ones
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The archaeology of human bones [Electronic book] / Simon Mays.
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The archaeology of ethnicity : constructing identities in the past and present [Electronic book] / Siân Jones.
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Shear zones in granular mixtures of hard and soft particles with high and low friction
Soft Matter, 2024, 20,3118-3130
DOI: 10.1039/D4SM00100A, Paper
DOI: 10.1039/D4SM00100A, Paper
Open Access
This article is licensed under a Creative Commons Attribution 3.0 Unported Licence.
Aditya Pratap Singh, Vasileios Angelidakis, Thorsten Pöschel, Sudeshna Roy
Granular materials show inhomogeneous flows characterized by strain localization.
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Granular materials show inhomogeneous flows characterized by strain localization.
The content of this RSS Feed (c) The Royal Society of Chemistry
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Nickel-catalyzed γ-alkylation of cyclopropyl ketones with unactivated primary alkyl chlorides: balancing reactivity and selectivity via halide exchange
RSC Adv., 2024, 14,12883-12887
DOI: 10.1039/D4RA02616K, Paper
DOI: 10.1039/D4RA02616K, Paper
Open Access
This article is licensed under a Creative Commons Attribution-NonCommercial 3.0 Unported Licence.
Zheng-Ying Wang, Shi-Zheng Liu, Cong Guo, Yi-Zheng Cheng, Qiang Li, Jianmin Dou, Dacheng Li
Nickel-catalyzed cross-electrophile coupling of cyclopropyl ketones and alkyl chlorides. High reactivity and selectivity can be achieved with sodium iodide as a cocatalyst that generates a low concentration of alkyl iodide via halide exchange.
The content of this RSS Feed (c) The Royal Society of Chemistry
Nickel-catalyzed cross-electrophile coupling of cyclopropyl ketones and alkyl chlorides. High reactivity and selectivity can be achieved with sodium iodide as a cocatalyst that generates a low concentration of alkyl iodide via halide exchange.
The content of this RSS Feed (c) The Royal Society of Chemistry
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DFT rationalization of the mechanism and selectivity in a gold-catalyzed oxidative cyclization of diynones with alcohols
Phys. Chem. Chem. Phys., 2024, Advance Article
DOI: 10.1039/D4CP01700E, Paper
DOI: 10.1039/D4CP01700E, Paper
Guowei Yan, Ji Ma, Simeng Qi, Alexander M. Kirillov, Lizi Yang, Ran Fang
The mechanism, regioselectivity, and chemoselectivity in a gold-catalyzed oxidative cyclization of diynones with alcohols to give furan-3-carboxylate derivatives were explored by density functional theory (DFT).
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The mechanism, regioselectivity, and chemoselectivity in a gold-catalyzed oxidative cyclization of diynones with alcohols to give furan-3-carboxylate derivatives were explored by density functional theory (DFT).
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Expedient (3+3)-annulation of carbonyl ylides with azaoxyallyl cations: formal access to oxa-benzo[c]azepin-3-ones
Chem. Commun., 2024, 60,13368-13371
DOI: 10.1039/D4CC04946B, Communication
DOI: 10.1039/D4CC04946B, Communication
Kshitiz Verma, Hemanga Bhattacharyya, Sharajit Saha, Tharmalingam Punniyamurthy
Cascade C–C/C–N bond formation of carbonyl ylides with azaoxyallyl cations generated in situ using Rh-catalysis has been accomplished in the presence of a base at room temperature.
The content of this RSS Feed (c) The Royal Society of Chemistry
Cascade C–C/C–N bond formation of carbonyl ylides with azaoxyallyl cations generated in situ using Rh-catalysis has been accomplished in the presence of a base at room temperature.
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Facile synthesis of spiro-pyrazolone-tetrahydrofurans/pyrans: ipso-cyclization of arylidene pyrazolones with haloalcohols
New J. Chem., 2024, Advance Article
DOI: 10.1039/D4NJ00447G, Paper
DOI: 10.1039/D4NJ00447G, Paper
Kavyashree Kuppayya Gond, Mahagundappa Rachappa Maddani
Facile synthesis of spiro-pyrazolone-tetrahydrofurans & pyrans by base-mediated cascade ipso-cyclization of haloalcohols & arylidine pyrazolones is realised. Features include brief reaction time, practicality, good yields and mild reaction conditions.
