tri

Dielectric thin film-forming composition, method of forming dielectric thin film and dielectric thin film formed by the method

A liquid composition is provided for forming a thin film in the form of a mixed composite metal oxide in which a composite oxide B containing copper (Cu) and a composite oxide C containing manganese (Mn) are mixed into a composite metal oxide A represented with the general formula: Ba1-xSrxTiyO3, wherein the molar ratio B/A of the composite oxide B to the composite metal oxide A is within the range of 0.002




tri

Dielectric composition and preparation method thereof

There are provided a dielectric composition and a preparation method thereof, the dielectric composition including: a first perovskite powder for a core represented by ABO3: and a second perovskite powder for a shell represented by ABO3, having an average particle diameter corresponding to ⅓ to 1/10 of an average particle diameter of the first perovskite powder, and included in an amount of 1 to 70 parts by weight with respect to 100 parts by weight of the first perovskite powder, wherein particles of the second perovskite powder have pores having a volume fraction of 3 to 50 vol % therein. According to the present invention, there are provided a dielectric composition having excellent dielectric characteristics and electrical characteristics, and a preparation method thereof.




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Dielectric ceramic material and multilayer ceramic capacitor using the same

A dielectric ceramic material comprises a primary component of barium titanate (BaTiO3) and at least one additive component. The additive component has a mole percentage from 1% to 50% and is selected from the group consisting of lithium tantalite (LiTaO3), barium cerate (BaCeO3), sodium metaniobate (NaNbO3) and the combinations thereof.




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Dielectric composition and ceramic electronic component including the same

There is provided a dielectric composition including: a base powder including BaTiO3; a first accessory component including a content (x1) of 0.1 to 1.0 at % of an oxide or a carbonate including transition metals, based on 100 moles of the base powder; a second accessory component including a content (y) of 0.01 to 3.0 at % of oxide or carbonate including a fixed valence acceptor element, based on 100 moles of the base powder; a third accessory component including an oxide or a carbonate including a Ce element (content of z at %) and at least one rare earth element (content of w at %); and a fourth accessory component including a sintering aid, wherein 0.01≦z≦x1+4y and 0.01≦z+w≦x1+4y based on 100 moles of the base powder.




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Avoiding processing flaws in a computer processor triggered by a predetermined sequence of hardware events

A system, method and computer program product for avoiding a processing flaw in a computer processor triggered by a predetermined sequence of hardware events. The system may include a detecting unit and a power-on reset unit. The detecting unit detects that the predetermined sequence of hardware events is going to occur at the computer processor. The power-on reset unit initializes the computer processor to a state stored in computer memory in response to detecting the sequence of hardware events.




tri

Banking of reliability metrics

In one embodiment, a processor includes at least one functional block and banking logic. The banking logic may be to determine an average reliability metric associated with the at least one functional block. The banking logic may also be to, if the average reliability metric exceeds a required level, implement a reduced reliability mode in the at least one functional block, where the reduced reliability mode is associated with a reduction in the average reliability metric. Other embodiments are described and claimed.




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Distributed ECC engine for storage media

Embodiments of the present invention relate to an apparatus, method, and/or sequence for a distributed ECC that may be used in a storage system. In another embodiment of the invention, an apparatus for handling distributed error correction code (ECC) operations, includes: a plurality of ECC engines configured to perform ECC operations in parallel on multiple data parts; the plurality of ECC engines distributed in parallel to receive some of the multiple data parts that are read from storage media devices and to receive some of the other multiple data parts that are to be written to the storage media devices; and the plurality of ECC engines configured to use respective ECC bytes corresponding to respective ones of the multiple data parts.




tri

Parity error recovery method for string search CAM

Data is compressed using content addressable memory without disruption despite error using a plurality of content addressable memories to detect sequentially repeating data elements of the data. Compression information is generated for each sequence of repeating data elements that repeat for at least a compression threshold without any one of the plurality of content addressable memories generating an indication of an error for a matching content addressable memory entry. Individual data elements are output for each of the data elements that do not repeat for the compression threshold. Compression information is generated for each sequence of repeating data elements that repeat for at least the compression threshold and then generating a currently searched data element that matches the repeating data elements when any one of the plurality of content addressable memories generates an indication of an error for a content addressable memory entry that matches the currently searched data element.




tri

Apparatus and method for the granulation of radioactive waste, and vitrification method thereof

An apparatus and method for the granulation of radioactive waste in which a preprocessing method for the vitrification of radioactive waste is simplified to conform to onsite conditions of a nuclear power plant, additives are improved, and pellets suitable for vitrification are manufactured. The apparatus for the granulation of radioactive waste includes: a body frame having an inlet and an outlet; a hopper supplying the radioactive waste to be transferred and fed through the inlet; a feeder transferring/supplying the radioactive waste supplied to a specific position and in a certain quantity; a stirrer pulverizing/mixing lumps of the radioactive waste supplied; an additive supply part supplying a lubricant to the radioactive waste fed into the stirrer; and a pellet press pressing the radioactive waste fed through the feeder into a pellet shape and discharging the pellet through the outlet.




