ac ***WITHDRAWN PATENT AS PER THE LATEST USPTO WITHDRAWN LIST***Method for producing aqueous acrylamide solution By www.freepatentsonline.com Published On :: Tue, 12 May 2015 08:00:00 EDT There is provided a method for producing an aqueous acrylamide solution by reacting a composition including acrylonitrile with water to produce acrylamide, in which the composition including acrylonitrile includes 3 to 15 mg of propionitrile per 1 kg of the total weight of the composition including acrylonitrile. According to the present invention, a production method with which it is possible to suppress acrylamide polymerization without lowering quality and thereby obtain a stable aqueous acrylamide solution can be provided. Full Article
ac Halo active aromatic sulfonamide organic compounds and uses therefor By www.freepatentsonline.com Published On :: Tue, 26 May 2015 08:00:00 EDT Aromatic N-halosulfonamide organic compounds have been known for over one hundred years. The ability of these compounds to release active halogen ions has been utilized in a range of biocidal and fungicidal applications. This disclosure deals with the use of halo active aromatic sulfonamide organic compounds as odor control and/or biocidal agents in a cleaning solution for use with bovines and other dairy animals. Full Article
ac Method for producing aqueous acrylamide solution By www.freepatentsonline.com Published On :: Tue, 16 Jun 2015 08:00:00 EDT There is provided a method for producing an aqueous acrylamide solution by reacting a composition including acrylonitrile with water to produce acrylamide, in which the composition including acrylonitrile includes 3 to 15 mg of propionitrile per 1 kg of the total weight of the composition including acrylonitrile. According to the present invention, a production method with which it is possible to suppress acrylamide polymerization without lowering quality and thereby obtain a stable aqueous acrylamide solution can be provided. Full Article
ac Managed access to media services By www.freepatentsonline.com Published On :: Tue, 26 May 2015 08:00:00 EDT Methods, apparatuses and systems directed to account-based access to media services are described. A media access controller server validates a voucher for an offer of network content and issues a token permitting access to the content. A media access manager server validates the token and invokes a playlist-generation step at a publishing point, and returns the content to a user's media player. A custom plug-in on the media access manager may enforce terms of service imposed by the publisher, such as a maximum number of simultaneous streams permitted by a single voucher, or a time window for use of the voucher. Streams whose voucher's end time has expired are terminated by the plug-in. Full Article
ac Streaming playback and dynamic ad insertion By www.freepatentsonline.com Published On :: Tue, 26 May 2015 08:00:00 EDT There is provided a system and method for dynamically generated client side streaming playlists. There is provided a method comprising receiving a request to stream a video asset for playback, retrieving, from a network, a video asset playlist corresponding to the video asset and an ad campaign playlist, generating a consolidated video playlist including the video asset playlist and the ad campaign playlist, and processing the consolidated video playlist using a media playback framework to stream a plurality of video files from the network for decoding and output to a display. Discontinuity tags within the video asset playlist may be utilized as insertion points for portions of the ad campaign playlist. The consolidated video playlist may be accessed through a local HTTP web server, advantageously allowing the use of commonly installed media playback framework models such as QuickTime X to trigger adaptive bitrate support through HTTP Live Streaming. Full Article
ac Interfaces for digital media processing By www.freepatentsonline.com Published On :: Tue, 26 May 2015 08:00:00 EDT APIs discussed herein promote efficient and timely interoperability between hardware and software components within the media processing pipelines of media content players. A PhysMemDataStructure API facilitates a hardware component's direct access to information within a memory used by a software component, to enable the hardware component to use direct memory access techniques to obtain the contents of the memory, instead of using processor cycles to execute copy commands. The PhysMemDataStructure API exposes one or more fields of data structures associated with units of media content stored in a memory used by a software component, and the exposed fields store information about the physical properties of the memory locations of the units of media content. SyncHelper APIs are used for obtaining information from, and passing information to, hardware components, which information is used to adjust the hardware components' timing for preparing media samples of synchronously-presentable media content streams. Full Article