To cite this article before page numbers are assigned, use the DOI form of citation above.
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Facile synthesis of spiro-pyrazolone-tetrahydrofurans & pyrans by base-mediated cascade ipso-cyclization of haloalcohols & arylidine pyrazolones is realised. Features include brief reaction time, practicality, good yields and mild reaction conditions.
To cite this article before page numbers are assigned, use the DOI form of citation above.
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Sharing our latest differential privacy milestones and advancements
Google is committed to investing in privacy-enhancing technologies (PETs) to ensure user data privacy, improving products like Google Home and Google Search.
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Alleviation of Cadmium-Induced Oxidative Damage through Application of Zinc Oxide Nanoparticles and Strigolactones in Solanum lycopersicum L.
Environ. Sci.: Nano, 2024, Accepted Manuscript
DOI: 10.1039/D3EN00796K, Paper
DOI: 10.1039/D3EN00796K, Paper
Vaseem Raja, Karanpal Singh, Sami Ullah Qadir, Jagpreet Singh, Ki-Hyun Kim
In this research, zinc oxide nanoparticles (ZnO NPs) are bio-synthesized using Mangifera indica leaf extract as a sustainable capping and stabilizing source. The spherical morphology, crystallinity, and average size (17.97...
The content of this RSS Feed (c) The Royal Society of Chemistry
In this research, zinc oxide nanoparticles (ZnO NPs) are bio-synthesized using Mangifera indica leaf extract as a sustainable capping and stabilizing source. The spherical morphology, crystallinity, and average size (17.97...
The content of this RSS Feed (c) The Royal Society of Chemistry
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New York City bans use of TikTok on city-owned phones
Joins US federal government, majority of states in banning the social media app on security concerns
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How Will the Prabowo Administration Shape Indonesia’s Foreign Policy as a Middle Power?
How Will the Prabowo Administration Shape Indonesia’s Foreign Policy as a Middle Power? How Will the Prabowo Administration Shape Indonesia’s Foreign Policy as a Middle Power?
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Strategic Partners or Fickle Friends? Indonesia’s Perceptions of the US-Australia Defense and Security Relationship
Strategic Partners or Fickle Friends? Indonesia’s Perceptions of the US-Australia Defense and Security Relationship Strategic Partners or Fickle Friends? Indonesia’s Perceptions of the US-Australia Defense and Security Relationship
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Clean facts on cyclones and climate change
Higher sea surface temperatures hold out the threat of more cyclones and deep depressions in the Bay of Bengal and Arabian Sea.
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Apple ships $6 billion of iPhones from India in big China shift
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Synthesis of 3,5-disubstituted isoxazoles by domino reductive Nef reaction/cyclization of β-nitroenones
Org. Biomol. Chem., 2024, Advance Article
DOI: 10.1039/D4OB00232F, Paper
DOI: 10.1039/D4OB00232F, Paper
Open Access
This article is licensed under a Creative Commons Attribution 3.0 Unported Licence.
Muhammad Ehtisham Ibraheem Khan, Tomas Lighuen Cassini, Marino Petrini, Alessandro Palmieri
β-Nitroenones were converted into 3,5-disubstituted isoxazoles via a domino reaction promoted by tin(II) dichloride. The protocol efficiently works under both microwave and flow conditions.
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β-Nitroenones were converted into 3,5-disubstituted isoxazoles via a domino reaction promoted by tin(II) dichloride. The protocol efficiently works under both microwave and flow conditions.
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Dehydrative alkynylation of 3-hydroxyisoindolinones with terminal alkynes for the synthesis of 3-alkynylated 3,3-disubstituted isoindolinones
Org. Biomol. Chem., 2024, Advance Article
DOI: 10.1039/D4OB00190G, Paper
DOI: 10.1039/D4OB00190G, Paper
Kai-Cheng Yang, Shi-Lu Zheng, Zhong Wen, Yu-Shan Zhang, Hai-Liang Ni, Long Chen
A HOTf or Fe(OTf)3-catalyzed dehydrative alkynylation of 3-hydroxyisoindolinones with terminal alkynes was developed, which represents a brand-new procedure for the synthesis of 3-alkynylated 3,3-disubstituted isoindolinones.