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Mitigation of secondary phase formation during waste vitrification

A method for vitrification of waste to reduce the formation of persistent secondary phases comprising separating at least one glass frit constituent from an initial glass frit to form a modified glass frit. The waste, modified glass frit, and the at least one glass frit constituent are mixed together with the modified glass frit and the at least one glass frit constituent being added as separate components. The resulting mixture is vitrified.




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Method for limiting the degassing of tritiated waste issued from the nuclear industry

A method and device for limiting the degassing of tritiated waste issued from the nuclear industry are provided. The method reduces an amount of generated tritiated hydrogen (T2 or HT) and/or tritiated water (HTO or T2O) including at least one piece of tritiated waste from the nuclear industry. The method includes placing the package in contact with a mixture including manganese dioxide (MnO2) combined with a component that includes silver; and placing the package in contact with a molecular sieve.




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Method and apparatus for distributing objects

A method and apparatus for distributing objects. In one embodiment, the method comprises computing a modulus operand based on a number of objects to be distributed and a number of objects pertaining to a first category; computing a modulus operation based on a number of distributed objects and the modulus operand; and distributing a first object or a second object based on a result of computing the modulus operation.




tri

Method and apparatus for a geographically determined Jewish religious clock and electrical device combination with holiday and preference modes

An independently functioning or centrally controlled wall light switch is configured to operate in normal mode and a Jewish holiday mode wherein the state of the light is fixed, regardless of the user's physical manipulation of the light switch. The control system automatically activates holiday mode by combining a geographically determined Jewish religious clock executed by software and hardware that utilizes the current time, date and geographical location of the apparatus in accordance with the Jewish definition of time and laws for calculating numerous religiously significant shifting daily points in time. The control system further incorporates several energy saving and preference modes by utilizing a particular day's calculated religious points in time in conjunction with holiday behavior patterns common to most Jewish families to provide the user with a greatly simplified means of programming an automatically adjusting on/off light timer and dimming overlay functionality during holiday mode.




tri

Distributed processing system and method for discrete logarithm calculation

Distributed processing system and method for discrete logarithm calculation. The speed and resource efficiency of discrete logarithm calculation may be improved by allowing a plurality of operation agents to distributively process an operation of generating a modulo multiplication auxiliary table, an operation of generating a pre-calculation table, and an operation of searching for an answer by applying an iterated function for discrete logarithm calculation in a discrete logarithm calculation operation using the pre-calculation table.




tri

Determination of physical connectivity status of devices based on electrical measurement

Embodiments of the invention are generally directed to determination of physical connectivity status of devices based on electrical measurement. An embodiment of a method includes discovering a connection of a first device with a second device, and performing an electrical measurement of the second device by the first device via the connection between the first device and the second device, where performing the electrical measurement includes sensing by the first device of an element of the second device. The method further includes, if the sensing by the first device fails to detect the element of the second device and a predetermined condition for the electrical measurement is enabled, then determining by the first device that the connection with the second device has been lost.




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Reducing cross queue synchronization on systems with low memory latency across distributed processing nodes

A method for efficient dispatch/completion of a work element within a multi-node data processing system. The method comprises: selecting specific processing units from among the processing nodes to complete execution of a work element that has multiple individual work items that may be independently executed by different ones of the processing units; generating an allocated processor unit (APU) bit mask that identifies at least one of the processing units that has been selected; placing the work element in a first entry of a global command queue (GCQ); associating the APU mask with the work element in the GCQ; and responsive to receipt at the GCQ of work requests from each of the multiple processing nodes or the processing units, enabling only the selected specific ones of the processing nodes or the processing units to be able to retrieve work from the work element in the GCQ.




tri

Apparatus and methods for adaptive thread scheduling on asymmetric multiprocessor

Techniques for adaptive thread scheduling on a plurality of cores for reducing system energy are described. In one embodiment, a thread scheduler receives leakage current information associated with the plurality of cores. The leakage current information is employed to schedule a thread on one of the plurality of cores to reduce system energy usage. On chip calibration of the sensors is also described.




tri

Two-tiered dynamic load balancing using sets of distributed thread pools

By employing a two-tier load balancing scheme, embodiments of the present invention may reduce the overhead of shared resource management, while increasing the potential aggregate throughput of a thread pool. As a result, the techniques presented herein may lead to increased performance in many computing environments, such as graphics intensive gaming.