ac Facilitating context delivery during communication sessions By www.freepatentsonline.com Published On :: Tue, 07 Jul 2015 08:00:00 EDT An approach is disclosed that facilitates context delivery during communication sessions. The approach may be implemented in a computer infrastructure having computer executable code tangibly embodied on a computer readable storage medium having programming instructions operable to: render at least one service to a user device through a communication session; collect information of the communication session; and send the information of the communication session to a service provider when a call is setup between the user device and the service provider. The service provider renders the information of the communication session for viewing by the service provider. Full Article
ac Application programming interface, system, and method for collaborative online applications By www.freepatentsonline.com Published On :: Tue, 08 Sep 2015 08:00:00 EDT An application framework including different application programming interfaces (APIs) is described which performs a variety of mobile device functions in response to API calls from applications. For example, in response to relatively simple API calls made by applications the application framework manages the complex tasks associated with invitations and matchmaking. By way of example, the details of complex transactions such as establishing peer-to-peer connections between mobile devices may be transparent to the application developer, thereby simplifying the application design process. The application framework may include an application daemon for communicating with a first set of services and an applications services module for communicating with a separate set of services. The application framework may also include a cache for caching data for each of the services based on different cache management policies driven by each of the services. The cache may be updated by push notification cache updates sent from each of the services. Full Article
ac Trivial file transfer protocol (TFTP) accelerated file retry option By www.freepatentsonline.com Published On :: Tue, 22 Sep 2015 08:00:00 EDT A method of transferring data using a Trivial File Transport Protocol (TFTP) includes sending first request packet from client to server, first request packet requesting that first file be transferred; transferring first file according to first request packet if first acknowledgement packet is received at client from server indicating that server can accommodate request of first request packet; sending second request packet from client to the server if transfer of first file does not complete successfully, the second request packet including TFTP option indicating that transfer of first file be retried beginning at first block after final block that was successfully transferred in response to first request packet; and retrying transfer of first file according to second request packet if second acknowledgement packet is received at client from server indicating that server can accommodate request of second request packet. Full Article
ac System and method for supporting video processing load balancing for user account management in a computing environment By www.freepatentsonline.com Published On :: Tue, 29 Sep 2015 08:00:00 EDT A system and method can support user account management in a computing environment. The computing environment can include a video encoding pool to support load balancing and a managing server, such as a privileged account manager server. The video encoding pool includes a set of nodes that are able to perform one or more video processing tasks for another node. Furthermore, the managing server can receive a request from a managed node in the computing environment for delegating a video processing task, and can select one or more nodes from the video encoding pool to load babalance and to perform the video processing task. Full Article
ac Software-based aliasing for accessing multiple shared resources on a single remote host By www.freepatentsonline.com Published On :: Tue, 22 Dec 2015 08:00:00 EST In order to allow a single user registered on a single local host or other machine to access multiple shared resources on a remote host, an aliasing mechanism is employed so that multiple concurrent connections can be established by the user to a single remote host, with each connection using a different identity. Each connection can therefore be used to access a different shared resource on the remote host. In some illustrative examples, a user's identifier such as his or her machine log-in identification may be associated with two or more resource sharing aliases. As a result, two or more resource sharing sessions can be established by the user with a single remote host, with each of the sessions using a different one of the aliases. The resource sharing sessions are usually established in accordance with a resource sharing protocol such as the Server Block Message (SBM) protocol. Full Article