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A HOTf or Fe(OTf)3-catalyzed dehydrative alkynylation of 3-hydroxyisoindolinones with terminal alkynes was developed, which represents a brand-new procedure for the synthesis of 3-alkynylated 3,3-disubstituted isoindolinones.
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Diastereoselective synthesis of functionalized spiroindolines via intramolecular ipso-iodocyclization/nucleophile addition cascade reactions of indole-tethered ynones
Org. Biomol. Chem., 2024, Advance Article
DOI: 10.1039/D4OB00112E, Paper
DOI: 10.1039/D4OB00112E, Paper
Debojyoti Bag, Sanghapal D. Sawant
Herein, we describe a highly diastereoselective approach for synthesizing polyfunctionalized spiroindolines from indolyl-ynones involving an ipso-iodocyclization/nucleophile addition cascade.
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Herein, we describe a highly diastereoselective approach for synthesizing polyfunctionalized spiroindolines from indolyl-ynones involving an ipso-iodocyclization/nucleophile addition cascade.
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Copper catalyzed dehydrogenative cyclization, alkenylation towards dihydroquinolinones
Org. Biomol. Chem., 2024, Accepted Manuscript
DOI: 10.1039/D4OB00134F, Paper
DOI: 10.1039/D4OB00134F, Paper
Pari Keerthana, Fazlur-Rahman Nawaz Khan
An efficient copper-catalysized one-pot sequential synthesis of alkenylated quinolinyldihydroquinolinones is reported utilizing ketones, 1,3-cyclohexanediones, and benzyl alcohols via dehydrogenative cyclisation, followed by alkenylation. This highly straightforward method provides a mild...
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An efficient copper-catalysized one-pot sequential synthesis of alkenylated quinolinyldihydroquinolinones is reported utilizing ketones, 1,3-cyclohexanediones, and benzyl alcohols via dehydrogenative cyclisation, followed by alkenylation. This highly straightforward method provides a mild...
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Generation of sulfones utilizing β-sulfinyl esters as masked aryl sulfinates under redox-neutral conditions
Org. Biomol. Chem., 2024, Advance Article
DOI: 10.1039/D4OB00238E, Communication
DOI: 10.1039/D4OB00238E, Communication
Yixin Zhang, Zhu Yang, Hongjun Yang, Xuefeng Li, Lu Yang
A method for generation of SVI sulfones from β-sulfinyl esters (SIV) under transition-metal-free non-oxidative mild conditions is presented.
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A method for generation of SVI sulfones from β-sulfinyl esters (SIV) under transition-metal-free non-oxidative mild conditions is presented.
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A copper-catalyzed asymmetric Friedel–Crafts hydroxyalkylation of pyrazole-4,5-diones with 5-aminoisoxazoles
Org. Biomol. Chem., 2024, Advance Article
DOI: 10.1039/D4OB00322E, Communication
DOI: 10.1039/D4OB00322E, Communication
Siyu Gao, Xiang Sun, Sijie Peng, Zhenggen Zha, Qi Sun, Zhiyong Wang
An asymmetric Friede-Crafts hydroxyalkylation reaction was developed under the catalysis of chiral copper complexes. A variety of pyrazolone derivatives were obtained with excellent yields and enantioselectivities.
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An asymmetric Friede-Crafts hydroxyalkylation reaction was developed under the catalysis of chiral copper complexes. A variety of pyrazolone derivatives were obtained with excellent yields and enantioselectivities.
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Rh(III)-catalysed C-H annulation of cis-stilbene acids with 2-diazo-1,3-diketones: A facile access to 6,7-dihydrobenzofuran-4(5H)-one and α-pyrone scaffolds
Org. Biomol. Chem., 2024, Accepted Manuscript
DOI: 10.1039/D4OB00151F, Paper
DOI: 10.1039/D4OB00151F, Paper
Shankaraiah Nagula, Mary Sravani Galla, Nandini B. Kale, Akshay Kumawat, Darshana Bora
An efficient Rh(III)-catalysed C-H functionalization, tandem annulation of cis-stilbene acids using 2-diazo-1,3-diketones was devised. The protocol has solely afforded 6,7-dihydrobenzofuran-4(5H)-ones using alicyclic diazocarbonyls via decarbonylation and α-pyrones with aliphatic diazo...