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Process for producing 1,2-dichloro-3,3,3-trifluoropropene

Disclosed is a process for producing 1,2-dichloro-3,3,3-trifluoropropene, which is characterized by that 1-halogeno-3,3,3-trifluoropropene represented by the general formula [1]: (In the formula, X represents a fluorine atom, chlorine atom or bromine atom.) is reacted with chlorine in a gas phase in the presence of a catalyst. It is possible by this process to produce 1,2-dichloro-3,3,3-trifluoropropene in an industrial scale with good yield by using 1-halogeno-3,3,3-trifluoropropene, which is available with a low price, as the raw material.




tri

Production method for 1-chloro-3,3,3-trifluoropropene

A production method of 1-chloro-3,3,3-trifluoropropene according to the present invention includes reaction of 1,1,1,3,3-pentachloropropane with hydrogen fluoride, characterized in that the concentrations of respective catalytic components in the 1,1,1,3,3-pentachloropropane as the raw material is controlled to a predetermined level or less. By controlling the concentrations of the respective catalytic components in the 1,1,1,3,3-pentachloropropane to the predetermined level or less, it is possible to improve the problems of shortening of catalyst life, retardation of reaction and scaling or corrosion of equipment in the production of the 1-chloro-3,3,3-trifluoropropene. In addition, the 1,1,1,3,3-pentachloropropane can be obtained selectively with high yield by telomerization reaction of carbon tetrachloride and vinyl chloride. The present invention is thus useful as the method for industrially advantageous, high-yield production of the 1-chloro-3,3,3-trifluoropropene.




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Methods for producing 1-chloro-3,3,3-trifluoropropene from 2-chloro-3,3,3-trifluoropropene

The present invention provides processes for the production of HCFO-1233zd, 1-chloro-3,3,3-trifluoropropene, from the starting material, 2-chloro-3,3,3-trifluoropropene (HCFO-1233xf). In a first process, HCFO-1233zd is produced by the isomerization of HCFO-1233xf. In a second process, HCFO-1233zd is produced in a two-step procedure which includes (i) dehydrochlorination of HCFO-1233xf into trifluoropropyne; and (ii) hydrochlorination of the trifluoropropyne into HCFO-1233zd.




tri

Integrated process for the production of 1-chloro-3,3,3-trifluoropropene

The present invention is directed to processes for the production of 1233zd from 240fa and HF, with or without a catalyst, at a commercial scale. The 240fa and HF are fed to a reactor operating at high pressure. The resulting product stream comprising 1233zd, HCl, HF, and other byproducts is treated to one or more purification techniques including phase separation and one or more distillations to provide purified 1233zd, which meets commercial product specifications, i.e., having a GC purity of 99.5% or greater.




tri

Catalytic gas phase fluorination of 1,1,2-trichloroethane and/or 1,2-dichloroethene to produce 1-chloro-2,2-difluoroethane

The invention is directed to a catalyst for the gas phase fluorination of 1,1,2-trichloroethane and/or 1,2-dichloroethene with HF to give 1-chloro-2,2-difluoroethane which catalyst is prepared by co-depositing FeCl3 and MgCl2 on chromia-alumina, or co-depositing Cr(NO3)3 and Ni(NO3)2 on active carbon, or by doping alumina with ZnCl2, and to a process for the preparation of 1-chloro-2,2-difluoroethane comprising a catalytic gas phase fluorination of 1,1,2-trichloroethane and/or 1,2-dichloroethene wherein one of the catalysts according to claim 2 or 3 is used.




