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[ASAP] Au/Pb Interface Allows the Methane Formation Pathway in Carbon Dioxide Electroreduction

ACS Catalysis
DOI: 10.1021/acscatal.0c00749




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[ASAP] Role of Water on the Structure of Palladium for Complete Oxidation of Methane

ACS Catalysis
DOI: 10.1021/acscatal.0c01069




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[ASAP] Methanol Synthesis from CO<sub>2</sub> Hydrogenation over a Potassium-Promoted Cu<italic toggle="yes"><sub>x</sub></italic>O/Cu(111) (<italic toggle="yes">x</italic> = 2) Model Sur

ACS Catalysis
DOI: 10.1021/acscatal.9b05226




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[ASAP] Alkene Isomerization through Allylmetals as a Strategic Tool in Stereoselective Synthesis

ACS Catalysis
DOI: 10.1021/acscatal.0c01174




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[ASAP] Spectroscopic Signatures Reveal Cyclopentenyl Cation Contributions in Methanol-to-Olefins Catalysis

ACS Catalysis
DOI: 10.1021/acscatal.0c00721




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[ASAP] Asymmetric Allylic Alkylation of ß-Ketoesters via C–N Bond Cleavage of <italic toggle="yes">N</italic>-Allyl-<italic toggle="yes">N</italic>-methylaniline Derivatives Catalyzed by a Nickel–Diphosphin

ACS Catalysis
DOI: 10.1021/acscatal.0c01356




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[ASAP] Pd/Cu-Catalyzed Dehydrogenative Coupling of Dimethyl Phthalate: Synchrotron Radiation Sheds Light on the Cu Cycle Mechanism

ACS Catalysis
DOI: 10.1021/acscatal.0c00918




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[ASAP] Development of Ketone-Based Brominating Agents (KBA) for the Practical Asymmetric a-Bromination of Aldehydes Catalyzed by Tritylpyrrolidine

ACS Catalysis
DOI: 10.1021/acscatal.0c01596




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Metropolis: Roman / Thea von Harbou ; [mit einem Nachwort von Franz Rottensteiner]

Hayden Library - PT2615.A62 M4 2014




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The metamorphosis: a new translation, texts and contexts, criticism / Franz Kafka ; translated by Susan Bernofsky, Columbia University ; edited by Mark M. Anderson, Columbia University

Hayden Library - PT2621.A26 V413 2016




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Goethe and the poets of Arabia / Katharina Mommsen ; translated by Michael M. Metzger

Hayden Library - PT2190.A3 M65 2014




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Metropolis / Thea Von Harbou

Hayden Library - PT2615.A62 M413 2015




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How comets change seasonally and a news roundup

Myrtha Hässig discusses variability and heterogeneity of the coma of comet 67P as part of Science's special issue on the Rosetta spacecraft. Meghna Sachdev discusses daily news stories. Hosted by Susanne Bard. [Img: European Space Agency/Rosetta/NAVCAM]




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Metallic hydrogen and a daily news roundup.

Marcus Knudson discusses making metallic hydrogen and how it can better our understanding of gas giant planets and David Grimm brings online news stories about kid justice, part-time dieting, and bird brains. Hosted by Sarah Crespi. [Img: NASA/ESA]




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Comet chemistry and a news roundup

Fred Goesmann discusses Philae's bumpy landing on Comet 67P, and the organic compounds it detected there, and Hanae Armitage talks with Sarah Crespi about this week’s online news stories. Hosted by Susanne Bard. [Img: NAVCAM/ESA/Rosetta]




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Podcast: When good lions go bad, listening to meteor crashes, and how humans learn to change the world

This week, meteors’ hiss may come from radio waves, pigeons that build on the wings of those that came before, and a potential answer to the century-old mystery of what turned two lions into people eaters with Online News Editor David Grimm. Elise Amel joins Julia Rosen to discuss the role of evolution and psychology in humans’ ability to overcome norms and change the world, as part of a special issue on conservation this week in Science. Listen to previous podcasts. Download the show transcript  Transcripts courtesy Scribie.com  [Image: bjdlzx/iStockphoto; Music: Jeffrey Cook]




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Metaresearchers take on meta-analyses, and hoary old myths about science