The content of this RSS Feed (c) The Royal Society of Chemistry
An efficient Rh(III)-catalysed C-H functionalization, tandem annulation of cis-stilbene acids using 2-diazo-1,3-diketones was devised. The protocol has solely afforded 6,7-dihydrobenzofuran-4(5H)-ones using alicyclic diazocarbonyls via decarbonylation and α-pyrones with aliphatic diazo...
The content of this RSS Feed (c) The Royal Society of Chemistry
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Synthesis of alkenylphosphine oxides via Tf2O promoted addition–elimination of ketones and secondary phosphine oxides
Org. Biomol. Chem., 2024, Advance Article
DOI: 10.1039/D4OB00318G, Communication
DOI: 10.1039/D4OB00318G, Communication
Jiangkai Ma, Lianjie Wang, Anjiang Qiao, Zhongxian Li, Fengqian Zhao, Junliang Wu
An efficient method for the synthesis of alkenylphosphine oxides via the addition-elimination of SPOs to ketones has been developed. The reaction exhibits good yields and compatibility. Several conversions have also proven the value of this method.
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An efficient method for the synthesis of alkenylphosphine oxides via the addition-elimination of SPOs to ketones has been developed. The reaction exhibits good yields and compatibility. Several conversions have also proven the value of this method.
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Electrochemical nickel-catalyzed cross-coupling of glycosyl thiols with preactivated phenols and ketones
Org. Biomol. Chem., 2024, Advance Article
DOI: 10.1039/D4OB00442F, Communication
DOI: 10.1039/D4OB00442F, Communication
Fuxin Li, Hui Liu, Wanyu Xing, Qingju Zhang, Liming Wang
Here we report an efficient electrochemical nickel-catalyzed cross-coupling reaction for the synthesis of S-glycosides from preactivated phenols and ketones.
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Here we report an efficient electrochemical nickel-catalyzed cross-coupling reaction for the synthesis of S-glycosides from preactivated phenols and ketones.
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Stereoselective Synthesis of gem-Dihalopiperidines via Halo-Aza-Prins Cyclization Reaction: Access to Piperidin-4-ones and Pyridines
Org. Biomol. Chem., 2024, Accepted Manuscript
DOI: 10.1039/D4OB00338A, Paper
DOI: 10.1039/D4OB00338A, Paper
Anil Kumar Saikia, Surjya Kumar Bora, Subhamoy Biswas, Bipin Kumar Behera
An efficient methodology for the synthesis of 4,4-dihalopiperidine derivatives has been developed from N-(3-halobut-3-en-1-yl)-4-methylbenzenesulfonamide and aldehyde catalyzed by In(OTf)3 in excellent yields. The reaction involves an initial formation of six...
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An efficient methodology for the synthesis of 4,4-dihalopiperidine derivatives has been developed from N-(3-halobut-3-en-1-yl)-4-methylbenzenesulfonamide and aldehyde catalyzed by In(OTf)3 in excellent yields. The reaction involves an initial formation of six...
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Photogenerated chlorine radicals activate C(sp3)–H bonds of alkylbenzenes to access quinazolinones
Org. Biomol. Chem., 2024, 22,2968-2973
DOI: 10.1039/D4OB00129J, Communication
DOI: 10.1039/D4OB00129J, Communication
Xin-Yao Pan, Gui-Xia Sun, Fang-Ping Huang, Wen-Jian Qin, Qing-Hu Teng, Kai Wang
An Fe-catalyzed visible-light induced condensation of alkylbenzenes with anthranilamides has been developed.
The content of this RSS Feed (c) The Royal Society of Chemistry
An Fe-catalyzed visible-light induced condensation of alkylbenzenes with anthranilamides has been developed.
