A target and object receiving device that includes a base portion having an outer edge and a lower coupling area disposed on a top surface of the base portion. An upper portion is spaced vertically from the base portion and includes an outer edge and an upper coupling area disposed on a bottom surface of the upper portion. A separator extends vertically from the lower coupling area to the upper coupling area. Either: (a) the top surface of the base portion approaches the bottom surface of the upper portion as the top surface extends from the outer edge of the base portion toward the lower coupling area; or (b) the bottom surface of the upper portion approaches the top surface of the base portion as the bottom surface of the upper portion extends from the outer edge of the base portion toward the upper coupling area.

A graphic may include a consumable and having optically encoded information.

A frequency tripler device is disclosed. The frequency tripler device includes a first graphene based field effect transistor (FET) of a first dopant type, having a gate, a drain, and a source, and a second graphene based FET of a second dopant type, having a gate, a drain, and a source, the gate of the first FET coupled to the gate of the second FET and coupled to an input signal having an alternating current (AC) signal of a first frequency, the combination of the first and second FETs generates an output signal with a dominant AC signal of a frequency of about three times the first frequency.

A digital phase locked loop (DPLL), a method of operating the same, and a device including the same are provided. The DPLL includes a digitally-controlled oscillator configured to change a frequency and a phase of an output oscillation signal in response to a digital control code; a main divider configured to divide the frequency of the output oscillation signal and generate a first feedback signal based on the divided frequency; and a phase-to-digital converter configured to subdivide the phase of the output oscillation signal and to generate a quantized code by converting a phase difference between a reference signal and the first feedback signal using a phase-subdivided signal resulting from the subdivision. The digital control code is generated based on the quantized code.

Methods, systems, and apparatuses are described for compensating for an undesired fractional spur due to a PLL in a communication system. The communication system includes a time-to-digital converter (TDC) that is configured to execute in parallel to the PLL. The TDC is configured to determine a phase difference between a reference frequency and an output oscillation signal provided by the PLL. The phase difference is received by a processor to estimate particular characteristics of the undesired fractional spur, and the estimate of the characteristics is used to construct an estimate of the undesired fractional spur.

A circuit includes a power supply terminal and a clock parsing circuit configured to produce multiple clock signals having a common clock period and different phases. The circuit further includes a plurality of digital circuits coupled to the clock parsing circuit and the power supply terminal. Each digital circuit includes an input to receive data and logic to process the data. Each digital circuit is responsive to a phase associated with a respective clock signal of the multiple clock signals to draw current from the regulated power supply terminal to process the data to produce a data output. Additionally, the circuit includes an output timing management circuit coupled to each of the plurality of digital circuits and configured to control data outputs of each of plurality of digital circuits to prevent timing violations at one or more destination circuits.

A phase locked loop (PLL) includes a first loop, a second loop, and a lock detector. The first loop locks a feedback signal having a frequency equal to a fraction of a frequency of an output signal to a reference signal in phase. The first loop has a first bandwidth. The second loop locks the feedback signal to the reference signal in frequency and has a second bandwidth. The first bandwidth is higher than the second bandwidth. The lock detector is coupled to the second loop and increases the second bandwidth in response to detecting that the feedback signal is not locked to the reference signal.

A porous silica material in which silica particles are connected to one another three-dimensionally, wherein: the porous silica material includes a through hole including first pores smaller than a mean free path of an air, and second pores larger than the first pores; the porous silica material has a density of 100 kg/m3 or more and 300 kg/m3 or less; and an isobutyl group is bound to silicon of silica of the silica particles.

The invention relates to a process and apparatus for recovering sulfur (9). In a sour gas scrubbing apparatus (S) comprises a scrubbing part (SP) and a regeneration part (RP), wherein sulfur components and carbon dioxide are selectively removed from a crude synthesis gas (2) with the aid of a circulating scrubbing agent (3). A sulfur-containing gas fraction (8) produced during the regeneration of loaded scrubbing agent is supplied to a sulfur recovery system (SR) in which an off-gas (10) comprising carbon dioxide and also sulfur components is formed. The off-gas is hydrogenated (H) and subsequently subjected to a gas scrubbing operation (Z). The hydrogenated off-gas (12) is scrubbed, independently of the crude synthesis gas (2), and scrubbing agent (13) removed from the scrubbing agent circuit of the sour gas scrubbing apparatus (S) is used to scrub out sulfur components from the hydrogenated off-gas (12).