ac Device and method for providing accurate time and/or frequency By www.freepatentsonline.com Published On :: Tue, 28 Dec 1993 08:00:00 EST A device and method provide for an accurate output from a unit, such as an oscillator and/or clock providing an output indicative of frequency and/or time. The device includes a processing section having a microprocessor that develops a model characterizing the performance of the device, including establishing predicted accuracy variations, and the model is then used to correct the unit output. An external reference is used to provide a reference input for updating the model, including updating of predicted variations of the unit, by comparison of the reference input with the unit output. The ability of the model to accurately predict the performance of the unit improves as additional updates are carried out, and this allows the interval between the updates to be lengthened and/or the overall accuracy of the device to be improved. The accuracy of the output is thus adaptively optimized in the presence of systematic and random variations. Full Article
ac Watch case back opener By www.freepatentsonline.com Published On :: Tue, 07 Feb 1995 08:00:00 EST A watch case back opener is provided having a base. A vise is rotatably mounted on the base for securing a watch case to the base. The vise includes a first jaw and a second jaw movable between an open and closed position. Holes are formed in the jaw. They are adapted to receive a plurality of posts to secure a plurality of different sized and shaped watch cases to the vise. An opener unit including an opening blade is mounted on the base for separating a watch case back from the watch case by twisting the lever relative to the base and then lifting the blade relative to the base. Full Article
ac Method of moulding and applying marks on a surface By www.freepatentsonline.com Published On :: Tue, 05 Sep 2000 08:00:00 EDT PCT No. PCT/CH96/00292 Sec. 371 Date May 22, 1998 Sec. 102(e) Date May 22, 1998 PCT Filed Aug. 23, 1996 PCT Pub. No. WO97/08592 PCT Pub. Date Mar. 6, 1997A method by which an elastomer is applied to a model (1) with relief marks to be reproduced. The purpose of the elastomer once set is to form a mold membrane (14) and incorporate within its own material the shape of the marks on the model. The mold membrane is then separated from the model and filled with a setting material, and the mold membrane is applied to a support in order to transfer the marks after preliminary pasting. Full Article
ac Moon phase menstrual tracking and educational system By www.freepatentsonline.com Published On :: Tue, 24 Feb 2009 08:00:00 EST A system and method for tracking and informing about a physical, emotional, or physiological cycle, such as a menstrual cycle, includes at least one definition entry and at least one date indicator. Each definition entry defines indicia such as color to represent a stage of a physical, emotional, or physiological cycle. Each date indicator includes a date section and a tracking section corresponding to each date section. The date section of the date indicator indicates at least one date, wherein the tracking section is capable of being marked so as to indicate indicia corresponding to a definition entry to signify the stage of the physical, emotional, or physiological cycle for each date. According to one embodiment, the date indicators are arranged according to phases of the moon to allow correlation of a user's cycle to the lunar cycle. Full Article
ac Microelectronic machine-based ariable By www.freepatentsonline.com Published On :: Tue, 02 Dec 2014 08:00:00 EST A tunable resonator is provided that has a high Q for each resonate frequency. The tunable resonator is a MEMs tunable resonator wherein the tuner is affected by moving a moveable mass, associated with the resonating portion of the resonator, form a first position to a second position such that the moveable mass is held in the first position or second position by a detent rather than a constant electromagnet magnetic or electrostatic force applied thereon. Full Article
ac Lighter and method for eliminating smoking that includes interactive self-learning software By www.freepatentsonline.com Published On :: Tue, 06 Jan 2015 08:00:00 EST Smoking cessation lighter is configured for lighting cigarettes for a smoker, and learning software is provided for monitoring smoking behavior of a smoker during a first data collection period and guiding a smoker's smoking cessation by directing the smoker when the smoker is to smoke a cigarette based on data collected during the first data collection period. The learning software monitors user behavior and collects data during use of the lighter by the smoker after the initial data collection period in order to analyze and further guide the smoker based on the smoker's cheating behavior, the smoker's behavior of lighting a cigarette for a friend, and the smoker's behavior of skipping use of the lighter at a time when the smoker has been directed to light a cigarette by the lighter. Full Article