Meta-analyses—structured analyses of many studies on the same topic—were once seen as objective and definitive projects that helped sort out conflicts amongst smaller studies. These days, thousands of meta-analyses are published every year—many either redundant or contrary to earlier metaworks. Host Sarah Crespi talks to freelance science journalist Jop de Vrieze about ongoing meta-analysis wars in which opposing research teams churn out conflicting metastudies around important public health questions such as links between violent video games and school shootings and the effects of antidepressants. They also talk about what clues to look for when trying to evaluate the quality of a meta-analysis. Sarah also talked with three other contributors to our “Research on Research” special issue. Pierre Azoulay of the Massachusetts Institute of Technology (MIT) in Cambridge, Ben Jones of Northwestern University in Evanston, Illinois, and MIT’s Heidi Williams discuss the evidence for some hoary old scientific home truths. See whether you can guess who originally made these claims and how right or wrong they were: Do scientists make great contributions after age 30? How important is it to stand on the shoulders of giants? Does the truth win, or do its opponents just eventually die out? Read the rest of the package on science under scrutiny here. This week’s episode was edited by Podigy. Download a transcript of this episode (PDF) Listen to previous podcasts. About the Science Podcast [Image: Davide Bonazzi/@SalzmanArt; Show music: Jeffrey Cook; additional music: Nguyen Khoi Nguyen]




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A big increase in monkey research and an overhaul for the metric system

A new report suggests a big increase in the use of monkeys in laboratory experiments in the United States in 2017. Online News Editor David Grimm joins host Sarah Crespi to discuss which areas of research are experiencing this rise and the possible reasons behind it. Also this week, host Meagan Cantwell talks with staff writer Adrian Cho about a final push to affix the metric system’s measures to physical constants instead of physical objects. That means the perfectly formed 1-kilogram cylinder known as Le Grand K is no more; it also means that the meter, the ampere, and other units of measure are now derived using complex calculations and experiments.  This week’s episode was edited by Podigy. Download a transcript (PDF) Listen to previous podcasts. About the Science Podcast [Image: Peter Nijenhuis/Flickr; Music: Jeffrey Cook] 




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Vacuuming potato-size nodules of valuable metals in the deep sea, and an expedition to an asteroid 290 million kilometers away

Pirate’s gold may not be that far off, as there are valuable metals embedded in potato-size nodules thousands of meters down in the depths of the ocean. Host Meagan Cantwell talks with Staff Writer Paul Voosen about the first deep-sea test of a bus-size machine designed to scoop up these nodules, and its potential impact on the surrounding ecosystem. In an expedition well above sea level, the Hayabusa2 spacecraft touched down on the asteroid Ryugu last month. And although the craft won’t return to Earth until 2020, researchers have learned a lot about Ryugu in the meantime. Meagan speaks with Seiji Sugita, a professor at the University of Tokyo and principal investigator of the Optical Navigation Camera of Hayabusa 2, about Ryugu’s parent body, and how this study can better inform future asteroid missions. This week’s episode was edited by Podigy. Download transcript (PDF) Listen to previous podcasts. About the Science Podcast [Image: Japan Aerospace Exploration Agency; Music: Jeffrey Cook]




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Studying human health at 5100 meters, and playing hide and seek with rats

In La Rinconada, Peru, a town 5100 meters up in the Peruvian Andes, residents get by breathing air with 50% less oxygen than at sea level. International News Editor Martin Enserink visited the site with researchers studying chronic mountain sickness—when the body makes excess red blood cells in an effort to cope with oxygen deprivation—in these extreme conditions. Martin talks with host Sarah Crespi about how understanding why this illness occurs in some people and not others could help the residents of La Rinconada and the 140 million people worldwide living above 2500 meters. Read the whole special issue on mountains.  Sarah also talks with Annika Stefanie Reinhold about her work at the Bernstein Center for Computational Neuroscience in Berlin training rats to play hide and seek. Surprisingly, rats learned the game easily and were even able to switch roles—sometimes playing as the seeker, other times the hider. Annika talks with Sarah about why studying play behavior in animals is important for understanding the connections between play and learning in both rats and humans. This week’s episode was edited by Podigy. Ads on this week’s show: MOVA Globes; Kroger’s Zero Hunger, Zero Waste campaign Download a transcript (PDF)  Listen to previous podcasts. About the Science Podcast [Image: Tambako The Jaguar/Flickr; Music: Jeffrey Cook]




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Surface Modification of Polymers: Methods and Applications


 
A guide to modifying and functionalizing the surfaces of polymers

Surface Modification of Polymers is an essential guide to the myriad methods that can be employed to modify and functionalize the surfaces of polymers. The functionalization of polymer surfaces is often required for applications in sensors, membranes, medicinal devices, and others. The contributors?noted experts on the topic?describe the polymer surface in detail and discuss the internal

Read More...