An object the invention is to provide a phosphorus pentafluoride producing process wherein phosphorus pentafluoride is separated/extracted from a pentavalent phosphorus compound or a solution thereof, or a composition obtained by allowing the pentavalent phosphorus compound or the solution thereof to react with hydrogen fluoride, thereby producing phosphorus pentafluoride; and a phosphate hexafluoride producing process wherein the resultant phosphorus pentafluoride is used as raw material to produce a phosphate hexafluoride high in purity. The present invention relates to a process for producing phosphorus pentafluoride, wherein a carrier gas is brought into contact with either of the following one: a pentavalent phosphorus compound, a solution thereof, or a solution in which a composition obtained by allowing the pentavalent phosphorus compound or the solution thereof to react with hydrogen fluoride is dissolved, thereby a phosphorus pentafluoride is extracted into the career gas.

System and method for sustainable economic development which includes hydrogen extracted from substances, for example, sea water, industrial waste water, agricultural waste water, sewage, and landfill waste water. The hydrogen extraction is accomplished by thermal dissociation, electrical dissociation, optical dissociation, and magnetic dissociation. The hydrogen extraction further includes operation in conjunction with energy addition from renewable resources, for example, solar, wind, moving water, geothermal, or biomass resources.

A method of preparing functionalized graphene, comprises treating graphene with an alkali metal in the presence of an electron transfer agent and coordinating solvent, and adding a functionalizing compound. The method further includes quenching unreacted alkali metal by addition of a protic medium, and isolating the functionalized graphene.

Providing a roaster that operates at temperatures in the range of 800° Celsius to 2000° Celsius with inert, optional oxidizing and reducing gases to treat graphite contaminated with radionuclides including tritium, carbon-14, and chlorine-36. The combination of temperatures and gases allow for the removal of most to substantially all the carbon-14 within the graphite while substantially limiting gasifying the bulk graphite.

The present invention relates to a method of preparing a spherical mesoporous silica structure containing silver nanoparticles dispersed therein by adding a silver nitrate solution to an aqueous surfactant solution and performing a sol-gel process and to spherical mesoporous silica prepared thereby. The spherical mesoporous silica is cost-effective compared to a conventional method that uses silver nanoparticles as a raw material, because the silver nitrate solution that is inexpensive compared to silver nanoparticles is used. Also, the spherical mesoporous silica can be with high productivity in large amounts, and thus is easily commercialized. Moreover, because silver nanoparticles are incorporated into the pores of the mesoporous silica, the silver nanoparticles are used stably and do not change color and odor. In addition, the spherical mesoporous silica exhibits various additional effects, including far-infrared ray emission and deodorization, attributable to silica.

A method is provided for constructing a tomographic reconstruction through the application of statistical inversion. Unknowns associated with points of a reconstruction grid are represented with components of a vector-valued variable. A next version of the vector-valued variable is repeatedly created by drawing for each component a value from a conditional distribution. The components of a so generated version of the vector-valued variable are used as the tomographic reconstruction. The components are divided into sets, so that components in a set represent unknowns associated with mutually independent points of the reconstruction grid, or into independent collections. For at least two components of a set or at least two collections, the drawing of values from a conditional distribution is performed in parallel in a computer-implemented process.

A radio tomographic image generation device includes a reconstruction unit for generating a plurality of reconstructed images of different iteration numbers by a successive approximation process; a region segmentation unit for obtaining information about structure based on radiographic image signals, and segmenting, based on the information about structure, a region, of which the tomographic image is generated, into a plurality of segmented regions having different information about structure; and an image combining unit for generating partial tomographic images by using the reconstructed images of different iteration numbers for the individual segmented regions based on the information about structure of the individual segmented regions, and generating a tomographic image of a subject by using the generated partial tomographic images for the individual segmented regions.

The present invention pertains to a system and method for X-ray imaging wherein a targeted fluence at the detector for projection images can be achieved at a plurality of projection angles around the imaging subject by control of exposure times implemented during image acquisition. Exposure time for a second projection image may be determined by the fluence in a first projection image, and in a third projection image by the fluence in a second projection image, where projection images are acquired within two degrees of one another. An acquisition parameter calculation can be configured to calculate acquisition parameters, such as said exposure times, to achieve the targeted fluence in projection images and can be coupled to a rotation controller that implements the acquisition parameters by controlling a relative angle between the imaging subject and X-ray image acquisition device.

