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Versatile additively manufactured (3D printed) wall-jet flow cell for high performance liquid chromatography-amperometric analysis: application to the detection and quantification of new psychoactive substances (NBOMes)

Anal. Methods, 2020, 12,2152-2165
DOI: 10.1039/D0AY00500B, Paper
Open Access
Hadil M. Elbardisy, Eduardo M. Richter, Robert D. Crapnell, Michael P. Down, Peter G. Gough, Tarek S. Belal, Wael Talaat, Hoda G. Daabees, Craig E. Banks
Additive manufacturing is an emerging technology of vast applicability, receiving significant interest in a plethora of industrial and research domains as it allows the translation of designs produced via computer software, into 3D printed objects.
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High cytotoxic activity of ZnO@leucovorin nanocomposite based materials against an MCF-7 cell model

Anal. Methods, 2020, 12,2176-2184
DOI: 10.1039/D0AY00498G, Paper
Mohamed Fathi Sanad, Esraa Samy Abu Serea, Shereen Magdy Bazid, Shimaa Nabih, Md Ariful Ahsan, Ahmed Esmail Shalan
In the current work, we design a multifunctional hybrid nanocomposite for treating MCF-7 cell lines, which act as a model for breast cancer cells, to overcome the serious side-effects of chemotherapy treatment pathways.
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Discrimination between fresh, chilled, and frozen/thawed chicken based on its skin's spectrochemical and optical properties

Anal. Methods, 2020, 12,2093-2101
DOI: 10.1039/D0AY00324G, Paper
Omnia Hamdy, Zienab Abdel-Salam, Mohamed Abdel-Harith
Monitoring of the spectrochemical and optical properties of biomaterials has been widely utilized in many biomedical applications for both diagnosis and therapy.
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Multi-residue determination of micropollutants in Nigerian fish from Lagos lagoon using ultrasound assisted extraction, solid phase extraction and ultra-high-performance liquid chromatography tandem mass spectrometry

Anal. Methods, 2020, 12,2114-2122
DOI: 10.1039/D0AY00411A, Paper
Idera Fabunmi, Natalie Sims, Kathryn Proctor, Aderonke Oyeyiola, Temilola Oluseyi, Kehinde Olayinka, Barbara Kasprzyk-Hordern
This reports for the first time a simple and robust approach in determining pharmaceuticals in different fish species in Nigeria.
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The characterization of self-assembled nanostructures in whole blood

Anal. Methods, 2020, 12,2068-2081
DOI: 10.1039/D0AY00170H, Tutorial Review
Mark Pitman, Jessica Larsen
This tutorial describes methods of characterizing nanomaterials in whole blood, and the associated benefits and shortcomings of each technique.
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Development of a paper-immobilized yeast biosensor for the detection of physiological concentrations of doxycycline in technology-limited settings

Anal. Methods, 2020, 12,2123-2132
DOI: 10.1039/D0AY00001A, Paper
Rachel A. Miller, Galen Brown, Elsa Barron, Jamie L. Luther, Marya Lieberman, Holly V. Goodson
To combat pharmaceutical counterfeiting in low- and middle-income countries (LMIC), there is a need for improved low-cost, portable methods that monitor pharmaceutical concentrations relevant to dosage forms and physiological fluids.
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Aptamer-based fluorometric determination of chloramphenicol by controlling the activity of hemin as a peroxidase mimetic

Anal. Methods, 2020, Advance Article
DOI: 10.1039/D0AY00389A, Paper
Ling-Chen Wang, Cheng-Yi Hong, Zheng-Zhong Lin, Xiao-Mei Chen, Zhi-Yong Huang
A method for the aptamer-based determination of chloramphenicol (CAP) was developed by exploiting the peroxidase mimicking activity of hemin.
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In situ imaging of intracellular human telomerase RNA with molecular beacon-functionalized gold nanoparticles

Anal. Methods, 2020, Advance Article
DOI: 10.1039/D0AY00461H, Paper
Tao Xie, Ziyan Fan, Ruilong Zhang, Xiaohe Tian, Guangmei Han, Zhengjie Liu, Zhongping Zhang
We develop molecular beacon-functionalized gold nanoparticles for in situ human telomerase RNA imaging in live cells.
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Determination of polychlorinated biphenyls and organochlorine pesticides in Chinese mitten crabs (Eriocheir sinensis) using modified QuEChERS followed by GC-MS