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The development and validation of a GC-MS method for the quantification of glycolaldehyde formed from carbohydrate fragmentation processes

Anal. Methods, 2020, 12,1975-1987
DOI: 10.1039/C9AY02639H, Paper
Samin Fathalinejad, Esben Taarning, Peter Christensen, Jan H. Christensen
Glycolaldehyde is a small sugar-like molecule that is readily formed by the thermochemical fragmentation of carbohydrates and it has similar physico-chemical properties to sugars.
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A bimetallic PtPd hybrid nanostructure-amplified enzyme-free conductometric immunoassay for lipocalin-2 in renal cell carcinoma on an interdigitated micro-comb electrode

Anal. Methods, 2020, 12,1988-1994
DOI: 10.1039/C9AY02525A, Paper
Chaoqun Huang, Fengling Zhang, Qingshui Wang, Yao Lin, Jiyi Huang
A new enzyme-free conductometric immunoassay based on bimetallic PtPd hybrid nanostructures was developed for the sensitive determination of lipocalin-2 in renal cell carcinoma.
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3D-printed microfluidic device with in-line amperometric detection that also enables multi-modal detection

Anal. Methods, 2020, 12,2046-2051
DOI: 10.1039/D0AY00368A, Technical Note
Elizabeth A. Hayter, Andre D. Castiaux, R. Scott Martin
A 3D-printed microfluidic device with amperometric detection employs a parallel-opposed electrode configuration, with threaded electrodes being in contact with the flow stream. This makes downstream detection of ATP via chemiluminescence possible.
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NMR-based plasma metabonomics in hyperlipidemia mice

Anal. Methods, 2020, 12,1995-2001
DOI: 10.1039/D0AY00487A, Paper
Yun Li, Xiu-ju Zhao
Hyperlipidemia dynamics need to be elucidated.
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Liquid–liquid microextraction of glyphosate, glufosinate and aminomethylphosphonic acid for the analysis of agricultural samples by liquid chromatography

Anal. Methods, 2020, 12,2039-2045
DOI: 10.1039/D0AY00120A, Paper
Javier Marín, Natalia Campillo, Manuel Hernández-Córdoba, Isabel Garrido, José Fenoll, Pilar Viñas
An ion-pair liquid–liquid microextraction procedure followed by LC tandem mass spectrometry allows a reliable and sensitive determination glyphosate, glufosinate y aminomethylphosphonic acid in agricultural samples.
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Bio-assay of non-amidated progastrin-derived peptide (G17-Gly) using Tailor-made recombinant antibody fragment and phages display method: A biomedical analysis

Anal. Methods, 2020, Accepted Manuscript
DOI: 10.1039/D0AY00627K, Paper
Deniz Sadighbayan, Mohammad Reza Tohid-kia, Tayebeh Mehdipour, Mohammad Hasanzadeh, Ahmad Yari Khosroushahi
In this research, four novel and sensitive immunosensor for electrochemical determination of G17-Gly were designed based on signal amplification and tailor-made recombinant antibody technology. Anti-G17-Glyantibody fragments (i.e. scFv and VL...
The content of this RSS Feed (c) The Royal Society of Chemistry




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Methodology for elemental analysis of mineral fertilizer, some of its raw materials and limestone using microwave-induced plasma optical emission spectrometry (MIP OES)

Anal. Methods, 2020, Accepted Manuscript
DOI: 10.1039/D0AY00459F, Paper
Dirce Pozebon, Alexandre Müller, Anderson Schwingel Ribeiro
Elemental analysis of complex matrices such as superphosphate-fertilizer and agricultural inputs by means of microwave induced plasma optical emission has been evaluated in the present study. A commercial single superphosphate-fertilizer...
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Recent advance in the analysis methodologies for microplastics in aquatic organisms: Current knowledge and research challenges