A mirror for the EUV wavelength range (1) having a layer arrangement (P) applied on a substrate (S), the layer arrangement having a periodic sequence of individual layers, where the periodic sequence has at least two individual layers—forming a period—composed respectively of silicon (Si) and ruthenium (Ru). Also disclosed are a projection objective for microlithography (2) including such a mirror, and a projection exposure apparatus for microlithography having such a projection objective (2).

An X-ray arrangement is suitable to record absorption, phase contrast, and dark field images of an object. The visibility of low absorbing specimens is improved and required radiation dose is reduced. The assembly includes an X-ray source; two or more gratings; a position-sensitive detector with spatially modulated detection sensitivity; a recorder for recording the images; an evaluator for evaluating the intensities for each pixel to identify the characteristic of the object for each individual pixel as an absorption and/or a differential phase contrast and/or an x-ray scattering dominated pixel. Images are collected by rotating from 0 to n or 2n either the sample or the assembly. The gratings are produced with planar geometry. The X-rays pass through the gratings parallel to the substrate. The grating structures extend along the X-ray path which determines the phase shift. The attenuation of the X-rays caused by the grating structures is no longer given by the thickness, but by the length of the grating structures.

A press plate that includes: a plate shaped press portion that is capable of resilient deformation; a first slit that is provided to a first wall portion of a support body with length direction along a first edge portion of the press portion, and that penetrates the first wall portion; second slits that are provided to a second wall portions of the support body with length direction along second edge portions of the press portion, and that penetrate the second wall portions; and a first corner portion slit that is provided straddling a corner portion between the first wall portion and the second wall portion and penetrating the corner portion, that is connected to the first slit, and that is disposed at a separation to the second slit.

An X-ray photography apparatus including: a turning arm that supports an X-ray generator and an X-ray detector which are opposed to each other so that the head of a patient can be interposed therebetween, and a moving mechanism that includes a turning part and a moving part. The turning part turns the turning arm about a turning axis with respect to the head. The moving part moves the turning arm relative to the head in a direction perpendicular to the turning axis. The X-ray photography apparatus also includes: an image processor that generates an X-ray image, a photographic region designation part that designates part of a row of teeth along a dental arch as a pseudo intraoral radiography region, and an X-ray forming mechanism that changes the irradiation direction in which the head is irradiated with an X-ray relative to the axial direction of the body axis of the patient.

An X-ray photography apparatus including: a turning arm that supports an X-ray generator and an X-ray detector while the X-ray generator and the X-ray detector are opposed to each other so that a head of a patient can be interposed therebetween; and a moving mechanism that turns the turning arm about a turning axis with respect to the head and moves the turning arm in a direction perpendicular to the turning axis with respect to the head. The X-ray photography apparatus further includes: an image processor that generates an X-ray image based on an electric signal output from the X-ray detector; and a photographic region designation receiving part that designates part of a row of teeth along a dental arch as a pseudo intraoral radiography region. The image processor generates plural tomographic images by applying convolution and filtered back projection to X-ray image data obtained by pseudo intraoral radiography.

A method for recording a four-dimensional angiography data record using an x-ray facility with a C-arm is proposed. Projection images are recorded from different projection directions at different time points of the cardiac cycle. A number of three-dimensional reconstruction image data records assigned respectively to a time segment of the cardiac cycle are reconstructed from the projection images and combined to form the four-dimensional angiography data record by temporal assignment in respect of the cardiac cycle. At least one recording parameter describing the temporal sequence is selected when recording the projection images as a function of cardiac stimulation performed to ensure a stable heart rate during recording so that the recording of the projection images takes place in such a manner that it is synchronized with the cardiac cycle.

A method for obtaining multi-material decomposition images of an object is presented. The method includes acquiring an image pair from a dual energy computed tomography scan of the imaged object. The method then includes selecting a material basis for multi-material decomposition of the image pair. The method further includes applying a physicochemical model for the material basis. Also, the method includes performing multi-material decomposition using at least one constraint imposed by the physicochemical model.

A method of projection domain processing based on a local transform and shrinkage for use in reconstructing digital images from a set of projections, the method including providing a target image of a target object, providing projection data of the target object, producing filtered projection data by applying a sparsifying transform and a shrinkage function to the projection data, followed by an inverse of the sparsifying transform, producing a restored image by applying a reconstruction transform to the filtered projection data, comparing the restored image to the target image, and producing an optimized projection domain shrinkage function by adapting the shrinkage function to minimize differences between the restored image and the target image. Related apparatus and methods are also described.