Anal. Methods, 2020, Advance Article
DOI: 10.1039/D0AY00519C, Paper
Ting Liu, Jianguang Zhou, Li He, Jinhua Gan
A new QuEChERS method followed by GC-MS was developed for the simultaneous analysis of polychlorinated biphenyls (PCBs) and organochlorine pesticides (OCPs) in Chinese mitten crabs.
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Au nanoparticle preconcentration coupled with CE-electrochemiluminescence detection for sensitive analysis of fluoroquinolones in European eel (Anguilla anguilla)

Anal. Methods, 2020, Accepted Manuscript
DOI: 10.1039/D0AY00264J, Paper
Longhua Guo, Meihua Liu, Yuechun Yin, Lifen Chen, Zhitao Chen, Jing-Jing Liu, Bin Qiu
In this work, a novel method based on gold nanoparticle preconcentration coupled with CE for electrochemiluminescent detection of ciprofloxacin, enrofloxacin, ofloxacin, and norfloxacin in European eels was developed. The addition...
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Plasticizer-free and pH-independent ion-selective optode films based on a solvatochromic dye

Anal. Methods, 2020, Accepted Manuscript
DOI: 10.1039/D0AY00439A, Communication
Xuewei Wang, Yang Zhou, Vanessa Decker, Mark E. Meyerhoff, Meng Sun, Yu Cui
A layer of a solvatochromic dye, an ionophore, and an ion-exchanger deposited on a Nylon membrane enables highly selective colorimetric and fluorometric ion sensing. This new platform does not suffer...
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Colorimetric speciation analysis of chromium using 2-thiobarbituric acid capped silver nanoparticles

Anal. Methods, 2020, Advance Article
DOI: 10.1039/D0AY00160K, Paper
Kamal Mousapour, Salahaddin Hajizadeh, Khalil Farhadi
Colorimetric determination of Cr(III) and Cr(VI) based on 2-thiobarbituric acid capped silver nanoparticles.
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Confirmation of brand identification in infant formulas by using near-infrared spectroscopy fingerprints

Anal. Methods, 2020, Advance Article
DOI: 10.1039/D0AY00375A, Paper
Shuyi Chang, Chengcheng Yin, Sha Liang, Mei Lu, Ping Wang, Zhicheng Li
The NIR spectra of 12 batches of each stage of Brand A infant formulas.
To cite this article before page numbers are assigned, use the DOI form of citation above.
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Portable and benchtop Raman spectrometers coupled to cluster analysis to identify quinine sulfate polymorphs in solid dosage forms and antimalarial drug quantification in solution by AuNPs-SERS with MCR-ALS

Anal. Methods, 2020, Advance Article
DOI: 10.1039/D0AY00693A, Paper
Sarmento J. Mazivila, Helena I. S. Nogueira, Ricardo N. M. J. Páscoa, David S. M. Ribeiro, João L. M. Santos, João M. M. Leitão, Joaquim C. G. Esteves da Silva
Raman spectrometers coupled to cluster analysis were able to identify two polymorphs of quinine sulfate in solid dosage forms. Gold nanoparticles-surface-enhanced Raman scattering with MCR-ALS was used to antimalarial drug quantification in solution.
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Comparison of surfactant-mediated liquid chromatographic modes with sodium dodecyl sulphate for the analysis of basic drugs

Anal. Methods, 2020, Advance Article
DOI: 10.1039/D0AY00526F, Paper
N. Pankajkumar-Patel, E. Peris-García, M. J. Ruiz-Angel, M. C. García-Alvarez-Coque
A comprehensive overview of the performance of MLC, HSLC and MELC for the analysis of basic compounds.
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Solid-phase microextraction using a β-ketoenamine-linked covalent organic framework coating for efficient enrichment of synthetic musks in water samples

Anal. Methods, 2020, Advance Article
DOI: 10.1039/C9AY02755F, Paper
Lian Wen, Peng Wu, Lei-Lei Wang, Li-Zong Chen, Ming-Lin Wang, Xia Wang, Jin-Ming Lin, Ru-Song Zhao
This study indicated the promising applicability of the TpPa-1 as a solid-phase microextraction fiber coating for reliably detecting synthetic musks at trace levels from environmental samples.
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One-step synthesis of mitochondrion-targeted fluorescence carbon dots and fluorescent detection of silver ions

Anal. Methods, 2020, Accepted Manuscript
DOI: 10.1039/D0AY00622J, Paper
Yue Hou, Hanxiao Liu, Zhanxian Li, Hongyan Zhang, Liuhe Wei, Mingming Yu
Silver ions (Ag+) are the most representative harmful ions found in water pollution and widely used in many industries, excessive ingestion of Ag+ in the human body may interact with...
The content of this RSS Feed (c) The Royal Society of Chemistry