Anal. Methods, 2020, Accepted Manuscript
DOI: 10.1039/D0AY00143K, Minireview
Jingkun Zhu, Can Wang
The widespread occurrence and high bioavailability of microplastics have increasingly attracted wide attention to society. Because of the presence of microplastics in aquatic organisms, it is necessary to investigate their...
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A simple and rapid method for blood plasma separation driven by capillary force with an application on protein detection

Anal. Methods, 2020, Accepted Manuscript
DOI: 10.1039/D0AY00240B, Paper
Qingxue Gao, Yongjia Chang, Qingmei Deng, Hui You
Blood plasma separation is a vital sample pre-treatment procedure for microfluidic devices of blood diagnostic, which requires reliability and speediness. In this work, we propose a novel and simple method...
The content of this RSS Feed (c) The Royal Society of Chemistry




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Effective methods for the determination of triphenyltin residues in surface water and soil samples by high-performance liquid chromatography with tandem mass spectrometry

Anal. Methods, 2020, Advance Article
DOI: 10.1039/D0AY00329H, Paper
Gabriel C. dos Santos, Állisson A. da S. Avellar, Rômulo de O. Schwaickhardt, Nelson M. G. Bandeira, Filipe F. Donato, Osmar D. Prestes, Renato Zanella
Monitoring of triphenyltin (TPhT) in the environment, particularly to control its misuse in agriculture, is of great importance because of its high toxicity.
To cite this article before page numbers are assigned, use the DOI form of citation above.
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Development of a magnetic dispersive micro-solid-phase extraction method based on a deep eutectic solvent as a carrier for the rapid determination of meloxicam in biological samples

Anal. Methods, 2020, Advance Article
DOI: 10.1039/D0AY00095G, Paper
Samira Rastbood, Mohammad Reza Hadjmohammadi, Seyedeh Maedeh Majidi
An environmentally friendly magnetic dispersive micro solid phase extraction based on a deep eutectic solvent as a carrier and disperser of adsorbents.
To cite this article before page numbers are assigned, use the DOI form of citation above.
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Dopamine-modified magnetic graphene oxide as a recoverable sorbent for the preconcentration of metal ions by an effervescence-assisted dispersive micro solid-phase extraction procedure

Anal. Methods, 2020, Advance Article
DOI: 10.1039/D0AY00522C, Paper
Basira Karbalaie, Maryam Rajabi, Bahareh Fahimirad
Nanomagnetic graphene oxide modified with dopamine (GO–Fe3O4–DA) was synthesized via a very simple procedure.
To cite this article before page numbers are assigned, use the DOI form of citation above.
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Shenling Baizhu San improves functional dyspepsia in rats as revealed by 1H-NMR based metabolomics

Anal. Methods, 2020, Advance Article
DOI: 10.1039/D0AY00580K, Paper
Shaobao Zhang, Zengmei Xu, Xueqing Cao, Yuzhen Xie, Lei Lin, Xiao Zhang, Baorong Zou, Deliang Liu, Ying Cai, Qiongfeng Liao, Zhiyong Xie
Functional dyspepsia (FD), a common gastrointestinal disorder around the world, is driven by multiple factors, making prevention and treatment a major challenge.
To cite this article before page numbers are assigned, use the DOI form of citation above.
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Targeted profiling of amino acid metabolome in serum by a liquid chromatography-mass spectrometry method: application to identify potential markers for diet-induced hyperlipidemia

Anal. Methods, 2020, Advance Article
DOI: 10.1039/D0AY00305K, Paper
Xiao-fan Wang, You-xi Zhang, Hai-ying Ma
Targeted profiling of amino acid metabolome in serum by LC-MS: application to identify potential markers for diet-induced hyperlipidemia.
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Multivariate optimization of an analytical method for the analysis of Abruzzo white wines by ICP OES