ac Distributing capacity slices across storage system nodes By www.freepatentsonline.com Published On :: Tue, 26 May 2015 08:00:00 EDT Various systems and methods are described for configuring a data storage system. In one embodiment, a plurality of actual capacities of a plurality of storage devices of the data storage system are identified and divided into a plurality of capacity slices. The plurality of capacity slices are combined into a plurality of chunks of capacity slices, each having a combination of characteristics of the underlying physical storage devices. The chunks of capacity slices are then mapped to a plurality of logical storage devices. A group of the plurality of logical storage devices is then organized into a redundant array of logical storage devices. Full Article
ac Efficient processing of cache segment waiters By www.freepatentsonline.com Published On :: Tue, 26 May 2015 08:00:00 EDT For a plurality of input/output (I/O) operations waiting to assemble complete data tracks from data segments, a process, separate from a process responsible for the data assembly into the complete data tracks, is initiated for waking a predetermined number of the waiting I/O operations. Full Article
ac Cache policies for uncacheable memory requests By www.freepatentsonline.com Published On :: Tue, 26 May 2015 08:00:00 EDT Systems, processors, and methods for keeping uncacheable data coherent. A processor includes a multi-level cache hierarchy, and uncacheable load memory operations can be cached at any level of the cache hierarchy. If an uncacheable load misses in the L2 cache, then allocation of the uncacheable load will be restricted to a subset of the ways of the L2 cache. If an uncacheable store memory operation hits in the L1 cache, then the hit cache line can be updated with the data from the memory operation. If the uncacheable store misses in the L1 cache, then the uncacheable store is sent to a core interface unit. Multiple contiguous store misses are merged into larger blocks of data in the core interface unit before being sent to the L2 cache. Full Article
ac Single instance buffer cache method and system By www.freepatentsonline.com Published On :: Tue, 26 May 2015 08:00:00 EDT Provided is a method and system for reducing duplicate buffers in buffer cache associated with a storage device. Reducing buffer duplication in a buffer cache includes accessing a file reference pointer associated with a file in a deduplicated filesystem when attempting to load a requested data block from the file into the buffer cache. To determine if the requested data block is already in the buffer cache, aspects of the invention compare a fingerprint that identifies the requested data block against one or more fingerprints identifying a corresponding one or more sharable data blocks in the buffer cache. A match between the fingerprint of the requested data block and the fingerprint from a sharable data block in the buffer cache indicates that the requested data block is already loaded in buffer cache. The sharable data block in buffer cache is used instead thereby reducing buffer duplication in the buffer cache. Full Article
ac Optimizing a cache back invalidation policy By www.freepatentsonline.com Published On :: Tue, 26 May 2015 08:00:00 EDT A method, a system and a computer program product for enhancing a cache back invalidation policy by utilizing least recently used (LRU) bits and presence bits in selecting cache-lines for eviction. A cache back invalidation (CBI) utility evicts cache-lines by using presence bits to avoid replacing a cache-line in a lower level cache that is also present in a higher level cache. Furthermore, the CBI utility selects the cache-line for eviction from an LRU group. The CBI utility ensures that dormant cache-lines in the higher level caches do not retain corresponding presence bits set in the lower level caches by unsetting the presence bits in the lower level cache when a line is replaced in the higher level cache. Additionally, when a processor core becomes idle, the CBI utility invalidates the corresponding higher level cache by unsetting the corresponding presence bits in the lower level cache. Full Article
ac Data bus efficiency via cache line usurpation By www.freepatentsonline.com Published On :: Tue, 26 May 2015 08:00:00 EDT Embodiments of the current invention permit a user to allocate cache memory to main memory more efficiently. The processor or a user allocates the cache memory and associates the cache memory to the main memory location, but suppresses or bypassing reading the main memory data into the cache memory. Some embodiments of the present invention permit the user to specify how many cache lines are allocated at a given time. Further, embodiments of the present invention may initialize the cache memory to a specified pattern. The cache memory may be zeroed or set to some desired pattern, such as all ones. Alternatively, a user may determine the initialization pattern through the processor. Full Article