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Sample treatment based on molecularly imprinted polymers for the analysis of veterinary drugs in food samples: a review

Anal. Methods, 2020, Accepted Manuscript
DOI: 10.1039/D0AY00533A, Critical Review
Israel Samuel Ibarra, J. M. Miranda, Irma Perez, Aldo C Jardinez, Gabriela Islas
The use of veterinary drugs in medical treatments and in the livestock industry is a recurrent practice. In subtherapeutic doses during prolonged times act to growth promoters. Residues of these...
The content of this RSS Feed (c) The Royal Society of Chemistry




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Multivariate optimization of an ultrasound-assisted extraction procedure for the determination of Cu, Fe, Mn, and Zn in plant samples by flame atomic absorption spectrometry

Anal. Methods, 2020, Advance Article
DOI: 10.1039/D0AY00554A, Paper
Floriatan Santos Costa, Raquel Viana Pinto Leal, Clissiane Soares Viana Pacheco, Fábio Alan Carqueija Amorim, Raildo Mota de Jesus, Luana Novaes Santos, Erik Galvão Paranhos da Silva
A new ultrasound-assisted extraction method simple and fast was developed employing multivariate optimization.
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Colorimetric indicators for volatile amines based on succinic anhydride (SAh)-grafted poly (lactic acid) (PLA)

Anal. Methods, 2020, Advance Article
DOI: 10.1039/D0AY00550A, Paper
Adrian Lopera-Valle, Anastasia Elias
Smart materials that can undergo changes in color upon the detection of amines have the potential to provide information on the freshness of fish and meat.
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Facile dispersive solid-phase extraction based on humic acid for the determination of aflatoxins in various edible oils

Anal. Methods, 2020, Advance Article
DOI: 10.1039/D0AY00534G, Paper
Ping Liu, Yan-Hua Liao, Hao-Bo Zheng, Yang Tang
Aflatoxins (AFs), as the secondary metabolites produced by some toxigenic fungi of Aspergillus species, are well known to be extremely harmful to humans and animals because of their high toxicity, mutagenicity, carcinogenicity, and teratogenicity.
To cite this article before page numbers are assigned, use the DOI form of citation above.
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Miniaturized QuEChERS method for determination of 97 pesticide residues in wine by ultra-high performance liquid chromatography coupled to tandem mass spectrometry

Anal. Methods, 2020, Accepted Manuscript
DOI: 10.1039/D0AY00744G, Paper
Gabrieli Bernardi, Magali Kemmerich, Martha B Adaime, Osmar Damian Prestes, Renato Zanella
A miniaturized sample preparation method was developed and validated for the multiresidue determination of 97 pesticide residues in wine samples. The proposed extraction procedure is based on QuEChERS acetate method...
The content of this RSS Feed (c) The Royal Society of Chemistry




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A rapid and colorimetric biosensor based on GR-5 DNAzyme and self-replicating catalyzed hairpin assembly for lead detection

Anal. Methods, 2020, 12,2215-2220
DOI: 10.1039/D0AY00091D, Paper
Fang Wang, Jianyuan Dai, Hongli Shi, Xiaoqian Luo, Lan Xiao, Cuisong Zhou, Yong Guo, Dan Xiao
A rapid and colorimetric biosensor for Pb2+ detection has been constructed on the basis of Pb2+-dependent GR-5 DNAzyme and the self-replicating catalyzed hairpin assembly (SRCHA) reaction.
The content of this RSS Feed (c) The Royal Society of Chemistry




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Detection of organophosphorus compounds using a surface acoustic wave array sensor based on supramolecular self-assembling imprinted films

Anal. Methods, 2020, 12,2206-2214
DOI: 10.1039/D0AY00211A, Paper
Yong Pan, Tengxiao Guo, Genwei Zhang, Junchao Yang, Liu Yang, Bingqing Cao
In this study, diisopropyl methylphosphonate (DIMP), tributyl phosphate (TBP), and dimethyl methylphosphonate (DMMP) were selected as organophosphorus chemical warfare agent (CWA) simulants.
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Hydrothermal synthesis of Auricularia auricula derived nitrogen, phosphorus-doped carbon dots and application in Ag(I) and 4-nitrophenol detection and bioimaging

Anal. Methods, 2020, 12,2237-2243
DOI: 10.1039/D0AY00316F, Paper
Yujiao Tu, Suping Wang, Xiaotian Yuan, Pengfei Song, Yunlin Wei, Kunhao Qin, Qi Zhang, Xiuling Ji
Schematic of the synthetic route for fluorescent Aa N,P-CDs and their application in the detection of 4-NP and Ag(I) and bioimaging.
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Adsorptive removal of Hg2+ from environmental water samples using thioglycerol-intercalated magnetic layered double hydroxides