The content of this RSS Feed (c) The Royal Society of Chemistry
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Iron-catalyzed selective construction of indole derivatives via oxidative C(sp3)–H functionalization of indolin-2-ones
Org. Biomol. Chem., 2024, 22,3073-3079
DOI: 10.1039/D4OB00133H, Paper
DOI: 10.1039/D4OB00133H, Paper
Wei Chen, Lang-Qi Wen, Xiao-Bing Lu, Hui Zhou
We have developed a clean and efficient iron-catalyzed C(sp3)–H functionalization of indolin-2-ones for the chemodivergent synthesis of value-added indole derivatives, including isatins, and symmetrical and non-symmetrical isoindigos.
The content of this RSS Feed (c) The Royal Society of Chemistry
We have developed a clean and efficient iron-catalyzed C(sp3)–H functionalization of indolin-2-ones for the chemodivergent synthesis of value-added indole derivatives, including isatins, and symmetrical and non-symmetrical isoindigos.
The content of this RSS Feed (c) The Royal Society of Chemistry
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BBr3-mediated dearomative spirocyclization of biaryl ynones: facile access to spiro[5.5]dienones
Org. Biomol. Chem., 2024, Advance Article
DOI: 10.1039/D4OB00274A, Communication
DOI: 10.1039/D4OB00274A, Communication
Gaurav Jaiswal, Subhas Chandra Pan
BBr3 mediated dearomative spirocyclization of biaryl ynones has been reported for the direct synthesis of spiro[5.5]dienones with a tri-substituted double bond.
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BBr3 mediated dearomative spirocyclization of biaryl ynones has been reported for the direct synthesis of spiro[5.5]dienones with a tri-substituted double bond.
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Exploring the mechanism of the reductive amination of acetophenones via Borch approach: the role of the acid catalyst
Org. Biomol. Chem., 2024, Accepted Manuscript
DOI: 10.1039/D4OB00160E, Paper
DOI: 10.1039/D4OB00160E, Paper
João Pedro Albuquerque Souza, Amanda Krauskopf Jacobs, Leandro Piovan, Renan Borsoi Campos
The energetic viability of several mechanistic variations of the reductive amination of acetophenones via the Borch approach was reexamined through density functional theory calculations. The crucial involvement of the acid...
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The energetic viability of several mechanistic variations of the reductive amination of acetophenones via the Borch approach was reexamined through density functional theory calculations. The crucial involvement of the acid...
The content of this RSS Feed (c) The Royal Society of Chemistry
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An FeCl3-catalyzed three-component reaction for the synthesis of β-(1,2,3-triazolyl)-ketones using DMF as a one-carbon source
Org. Biomol. Chem., 2024, Advance Article
DOI: 10.1039/D4OB00207E, Communication
DOI: 10.1039/D4OB00207E, Communication
Ruilin Fang, Lei Zheng, Xuyang Chen, Can Wang, Yunfeng Chen
FeCl3-catalyzed oxidative condensation of NH-1,2,3-triazoles and aryl methyl ketones and DMF has been reported.
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FeCl3-catalyzed oxidative condensation of NH-1,2,3-triazoles and aryl methyl ketones and DMF has been reported.
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Regioselective synthesis of 4-arylamino-1,2-naphthoquinones in eutectogel as a confined reaction medium using LED light
Org. Biomol. Chem., 2024, Advance Article
DOI: 10.1039/D4OB00140K, Communication
DOI: 10.1039/D4OB00140K, Communication
R. Vara Prasad, Yogendra Kumar, R. Arun Kumar, Tohira Banoo, Subbiah Nagarajan
The use of a simple carbohydrate-derived eutectogel facilitating a LED-light-induced regioselective synthesis of 4-arylamino-1,2-naphthoquinones in good yields is reported.
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The use of a simple carbohydrate-derived eutectogel facilitating a LED-light-induced regioselective synthesis of 4-arylamino-1,2-naphthoquinones in good yields is reported.