ac Distributed cache coherency protocol By www.freepatentsonline.com Published On :: Tue, 26 May 2015 08:00:00 EDT Systems, methods, and other embodiments associated with a distributed cache coherency protocol are described. According to one embodiment, a method includes receiving a request from a requester for access to one or more memory blocks in a block storage device that is shared by at least two physical computing machines and determining if a caching right to any of the one or more memory blocks has been granted to a different requester. If the caching right has not been granted to the different requester, access is granted to the one or more memory blocks to the requester. Full Article
ac Virtual machine trigger By www.freepatentsonline.com Published On :: Tue, 26 May 2015 08:00:00 EDT A computing system includes a parent partition, child partitions, a hypervisor, shared memories each associated with one of the child partitions, and trigger pages each associated with one of the child partitions. The hypervisor receives a system event signal from one of the child partitions and, in response to receiving the system event signal, accesses the trigger page associated with that child partition. The hypervisor determines whether the trigger page indicates whether data is available to be read from the shared memory associated with the child partition. The hypervisor can send an indication to either the parent partition or the child partitions that data is available to be read from the shared memory associated with the child partition if the hypervisor determines that the trigger page indicates that data is available to be read from the shared memory associated with the child partition. Full Article
ac Method and apparatus for optically backing up data By www.freepatentsonline.com Published On :: Tue, 26 May 2015 08:00:00 EDT An optical backup apparatus is provided and includes an optical storage device, an interface module to connect with at least one type of external storage medium, and a control unit to back up data from the external storage medium to the optical storage device in response to an external remote control operation. Full Article
ac System cache with quota-based control By www.freepatentsonline.com Published On :: Tue, 26 May 2015 08:00:00 EDT Methods and apparatuses for implementing a system cache with quota-based control. Quotas may be assigned on a group ID basis to each group ID that is assigned to use the system cache. The quota does not reserve space in the system cache, but rather the quota may be used within any way within the system cache. The quota may prevent a given group ID from consuming more than a desired amount of the system cache. Once a group ID's quota has been reached, no additional allocation will be permitted for that group ID. The total amount of allocated quota for all group IDs can exceed the size of system cache, such that the system cache can be oversubscribed. The sticky state can be used to prioritize data retention within the system cache when oversubscription is being used. Full Article
ac System and method for determining a level of success of operations on an abstraction of multiple logical data storage containers By www.freepatentsonline.com Published On :: Tue, 26 May 2015 08:00:00 EDT Various systems and methods are described for configuring a logical data storage container. In one embodiment, an instruction to perform an operation to modify an attribute of the logical data storage container that is an abstraction of a plurality of pertinent storage containers is received. A translated instruction to perform a sub-operation associated with the operation is transmitted to each of a number of the plurality of pertinent storage containers. A level of success of the performing of the operation on the logical data storage container is detected based on a comparison of a threshold value to a level of success of the performing of the sub-operation on each of the number of the plurality of pertinent storage containers. A report of the detected level of success is communicated. Full Article
ac System and method for virtual machine conversion By www.freepatentsonline.com Published On :: Tue, 26 May 2015 08:00:00 EDT System and method for conversion of virtual machine files without requiring copying of the virtual machine payload (data) from one location to another location. By eliminating this step, applicant's invention significantly enhances the efficiency of the conversion process. In one embodiment, a file system or storage system provides indirections to locations of data elements stored on a persistent storage media. A source virtual machine file includes hypervisor metadata (HM) data elements in one hypervisor file format, and virtual machine payload (VMP) data elements. The source virtual machine file is converted by transforming the HM data elements of the source file to create destination HM data elements in a destination hypervisor format different from the source hypervisor format; maintaining the locations of the VMP data elements stored on the persistent storage media constant during the conversion from source to destination file formats without reading or writing the VMP data elements; and creating indirections to reference the destination HM data elements in the destination hypervisor format and the existing stored VMP data elements. Full Article