A method is provided. The method includes acquiring a first dataset at a first energy spectrum and a second dataset at a second energy spectrum. The method also includes extracting a metal artifact correction signal using the first dataset and the second dataset or using a first reconstructed image and a second reconstructed image generated respectively from the first and the second datasets. The method further includes performing metal artifact correction on the first reconstructed image using the metal artifact correction signal to generate a first corrected image.

A method is disclosed for energy calibrating quantum-counting x-ray detectors in an x-ray installation including at least two x-ray systems turnable around a center of rotation. A target, for producing x-ray fluorescence radiation, is positioned between the first x-ray source and first x-ray detector and irradiated with x-radiation of the first x-ray source in such a way that x-ray fluorescence radiation which strikes the second x-ray detector from the target is produced by the x-radiation of the first x-ray source. The second x-ray detector is then energy calibrated by way of the x-ray fluorescence radiation of the target. The first x-ray detector can be energy calibrated in the same way with the aid of the x-radiation of the second x-ray source. With the proposed method, the x-ray detectors of a dual-source CT x-ray installation can be calibrated with little expenditure under conditions close to those of the system.

An image processing device of a computer tomography system includes an interface and a calibration data determiner. The interface is implemented to receive a first set of X-ray recordings of an object to be examined from first discrete recording angles and to receive a second set of X-ray recordings of the object to be examined from second discrete recording angles. The calibration data determiner is implemented to determine calibration data for the computer tomography system on the basis of the first set. The first set is further recorded during a first rotation run wherein the computer tomography system and the object to be examined rotate relative to each other, wherein the second set is recorded during at least a further rotation run after the first rotation run. On the basis of the calibration data and the first and second sets a computer tomography recording is reconstructable.

A compensation circuit 76 of an AEC unit 67 of an electronic cassette 13 defines the detection signal of a detection pixel 65 of the electronic cassette 13 as a detection signal corresponding to the detection signal of an old AEC sensor 25. The compensation circuit 76 performs compensation so as to exclude the influence on the detection signal due to a difference in the configuration of an intermediate member disposed between an X-ray source 10 and an FPD 35 of the electronic cassette 13 when the detection pixel 65 is used as an AEC sensor instead of the old AEC sensor 25. The detection signal is transmitted from a detection signal I/F 80 to a detection signal I/F 26 of a source control device 11 as it is (instantaneous value) or as an accumulated value obtained using an integration circuit 77.

Method for limiting an X-ray beam, wherein the X-ray beam is limited by a limiting unit comprising a couple of blades approaching each other or moving away from each other to adjust the width of a space between the blades the two blades being driven by an actuator (12) linked to both blades. The position of a symmetry axis (S) of the space between the blades is set in a shifting step by changing the distance between the blades and by impeding the motion of one blade in comparison with the motion of the other blade resulting in an asymmetric motion of the blades with respect to an initial position of the symmetry axis (S). The desired width (W) of the space between the blades is set in an adjustment step by an unimpeded symmetric motion of the blades with respect to the position of the symmetry axis (S) set in the shifting step.

The invention relates to an X-ray device comprising an x-ray sensitive camera for creating tomograms, especially panoramic tomograms. Means for creating 3D shots of a partial volume of the mandibular arch are also provided, said 3D shots being created especially by a second image receiver for creating a 2D shot and means for taking a plurality of 2D shots from different directions and creating a 3D shot therefrom, preferably according to conebeam technology with the associated reconstruction algorithms. The x-ray sensitive camera comprises a first x-ray sensitive image receiver for creating a tomogram, and a second x-ray sensitive image receiver for creating plane shots.

A cognitive disorder diagnostic system that employs cognitive cubes, gameplay associate with the cognitive cubes, and a data gathering as statistical analysis base device that may be a computer, that communicates the gathered data to a web server host according to a unique ID associated with particular cognitive cubes and further associated with a particular player. Using the statistical data gathered using the gameplay, various cognitive disorders may be successfully diagnosed and treated with higher reliability.

The present invention provides method and apparatus to perform combined cognitive and motor rehabilitation on a computerized non-portable system or on single portable device. A patient can play a variety of games that require the patient to perform a variety of memory exercises which involve physical exertion. The activities of the patient are monitored with pattern analysis software which provides feedback to the patient. The feedback can include voice synthesis, video guidance, progression messages etc. Patient data obtained while the patient is performing each of the memory exercises is stored locally on a database module and then uploaded to a cloud server. A remote psychologist/psychiatrist monitors the patient by logging into the same cloud, and updating cognition exercises. The same therapist can have live chats with the patient for further interaction and coaching.