Anal. Methods, 2020, 12,2279-2286
DOI: 10.1039/D0AY00448K, Paper
Ali Esrafili, Mahnaz Ghambarian, Mohammad Tajik, Mahroo Baharfar
Herein, the removal of Hg2+ from environmental water samples was carried out using a novel nanoadsorbent based on magnetite nanoparticles coated by a thioglycerol-intercalated layered double hydroxide.
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Identification of Gentiana rigescens from different geographical origins based on HPLC and FTIR fingerprints

Anal. Methods, 2020, 12,2260-2271
DOI: 10.1039/D0AY00309C, Paper
Yanli Zhao, Tianjun Yuan, Lihua Wu, Ji Zhang, Zhitian Zuo, Yuanzhong Wang
Gentiana rigescens is a traditional Chinese medicine with efficacy in liver protection, as a cholagogic, anti-hyperglycemic, and anti-hypertension agent, and in relieving spasms and pain.
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Simultaneous aptasensor assay of ochratoxin A and adenosine triphosphate in beer based on Fe3O4 and SiO2 nanoparticle as carriers

Anal. Methods, 2020, 12,2253-2259
DOI: 10.1039/D0AY00311E, Paper
Xiluan Yan, Mengmeng Jiang, Yuting Jian, Jing Luo, Xinxin Xue, Xin Chen, Xiangjuan Zheng, Fanrong Ai
In this work, a chemiluminescence (CL) method based on dual aptasensors using Fe3O4 and SiO2 nanoparticles (NPs) as carriers is developed for the simultaneous detection of ochratoxin A (OTA) and adenosine triphosphate (ATP) in beer.
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Detection of radium at the attogram per gram level in copper by inductively coupled plasma mass spectrometry after cation-exchange chromatography

Anal. Methods, 2020, 12,2272-2278
DOI: 10.1039/D0AY00512F, Paper
Mélodie Bonin, Dominic Larivière, Pavel P. Povinec
In this study, a new method was developed for the separation and isolation of radium from metallic copper.
The content of this RSS Feed (c) The Royal Society of Chemistry




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A simple paper-based approach for arsenic determination in water using hydride generation coupled with mercaptosuccinic-acid capped CdTe quantum dots

Anal. Methods, 2020, Accepted Manuscript
DOI: 10.1039/D0AY00273A, Paper
Oraphan Thepmanee, Kanlaya Prapainop Katewongsa, Obnithi Nooppha, Nuanlaor Ratanawimarnwong, Weena Siangproh, Orawon Chailapakul, Kriangsak Songsrirote
This research aims to develop a simple paper-based device for arsenic detection in water samples where a hydride generation technique coupled with mercaptosuccinic acid-capped CdTe quantum dots (MSA-CdTe QDs) as...
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Dispersive micro-solid phase extraction based on graphene/polydopamine composite for the extraction of pyrethroids in water samples

Anal. Methods, 2020, Accepted Manuscript
DOI: 10.1039/D0AY00562B, Paper
Qinqin Xu, Kexin Qiao, Chen Yan, Zikai Liu, Runhua Lu, Wenfeng Zhou
In this study, a simple, rapid, precise, and environmentally friendly microextraction named dispersive micro-solid phase extraction based on graphene/polydopamine composite as sorbent was investigated for the analysis of four pyrethroids...
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A flower-like Ag coated with molecularly imprinted polymers as surface-enhanced Raman scattering substrate for sensitive and selective detection of glibenclamide

Anal. Methods, 2020, Accepted Manuscript
DOI: 10.1039/D0AY00575D, Paper
Xiaohui Ren, Xin Li
The flower-like Ag, was formed by nanosheets self-assembly, as SERS active substrate was utilized for preparation of flower-like Ag@molecularly imprinted polymers (MIPs) surface-enhanced Raman scattering (SERS) sensor. Based on the...
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Rapid and colorimetric detection of nucleic acids based on entropy-driven circuit and DNAzyme mediated autocatalytic reaction

Anal. Methods, 2020, Accepted Manuscript
DOI: 10.1039/D0AY00341G, Paper
Hongli Shi, Jianyuan Dai, fang Wang, Yushun Xia, Dan Xiao, Cuisong Zhou
In this work, a novel, rapid and enzyme-free colorimetric biosensor for nucleic acids detection has been developed based on entropy-driven circuit (EDC) and DNAzyme mediated autocatalytic reaction. Upon sensing of...
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Fabrication of an electrochemical sensor based on metal-organic framework ZIF-8 for quantitation of silver ion: optimizing experimental conditions by central composite design (CCD)