ac Prefetch optimizer measuring execution time of instruction sequence cycling through each selectable hardware prefetch depth and cycling through disabling each software prefetch instruction of an instruction sequence of interest By www.freepatentsonline.com Published On :: Tue, 26 May 2015 08:00:00 EDT A prefetch optimizer tool for an information handling system (IHS) may improve effective memory access time by controlling both hardware prefetch operations and software prefetch operations. The prefetch optimizer tool selectively disables prefetch instructions in an instruction sequence of interest within an application. The tool measures execution times of the instruction sequence of interest when different prefetch instructions are disabled. The tool may hold hardware prefetch depth constant while cycling through disabling different prefetch instructions and taking corresponding execution time measurements. Alternatively, for each disabled prefetch instruction in the instruction sequence of interest, the tool may cycle through different hardware prefetch depths and take corresponding execution time measurements at each hardware prefetch depth. The tool selects a combination of hardware prefetch depth and prefetch instruction disablement that may improve the execution time in comparison with a baseline execution time. Full Article
ac Dynamically expandable and contractible fault-tolerant storage system with virtual hot spare By www.freepatentsonline.com Published On :: Tue, 26 May 2015 08:00:00 EDT A dynamically expandable and contractible fault-tolerant storage system employs a virtual hot spare that is created from unused storage capacity across a plurality of storage devices. This unused storage capacity is available if and when a storage device fails for storage of data recovered from the remaining storage device(s). On an ongoing basis, the storage system may determine the amount of unused storage capacity that would be required for the virtual hot spare (e.g., based on the number of storage devices, the capacities of the various storage devices, the amount of data stored, and the manner in which the data is stored) and generate a signal if additional storage capacity is needed for a virtual hot spare. Full Article
ac Dynamic consolidation of virtual machines By www.freepatentsonline.com Published On :: Tue, 26 May 2015 08:00:00 EDT A method and apparatus are disclosed of monitoring a number of virtual machines operating in an enterprise network. One example method of operation may include identifying a number of virtual machines currently operating in an enterprise network and determining performance metrics for each of the virtual machines. The method may also include identifying at least one candidate virtual machine from the virtual machines to optimize its active application load and modifying the candidate virtual machine to change its active application load. Full Article
ac Data caching method By www.freepatentsonline.com Published On :: Tue, 07 Jul 2015 08:00:00 EDT Data caching for use in a computer system including a lower cache memory and a higher cache memory. The higher cache memory receives a fetch request. It is then determined by the higher cache memory the state of the entry to be replaced next. If the state of the entry to be replaced next indicates that the entry is exclusively owned or modified, the state of the entry to be replaced next is changed such that a following cache access is processed at a higher speed compared to an access processed if the state would stay unchanged. Full Article
ac Decentralized caching system By www.freepatentsonline.com Published On :: Tue, 28 Jul 2015 08:00:00 EDT In a satellite communication system comprising at least a hub and a plurality of terminals, at least one terminal may include a cache for storing data objects. The cache may be based on a detachable memory device that may be inserted to or removed from the terminal at any given time, including after the terminal is deployed. Aspects are directed to preventing a prefetching of objects already stored in a cache of a remote terminal. In some embodiments, an efficient multicasting of content to terminals over an adaptive link may occur in a manner which may benefit terminals comprising a cache while not affecting or minimally affecting the performance of terminals that may not include a cache. Full Article
ac Method and system for dynamic distributed data caching By www.freepatentsonline.com Published On :: Tue, 08 Dec 2015 08:00:00 EST A method and system for dynamic distributed data caching is presented. The system includes one or more peer members and a master member. The master member and the one or more peer members form cache community for data storage. The master member is operable to select one of the one or more peer members to become a new master member. The master member is operable to update a peer list for the cache community by removing itself from the peer list. The master member is operable to send a nominate master message and an updated peer list to a peer member selected by the master member to become the new master member. Full Article
