GST Network, the company handling the technology backbone for Goods and Services Tax, cautioned against a fraud website onlinefilingindia.in asking taxpayers not to reveal personal and bank details.




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India looks to save Rs 25,000 crore by stocking cheap oil

India is looking to shave Rs 25,000 crore off its crude import bill by storing cheap oil in ships for future use, allowing the government fiscal headroom for spending on more public welfare measures needed in its fight against the coronavirus pandemic.




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Nabard refinances close to Rs 13,000 crore to state co-op banks and RRBs to assit farmers deal on-going lockdown

The loan has been disbursed under a refinance scheme by Nabard from its own resources and was given this week. "An amount of Rs 12,767 crore has been disbursed this week to StCBs and RRBs across the country in a bid to augment their resources during the ongoing lockdown conditions for extending credit to farmers," Nabard said.




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Coronavirus: There’s no free lunch, says CEA on demand for big-bang stimulus

KV Subramanian said India’s GDP is likely to grow 2 per cent for the full financial year.




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Covid alters India's borrowing plan, target now raised to Rs 12L cr

Govt will borrow Rs 6L cr from the market via gilts through the remaining part of the first half of the year.