Anal. Methods, 2020, Accepted Manuscript
DOI: 10.1039/D0AY00478B, Paper
Fabrizio Ruggieri, Angelo Antonio D'Archivio, Martina Foschi, Maria Anna Maggi
An inductively coupled plasma-optical emission spectrometry (ICP OES) method was optimized and applied for determining the concentration of 14 elements (Ba, Ca, Co, Cu, Fe, K, Li, Mg, Mn, Na,...
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Versatile additively manufactured (3D printed) wall-jet flow cell for high performance liquid chromatography-amperometric analysis: application to the detection and quantification of new psychoactive substances (NBOMes)

Anal. Methods, 2020, 12,2152-2165
DOI: 10.1039/D0AY00500B, Paper
Open Access
Hadil M. Elbardisy, Eduardo M. Richter, Robert D. Crapnell, Michael P. Down, Peter G. Gough, Tarek S. Belal, Wael Talaat, Hoda G. Daabees, Craig E. Banks
Additive manufacturing is an emerging technology of vast applicability, receiving significant interest in a plethora of industrial and research domains as it allows the translation of designs produced via computer software, into 3D printed objects.
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Quality by Design (QbD) approach for the development of a rapid UHPLC method for simultaneous determination of aglycone and glycoside forms of isoflavones in dietary supplements

Anal. Methods, 2020, 12,2082-2092
DOI: 10.1039/C9AY02778E, Paper
Kornelija Lasić, Ana Mornar, Biljana Nigović
Systematic development of a UHPLC method by QbD approach as performed for simultaneous determination of aglycone (genistein, daidzein, biochanin A and formononetin) and glycoside (genistin, daidzin, sissotrin, ononin) forms of isoflavones.
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A sensitive HPLC-FL method to simultaneously determine febuxostat and diclofenac in rat plasma: assessment of metabolic drug interactions in vitro and in vivo

Anal. Methods, 2020, 12,2166-2175
DOI: 10.1039/D0AY00471E, Paper
Dong-Gyun Han, Kyu-Sang Kim, Seong-Wook Seo, Young Mee Baek, Yunjin Jung, Dae-Duk Kim, In-Soo Yoon
We developed a sensitive, simple and validated HPLC-FL method for simultaneous determination of FEB and DIC in rat plasma. The method requires a relatively small volume of sample, has simple sample preparation and excellent sensitivity.
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Multi-residue determination of micropollutants in Nigerian fish from Lagos lagoon using ultrasound assisted extraction, solid phase extraction and ultra-high-performance liquid chromatography tandem mass spectrometry

Anal. Methods, 2020, 12,2114-2122
DOI: 10.1039/D0AY00411A, Paper
Idera Fabunmi, Natalie Sims, Kathryn Proctor, Aderonke Oyeyiola, Temilola Oluseyi, Kehinde Olayinka, Barbara Kasprzyk-Hordern
This reports for the first time a simple and robust approach in determining pharmaceuticals in different fish species in Nigeria.
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Aptamer-based fluorometric determination of chloramphenicol by controlling the activity of hemin as a peroxidase mimetic

Anal. Methods, 2020, Advance Article
DOI: 10.1039/D0AY00389A, Paper
Ling-Chen Wang, Cheng-Yi Hong, Zheng-Zhong Lin, Xiao-Mei Chen, Zhi-Yong Huang
A method for the aptamer-based determination of chloramphenicol (CAP) was developed by exploiting the peroxidase mimicking activity of hemin.
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Electrochemical determination of paracetamol in a pharmaceutical dose by adsorptive voltammetry with a carbon paste/La2O3 microcomposite

Anal. Methods, 2020, Accepted Manuscript
DOI: 10.1039/D0AY00442A, Paper
Edgar Nagles, Mario Ceroni, John Hurtado-Murillo, John Hurtado Belalcazar
This paper presents a new application for microcomposites based on carbon paste (CP) and La2O3 (LaOX). This simple and versatile microcomposite (LaOX/CPE) was applied toward the determination of paracetamol (PCM)...
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Colorimetric speciation analysis of chromium using 2-thiobarbituric acid capped silver nanoparticles

Anal. Methods, 2020, Advance Article
DOI: 10.1039/D0AY00160K, Paper
Kamal Mousapour, Salahaddin Hajizadeh, Khalil Farhadi
Colorimetric determination of Cr(III) and Cr(VI) based on 2-thiobarbituric acid capped silver nanoparticles.
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Portable and benchtop Raman spectrometers coupled to cluster analysis to identify quinine sulfate polymorphs in solid dosage forms and antimalarial drug quantification in solution by AuNPs-SERS with MCR-ALS