A system to teach phonemic awareness uses a plurality of phonemes and a plurality of graphemes. Each phoneme is a unique sound and an indivisible unit of sound in a spoken language, and each grapheme is a written representation of one of the plurality of phonemes. A plurality of distinct graphical images and a plurality of unique names are provided where each unique name is associated with one of the graphical images and represents a grouping of graphemes selected from the plurality of graphemes. The system uses a plurality of sets of display pieces having a plurality of individual display pieces. Each individual display piece includes at least a portion of one of the graphical images and the graphemes from the grouping of graphemes constituting the associated unique name. A predefined instructional environment defines a predefined spatial context and predefined rules governing the acquisition and utilization of individual display pieces.

One embodiment relates to a feedback receiver (FBR). The FBR includes a FBR signal input configured to receive a radio frequency (RF) signal, a first local oscillator (LO) signal input configured to receive a first LO signal having an LO frequency, and a second LO signal input configured to receive a second LO signal having the LO frequency. The second LO signal is phase shifted by approximately 90° relative to the first LO signal. FBR also includes a divider that induces a time-varying phase shift in the first and second LO signals while concurrently retaining a 90° phase shift between the first and second LO signals.

A phase offset compensator for compensating a phase offset is provided. The phase offset includes a first phase sub-offset and a second phase sub-offset. The phase offset compensator includes a feedback loop comprising a first loop filter, the feedback loop being configured to compensate the first phase sub-offset of the phase offset, and a feed forward loop comprising a second loop filter, the feed forward loop being configured to compensate the second phase sub-offset of the phase offset.

Systems and methods for carrier phase recovery are provided. One method includes providing a reference signal, detecting an input signal and determining a Signal to Noise Ratio (SNR) of the input signal. The method also includes employing a Minimum Mean Square Error (MMSE) algorithm based on the SNR to determine a Carrier Phase Recovery Loop (CPRL) bandwidth.

In some embodiments, a method for processing output of at least one microphone of a device (e.g., a headset) to identify at least one touch gesture exerted by a user on the device, including by distinguishing the gesture from input to the microphone other than a touch gesture intended by the user, and by distinguishing between a tap exerted by the user on the device and at least one dynamic gesture exerted by the user on the device, where the output of the at least one microphone is also indicative of ambient sound (e.g., voice utterences). Other embodiments are systems for detecting ambient sound (e.g., voice utterences) and touch gestures, each including a device including at least one microphone and a processor coupled and configured to process output of each microphone to identify at least one touch gesture exerted by a user on the device.

A client-server computing system includes a server that has a virtual display driver that classifies and, if necessary, translates graphics application programming interface (API) functions to a cross-platform format. Classification involves determining whether the graphics command(s) are platform-specific and/or client-supported functions. After classification and translation, the graphics command(s) are marshaled and transmitted to a client via a network. The client includes a client display driver that executes the functions using a client 3D library and renders the resulting image data to a display.

A right circular cylindrical body of an isotropic dielectric such as a cross-linked styrene copolymer, has respective pluralities of mutually parallel grooves formed in its axial end faces, spaced apart by an intermediate portion whose dimension c is a half wavelength. The axial lengths a, b of the grooves are such that when a wave passes through the body, a quarter wavelength phase difference is produced between a component of a wave having its E-vector parallel to the grooves and a component of the wave having its E-vector orthogonal to the grooves. Alternatively the plate may consist of two or more discrete bodies whose grooves are dimensioned to produce a total differential phase shift of one quarter wavelength.

A mobile device case includes a reel assembly, including a reel, a supporting plate, and a hub between the reel and the supporting plate. The hub includes a first cavity between the hub and the supporting plate for housing a spring, and a second cavity between the hub and the reel for housing a flat flexible cable (FFC). The spring is wound in a first direction, while the FFC is wound in a second direction. The FFC includes a first end for electrically coupling to a female jack connector of a device. A female connector is electrically coupled to a second end of the FFC for engaging a male jack connector of user-provided headphones. When the reel rotates in the first direction, the spring tightens and the FFC loosens. When the reel rotates in the second direction, the spring loosens and the FFC tightens.