ac Substituted 1-benzylcycloalkylcarboxylic acids and the use thereof By www.freepatentsonline.com Published On :: Tue, 28 Apr 2015 08:00:00 EDT The present application relates to novel substituted 1-benzylcycloalkylcarboxylic acid derivatives, to processes for their preparation, to their use for the treatment and/or prevention of diseases, and to their use for producing medicaments for the treatment and/or prevention of diseases, especially for the treatment and/or prevention of cardiovascular disorders. Full Article
ac α-keto alkylperacids and methods for producing and using the same By www.freepatentsonline.com Published On :: Tue, 28 Apr 2015 08:00:00 EDT The present invention provides α-keto alkylperacids and methods for producing and using the same. In particular, α-keto alkylperacids are useful as antimicrobial agents. Full Article
ac Substituted 3-phenylpropionic acids and the use thereof By www.freepatentsonline.com Published On :: Tue, 28 Apr 2015 08:00:00 EDT The present application relates to novel 3-phenylpropionic acid derivatives, to processes for their preparation, to their use for the treatment and/or prevention of diseases and to their use for preparing medicaments for the treatment and/or prevention of diseases, in particular for the treatment and/or prevention of cardiovascular disorders. Full Article
ac Process and system for the separation and drying of carboxylic acid crystals By www.freepatentsonline.com Published On :: Tue, 28 Apr 2015 08:00:00 EDT In a process for the separation and drying of crude carboxylic acid crystals from a slurry in a solvent, the slurry is supplied to a filter operating at pressure and at a temperature above the atmospheric boiling point of the solvent. A cake of separated crystals is removed from the filter and passed to a thermal dryer. In a system for the separation and drying of crude carboxylic acid from a slurry in a solvent, a pressure filter device has a slurry inlet and an outlet for a cake of carboxylic acid crystals. The system also has a thermal dryer and means for transporting the cake of carboxylic acid crystals from the pressure filter device to the dryer. The pressure filter device is configured to operate at a pressure and temperature above the atmospheric boiling point of the solvent. Full Article
ac Process for recovering aliphatic monocarboxylic acids from distillation By www.freepatentsonline.com Published On :: Tue, 28 Apr 2015 08:00:00 EDT A process is provided for recovering aliphatic monocarboxylic acids having from 4 to 11 carbon atoms from the distillation residue obtained in the oxidation of the corresponding aldehyde by means of oxygen or oxygen-containing gas mixtures in the presence of alkali metal carboxylates or alkaline earth metal carboxylates to form the corresponding monocarboxylic acid and subsequent distillation, characterized in that the distillation residue is reacted with an aqueous acid in a tube reactor and the two-phase mixture flowing out from the tube reactor is introduced into a settling vessel in which the organic phase which separates out has a pH of 4.5 or less. Full Article
ac Use of sulfonic acid for recovering glycerol resulting from the triglyceride transesterification reaction By www.freepatentsonline.com Published On :: Tue, 28 Apr 2015 08:00:00 EDT The present invention relates to the use of at least one sulfonic acid for recovering glycerol resulting from a reaction crude from transesterification of glycerides, in particular of triglycerides of vegetable and/or animal origin. The invention also relates to a process for purifying glycerol obtained as a by-product of triglyceride transesterification during the preparation of fatty acids, fatty esters and/or fatty acid salts, and also to a combined process for preparing, on the one hand, fatty acids, fatty esters and/or fatty acid salts and, on the other hand, glycerol, from triglycerides, using at least one sulfonic acid. Full Article
ac Actinic-ray- or radiation-sensitive resin composition, compound and method of forming pattern using the composition By www.freepatentsonline.com Published On :: Tue, 05 May 2015 08:00:00 EDT According to one embodiment, an actinic-ray- or radiation-sensitive resin composition includes any of the compounds (A) of general formula (I) below that when exposed to actinic rays or radiation, generates an acid and a resin (B) whose rate of dissolution into an alkali developer is increased by the action of an acid. (The characters used in general formula (I) have the meanings mentioned in the description.) Full Article