Anal. Methods, 2020, Advance Article
DOI: 10.1039/D0AY00693A, Paper
Sarmento J. Mazivila, Helena I. S. Nogueira, Ricardo N. M. J. Páscoa, David S. M. Ribeiro, João L. M. Santos, João M. M. Leitão, Joaquim C. G. Esteves da Silva
Raman spectrometers coupled to cluster analysis were able to identify two polymorphs of quinine sulfate in solid dosage forms. Gold nanoparticles-surface-enhanced Raman scattering with MCR-ALS was used to antimalarial drug quantification in solution.
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Quantification of Anthracene after dermal absorption test via APCI-Tandem Mass Spectrometry

Anal. Methods, 2020, Accepted Manuscript
DOI: 10.1039/D0AY00486C, Paper
Xinyi Sui, Julio E Teran, Chengcheng Feng, Killian Wustrow, Caroline J. Smith , Nelson R Vinueza
An analytical method for the detection and quantification of anthracene from dermal samples was developed by using Atmospheric Pressure Chemical Ionization-Tandem Mass Spectrometry (APCI-MS/MS). The anthracene samples were obtained from...
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Effects of harvesting and extraction methods on metabolite recovery from adherently growing mammalian cells

Anal. Methods, 2020, Advance Article
DOI: 10.1039/C9AY02753J, Paper
Yun Luo, Ningbo Geng, Baoqin Zhang, Jiping Chen, Haijun Zhang
We compare the efficiencies of different cell harvesting methods and metabolite extraction methods in sample preparation procedures and provide a cell sample processing protocol which focuses on maximizing metabolite recovery ranging from polar to lipidic ones.
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Multivariate optimization of an ultrasound-assisted extraction procedure for the determination of Cu, Fe, Mn, and Zn in plant samples by flame atomic absorption spectrometry

Anal. Methods, 2020, Advance Article
DOI: 10.1039/D0AY00554A, Paper
Floriatan Santos Costa, Raquel Viana Pinto Leal, Clissiane Soares Viana Pacheco, Fábio Alan Carqueija Amorim, Raildo Mota de Jesus, Luana Novaes Santos, Erik Galvão Paranhos da Silva
A new ultrasound-assisted extraction method simple and fast was developed employing multivariate optimization.
To cite this article before page numbers are assigned, use the DOI form of citation above.
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Colorimetric indicators for volatile amines based on succinic anhydride (SAh)-grafted poly (lactic acid) (PLA)

Anal. Methods, 2020, Advance Article
DOI: 10.1039/D0AY00550A, Paper
Adrian Lopera-Valle, Anastasia Elias
Smart materials that can undergo changes in color upon the detection of amines have the potential to provide information on the freshness of fish and meat.
To cite this article before page numbers are assigned, use the DOI form of citation above.
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Miniaturized QuEChERS method for determination of 97 pesticide residues in wine by ultra-high performance liquid chromatography coupled to tandem mass spectrometry

Anal. Methods, 2020, Accepted Manuscript
DOI: 10.1039/D0AY00744G, Paper
Gabrieli Bernardi, Magali Kemmerich, Martha B Adaime, Osmar Damian Prestes, Renato Zanella
A miniaturized sample preparation method was developed and validated for the multiresidue determination of 97 pesticide residues in wine samples. The proposed extraction procedure is based on QuEChERS acetate method...
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A rapid and colorimetric biosensor based on GR-5 DNAzyme and self-replicating catalyzed hairpin assembly for lead detection

Anal. Methods, 2020, 12,2215-2220
DOI: 10.1039/D0AY00091D, Paper
Fang Wang, Jianyuan Dai, Hongli Shi, Xiaoqian Luo, Lan Xiao, Cuisong Zhou, Yong Guo, Dan Xiao
A rapid and colorimetric biosensor for Pb2+ detection has been constructed on the basis of Pb2+-dependent GR-5 DNAzyme and the self-replicating catalyzed hairpin assembly (SRCHA) reaction.
The content of this RSS Feed (c) The Royal Society of Chemistry