Controlling a power system in a mining truck includes receiving data indicative of an expected change in suitability of the mining truck for on-trolley operation, and outputting a control command to an actuating mechanism for a pantograph responsive to the data and prior to occurrence of the expected suitability change. A mining truck and power system are further provided, wherein a pantograph having an electrical contactor is adjusted between a first configuration contacting an overhead trolley line, and a rest configuration, responsive to data indicative of the expected suitability change.

A pantograph assembly configured to transfer electrical power from an overhead conductor to a machine. The pantograph assembly includes a pantograph support detachably connected to the machine, an articulated assembly, a pan rail and a carbon brush. The pantograph support includes a first link, and a second link hingedly connected to the first link. The first link is connected to the pantograph support. The pan rail is supported by the second link of the articulated assembly. The carbon brush is supported by the pan rail along a longitudinal axis of the pan rail. The pantograph assembly further includes an end horn having a bridge portion connected to the carbon brush. The bridge portion is configured to transfer the overhead conductor between the end horn and the carbon brush.

Pharmaceutical product dispensers (e.g., in the shape of a common ink pen) are operable to indicate information regarding a dosing schedule of a pharmaceutical product dispensable from the dispenser. Embodiments of the dispensers may include a plurality of dosing segments, each corresponding to a different dose of the pharmaceutical product. Actuation of an actuator may result in interaction between the actuator and the pharmaceutical product storage area such that a dose of pharmaceutical product contained in the pharmaceutical product storage area is dispensed, along with a corresponding advancement of the plurality of dosing segments. The dispenser may also include one or more locks to prevent unauthorized access to the pharmaceutical product (e.g., by a child or the like). Furthermore, the pharmaceutical product dispenser may include a disabling mechanism to permanently disable actuation of the actuator of the dispenser.

In a preferred embodiment, an Automated Pharmacy Admixture System (APAS) may include a manipulator system to transport medical containers such as bags, vials, or syringes in a compounding chamber regulated to a pressure below atmospheric pressure. In a preferred implementation, the manipulator system is configured to grasp and convey syringes, IV bags, and vials of varying shapes and sizes from a storage system in an adjacent chamber regulated at a pressure above atmospheric pressure. Various embodiments may include a controller adapted to actuate the manipulator system to bring a fill port of an IV bag, vial, or syringe into register with a filling port at a fluid transfer station in the chamber. A preferred implementation includes a sanitization system that can substantially sanitize a bung on a fill port of a vial or IV bag in preparation for transport to the fluid transfer station.

A sharpener for sharpening a pencil, in particular a cosmetic pencil, is especially suitable, when used correctly, for producing a particularly uniform outer jacket edge in the region of the pencil tip. The sharpener includes a sharpener body, in which a pencil guide channel is provided. The pencil guide channel has a circular cone-shaped channel section and opens out in a pencil inlet opening on the outer side of the sharpener body. A paring blade is positioned tangentially to the lateral surface of the channel section. The paring blade serves to pare off a pencil tip, which includes a front lead section and a rear outer jacket section. A shaping tool cuts a shoulder into the pencil tip, the shoulder being set back in relation to a circular cone-shaped enveloping surface of the pencil tip. The shaping tool is arranged relative to the pencil guide channel to insert the shoulder into the transition between the lead section and the outer jacket section of the pencil tip.

This technology is a method and apparatus for the semi-continuous measurement of the concentration of constituents of airborne particles which couples a laminar flow, water condensation particle collector to a microfluidic device for assay of particle chemical composition by electrophoresis. The technology has been used for the assay of sulfates, nitrates, chlorides, and organic acids contained in fine and submicrometer atmospheric particles. For these compounds the apparatus and method described is capable of one-minute time resolution at concentrations at the level of micrograms of analyte species per cubic meter of air. Extension to other analytes is possible.

An electrode assembly for capillary electrophoresis (CE) comprises a manifold (310), a connector (305) a sheath (300), and a seal (325). A capillary tube (100) passes through the manifold, the connector, the sheath, and the seal, stopping just beyond the end of the sheath. The sheath is fillable with water (330) or another fluid that cools the capillary tube in the vicinity of the electrode, thereby preventing degradation of a sample due to heat. The sheath may be metal or plastic with a metal sleeve electrode on its exterior. The sheath is sufficiently strong to penetrate a rubber or other pierceable cap on a vial. The manifold and connector incorporate an air path (605, 312, 307) so that when the electrode is fully inserted into a vial, the contents (650) of the vial are at atmospheric pressure (or another applied pressure or vacuum).