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Efficient synthesis of SCF3-containing 3-alkenylquinoxalinones via three-component radical cascade reaction
Org. Biomol. Chem., 2024, Advance Article
DOI: 10.1039/D4OB00363B, Paper
DOI: 10.1039/D4OB00363B, Paper
Si-Yu Wang, Chu Liu, Wei Yang, Zhong-Ying Tian, Lin Yuan, Long-Yong Xie
A three-component cascade reaction of quinoxalinones, alkynes and AgSCF3 toward complete E-selective SCF3-containing 3-alkenylquinoxalinones was developed.
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A three-component cascade reaction of quinoxalinones, alkynes and AgSCF3 toward complete E-selective SCF3-containing 3-alkenylquinoxalinones was developed.
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Base- and sulfur-promoted oxidative lactonization of chalcone-acetate Michael adducts: access to pyran-2-ones
Org. Biomol. Chem., 2024, Advance Article
DOI: 10.1039/D4OB00479E, Communication
DOI: 10.1039/D4OB00479E, Communication
Cao Nguyen Nguyen, Duc Toan Nguyen, Ha An Tran, Dinh Hung Mac, Thi Thu Tram Nguyen, Pascal Retailleau, Thanh Binh Nguyen
A cost-effective, practical, straightforward and scalable synthesis of α-pyrones via base- and sulfur-promoted annulation of phenylacetates and chalcones is reported.
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A cost-effective, practical, straightforward and scalable synthesis of α-pyrones via base- and sulfur-promoted annulation of phenylacetates and chalcones is reported.
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Indonesia bans sales of Google phones days after blocking Apple's iPhone 16
Indonesia said it has banned sales of smartphones made by Alphabet's Google due to rules requiring the use of locally manufactured components
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Osteoporosis can shorten your life − here’s how to prevent fractures and keep bones healthy
The key to having healthy bones for a lifetime is to take some simple preventive measures – and the earlier, the better
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The five best ones
Bringing you the top five watches at the 2018 version of Salon International de la Haute Horlogerie
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The phones that light up your instagram
Camera phones that will help you take your Instagram game up a notch this festival season
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The real Charlotte / E. Œ. Somerville & Martin Ross ; afterword by Malcolm Jones.
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The war lawyers : the United States, Israel, and juridical warfare / Craig Jones.
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The medieval clergy, 800-1250 : a sourcebook / John S. Ott and Anna Trumbore Jones.
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Critique du De mundo de Thomas White / Thomas Hobbes ; introduction, texte critique et notes par Jean Jacquot et Harold Whitmore Jones.
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Biologist Explains How Drones Catching Whale "Snot" Helps Research
Whale research is difficult, but a conservation organization is trying to make it a bit easier with drones. WIRED's Matt Simon talks with Ocean Alliance CEO Iain Kerr about the benefits of flying the "SnotBot" into a whale's blow spout.
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What If... Time zones didn't exist? | What If
Daylight saving time means we change the clocks twice a year, and the world has over 30 different time zones. Some countries span multiple different time zones, while the likes of China and India choose to have just one time zone despite the huge differences in real time from east to west. Time influences almost every aspect of our lives – yet we barely ever stop to think about what time means exactly. Studies show the Daylight Savings Time leads to spikes in heart attacks and traffic accidents, while reduced sleep due changing times is linked to increased levels of obesity. So, why do we even bother? That's the argument of some scientists, who believe the whole world should switch to Coordinated Universal Time (UTC), which is already used in aviation and in space. In this video we ask, what if we abolished time zones (and clock changes) forever? This video was produced as part of Digital Society, a publishing partnership between WIRED and Vontobel where all content is editorially independent. Visit Vontobel Impact for more stories on how technology is shaping the future of society: https://www.vontobel.com/en-int/about-vontobel/impact/
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WIRED25 2020: Brie Larson, Van Jones, and Elijah Allan-Blitz on VR and Empathy
Brie Larson, Van Jones, and Elijah Allan-Blitz joined the WIRED25 event to discuss what divides us, and their approach with VR films to bridge those gaps.
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The Drop In with Guy Raz | Tilane Jones on Flipping the Script
Produced by WIRED Brand Lab with Dropbox | How do you not only sustain, but grow your business during the pandemic? Guy Raz and Tilane Jones, president of the distribution company ARRAY, discuss the future of work and staying flexible to meet the needs of consumers.