ac Process for producing terephthalic acid By www.freepatentsonline.com Published On :: Tue, 05 May 2015 08:00:00 EDT Methods of producing terephthalic acid are described. The methods involve using a substantially pure p-toluic acid stream. The substantially pure p-toluic acid stream, a solvent comprising an ionic liquid and optionally a carboxylic acid, a bromine source, a catalyst, and an oxidizing agent are contacted to produce a product comprising terephthalic acid. Full Article
ac Reactor and process for propane oxidation By www.freepatentsonline.com Published On :: Tue, 05 May 2015 08:00:00 EDT The amount of propionic acid produced in the process of oxidizing propane to acrylic acid is reduced by using a reactor with a length/diameter ratio >10 and/or maintaining the difference between the target reaction temperature and the peak temperature within the reactor to less than 20° C. Full Article
ac Method for recovering and purifying propionic acid By www.freepatentsonline.com Published On :: Tue, 05 May 2015 08:00:00 EDT The present invention provides a method for purifying and recovering propionic acid from an aqueous mixture containing a fermentation product obtained from a fermentation process using glycerol as substrate, the method comprising optionally acidifying the aqueous mixture to a pH below 4.5, subjecting the aqueous mixture to an extraction with extracting agent containing a heavy extractant and optionally a light extractant as a diluent to obtain an extract comprising the extracting agent and organic acids, and a raffinate comprising water and any unreacted glycerol, and subjecting the extract to vacuum evaporation to separate propionic acid-containing organic acids from the extractant. Full Article
ac Methods for producing acrylic acid and/or ester thereof and polymer of the acrylic acid and/or ester thereof By www.freepatentsonline.com Published On :: Tue, 12 May 2015 08:00:00 EDT A method for producing acrylic acid and/or an ester thereof from a raw material composition containing hydroxypropionic acid and/or an ester thereof, the method including the steps of: (a) evaporating the raw material composition; and (b) dehydrating the evaporated raw material composition by contact with a dehydration catalyst, wherein the total amount of hydroxypropionic acid and/or an ester thereof supplied in the step (b) is controlled to be 70% by mass or more based on 100% by mass of the total amount of hydroxypropionic acid and/or an ester thereof supplied in the step (a). Full Article
ac Method for the conversion of methylmercaptopropionaldehyde formed from crude acrolein and crude methyl mercaptan By www.freepatentsonline.com Published On :: Tue, 12 May 2015 08:00:00 EDT A reactive rectification column suitable for the production of 2-hydroxy-4-methylmercaptobutyric acid and/or methionine contains a weir having a height of 100 mm or more. Full Article
ac Process for producing (meth)acrylic acid By www.freepatentsonline.com Published On :: Tue, 12 May 2015 08:00:00 EDT A process for producing (meth)acrylic acid comprising the step of repeating a crystallization operation “n” times to produce purified (meth)acrylic acid from crude (meth)acrylic acid, wherein: the each crystallization operation comprises a crystallizing step and a melting step; a polymerization inhibitor is not added to a (meth)acrylic acid melt obtained in the melting step of the first to n−1th crystallization operation(s) and a (meth)acrylic acid solution subjected to the crystallizing step of the second to nth crystallization operation(s); and a concentration of a polymerization inhibitor in a (meth)acrylic acid solution subjected to the crystallizing step of the first crystallization operation is adjusted so that a concentration of the polymerization inhibitor in a (meth)acrylic acid solution subjected to the crystallizing step of the nth crystallization operation is 2 ppm by mass or higher. Full Article
ac Method for preparing high purity mono-hydrolyzed acyl halide compound By www.freepatentsonline.com Published On :: Tue, 12 May 2015 08:00:00 EDT A method for preparing a high purity (e.g. greater than 70 wt. %) mono-hydrolyzed acyl halide compound as a precipitate from solution comprising the steps of preparing a solution comprising: i) at least 80 v/v % of a hydrocarbon solvent, ii) water at a molar concentration greater than its solubility limit within the solvent but less that its solubility limit in solution, iii) a tri-hydrocarbyl phosphate compound, and iv) a polyfunctional acyl halide compound at molar ratio to both water and the tri-hydrocarbyl phosphate compound of at least 1:1. Full Article
ac L-ornithine phenyl acetate and methods of making thereof By www.freepatentsonline.com Published On :: Tue, 19 May 2015 08:00:00 EDT Disclosed herein are forms of L-ornithine phenyl acetate and methods of making the same. A crystalline form may, in some embodiments, be Forms I, II, III and V, or mixtures thereof. The crystalline forms may be formulated for treating subjects with liver disorders, such as hepatic encephalopathy. Accordingly, some embodiments include formulations and methods of administering L-ornithine phenyl acetate. Full Article