Anal. Methods, 2020, Accepted Manuscript
DOI: 10.1039/D0AY00843E, Paper
Farzaneh Hashemi , Ali Reza Zanganeh, Farid Naeimi , Maryam Tayebani
The ZIF-8 was synthesized and carbon paste electrode (CPE) modified with this metal-organic framework utilized for quantitation of silver(Ι) by differential pulse anodic stripping voltammetry (DPASV) technique. The prepared ZIF-8...
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May 30 Webinar: Happy Birthday Walt!: Digitized Walt Whitman Collections from the Manuscript Division

Reminder!!

Please join us for our May topical webinar:

Happy Birthday Walt!: Digitized Walt Whitman Collections from the Manuscript Division

May 2019 marks the 200th anniversary of the birth of poet Walt Whitman, who revolutionized the style and content of American poetry with his 1855 publication of Leaves of Grass. Whitman was also a journalist, printer, publisher, orator, and prose writer.

The Library of Congress holds the largest group of Whitman-related special collection materials in the world, including printed materials, rare books, photographs, and manuscripts. In this webinar program, Manuscript Division historian Barbara Bair highlights the content and research use of three digitized Whitman manuscript collections as well as programs celebrating Whitman’s birthday at the Library of Congress.

Date: Thursday, May 30
Time
: 1:00 pm – 2:00 pm EDT
Registration (required): Please register via Eventbrite.

This program will be held in real time via webinar software, which allows participants from around the country and the world to join us. Confirmation and log-on instructions will be sent via email. Please read the Library of Congress Comment and Posting Policy.

ADA: Request ADA accommodations five days in advance at (202) 707-6362 or ada@loc.gov. Registration for the program is also required.

Questions? Ask A Librarian!

 




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Perils of Perestroika : viewpoints from the Soviet press, 1989-1991 / edited by Isaac J. Tarasulo.

Wilmington, Del. : SR Books, 1992




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North American borders in comparative perspective [electronic resource] / edited by Guadalupe Correa-Cabrera and Victor Konrad.

Tucson : University of Arizona Press, 2020.




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Between Rome and Persia [electronic resource] : the middle Euphrates, Mesopotamia, and Palmyra under Roman control / Peter M. Edwell

London ; New York : Routledge, 2008




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The Oxford handbook of ancient Anatolia, 10,000-323 B.C.E. [electronic resource] / edited by Sharon R. Steadman and Gregory McMahon.

New York ; Oxford : Oxford University Press, 2011.




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The Oxford handbook of Anglo-Saxon archaeology [electronic resource] / edited by Helena Hamerow, David A. Hinton and Sally Crawford.

Oxford : Oxford University Press, 2011.




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The Oxford handbook of Roman Egypt [electronic resource] / edited by Christina Riggs.

Oxford : Oxford University Press, 2012.




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Egyptian mummies and modern science [electronic resource] / edited by Rosalie David

Cambridge ; New York : Cambridge University Press, 2008




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Recharting the Black Atlantic [electronic resource] : modern cultures, local communities, global connections / edited by Annalisa Oboe and Anna Scacchi

New York : Routledge, 2008




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Asian-European relations [electronic resource] : building blocks for global governance? / edited by Jürgen Rüland [and others]

London ; New York : Routledge, 2008




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The United States and Iran [electronic resource] : sanctions, wars and the policy of dual containment / Sasan Fayazmanesh

London ; New York : Routledge, 2008




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Tax relief likely on forced residency due to Coronavirus Lockdown

Their period of overstay in India due to lockdown could be exempted, as prescribed by OECD.




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Covid alters India's borrowing plan, target now raised to Rs 12L cr

Govt will borrow Rs 6L cr from the market via gilts through the remaining part of the first half of the year.




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Topics in Statistical Simulation [electronic resource] : Research Papers from the 7th International Workshop on Statistical Simulation / edited by V.B. Melas, Stefania Mignani, Paola Monari, Luigi Salmaso

New York, NY : Springer New York : Imprint: Springer, 2014




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Analysis and Geometry of Markov Diffusion Operators [electronic resource] / by Dominique Bakry, Ivan Gentil, Michel Ledoux

Cham : Springer International Publishing : Imprint: Springer, 2014




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German-Japanese Interchange of Data Analysis Results [electronic resource] / edited by Wolfgang Gaul, Andreas Geyer-Schulz, Yasumasa Baba, Akinori Okada

Cham : Springer International Publishing : Imprint: Springer, 2014