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Methods for the synthesis of 13C labeled iodotridecane and use as a reference standard

A method for preparing 13C labeled iodotridecane represented by Formula A: The method comprises the conversion of 13C labeled propargyl alcohol to 13C labeled iodotridecane via alkylation of propargyl alcohol with iododecane.




tri

Reactor and agitator useful in a process for making 1-chloro-3,3,3-trifluoropropene

Disclosed is a reactor and agitator useful in a high pressure process for making 1-chloro-3,3,3-trifluoropropene (1233zd) from the reaction of 1,1,1,3,3-pentachloropropane (240fa) and HF, wherein the agitator includes one or more of the following design improvements: (a) double mechanical seals with an inert barrier fluid or a single seal;(b) ceramics on the rotating faces of the seal;(c) ceramics on the static faces of seal;(d) wetted o-rings constructed of spring-energized Teflon and PTFE wedge or dynamic o-ring designs; and(e) wetted metal surfaces of the agitator constructed of a corrosion resistant alloy.




tri

Process for 1-chloro-3,3,3-trifluoropropene from trifluoromethane

The present invention provides routes for making 1-chloro-3,3,3-trifluoropropene (HCFO-1233zd) from commercially available raw materials. More specifically, this invention provides routes for HCFO-1233zd from inexpensive and commercially available trifluoromethane (HFC-23).




tri

Process for 1-chloro-3,3,3-trifluoropropene from trifluoropropene

The present invention provides routes for making 1-chloro-3,3,3-trifluoropropene (HCFO-1233zd) from commercially available raw materials. More specifically, this invention provides several routes for forming HCFO-1233zd from 3,3,3-trifluoropropene (FC-1234zf).




tri

Method of synthesizing bulk transition metal carbide, nitride and phosphide catalysts

A method for synthesizing catalyst beads of bulk transmission metal carbides, nitrides and phosphides is provided. The method includes providing an aqueous suspension of transition metal oxide particles in a gel forming base, dropping the suspension into an aqueous solution to form a gel bead matrix, heating the bead to remove the binder, and carburizing, nitriding or phosphiding the bead to form a transition metal carbide, nitride, or phosphide catalyst bead. The method can be tuned for control of porosity, mechanical strength, and dopant content of the beads. The produced catalyst beads are catalytically active, mechanically robust, and suitable for packed-bed reactor applications. The produced catalyst beads are suitable for biomass conversion, petrochemistry, petroleum refining, electrocatalysis, and other applications.




tri

System for accessing a register file using an address retrieved from the register file

A data processing system and method are disclosed. The system comprises an instruction-fetch stage where an instruction is fetched and a specific instruction is input into decode stage; a decode stage where said specific instruction indicates that contents of a register in a register file are used as an index, and then, the register file pointed to by said index is accessed based on said index; an execution stage where an access result of said decode stage is received, and computations are implemented according to the access result of the decode stage.




tri

Information processing apparatus for restricting access to memory area of first program from second program

A processor determines whether a first program is under execution when a second program is executed, and changes a setting of a memory management unit based on access prohibition information so that a fault occurs when the second program makes an access to a memory when the first program is under execution. Then, the processor determines whether an access from the second program to a memory area used by the first program is permitted based on memory restriction information when the fault occurs while the first program and the second program are under execution, and changes the setting of the memory management unit so that the fault does not occur when the access to the memory area is permitted.




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Software modification methods to provide master-slave execution for multi-processing and/or distributed parallel processing

In one embodiment of the invention, a method is disclosed for modifying a pre-existing application program for multi-processing and/or distributed parallel processing. The method includes searching an application program for a computational loop; analyzing the computational loop to determine independence of the computational transactions of the computational loop; and replacing the computational loop with master code and slave code to provide master-slave execution of the computational loop in response to analyzing the computational loop to determine independence of the computational transactions of the computational loop. Multiple instances of the modified application program are executed to provide multi-processing and/or distributed parallel processing.




tri

4(3)-(4-hydroxy-4-methylpentyl)-3-cyclohexene-1-carbonitrile

A compound and a fragrance composition containing the same are provided, wherein the compound has a citrus odor in addition to a muguet odor, which is useful as a fragrance, is stable in an aqueous vehicle, and can provide a bright muguet odor with good fragrance retention by being blended with another fragrance. Particularly, they are 4(3)-(4-hydroxy-4-methylpentyl)-3-cyclohexene-1-carbonitrile and a fragrance composition containing 4(3)-(4-hydroxy-4-methylpentyl)-3-cyclohexene-1-carbonitrile.




tri

Method for preparing 3-trifluoromethyl chalcones

Disclosed is a method for preparing a compound of Formula 1 wherein Q and Z are as defined in the disclosure comprising distilling water from a mixture comprising a compound of Formula 2, a compound of Formula 3, a base comprising at least one compound selected from the group consisting of alkaline earth metal hydroxides of Formula 4 wherein M is Ca, Sr or Ba, alkali metal carbonates of Formula 4a wherein M1 is Li, Na or K, 1,5-diazabicyclo[4.3.0]non-5-ene and 1,8-diazabicyclo[5.4.0]undec-7-ene, and an aprotic solvent capable of forming a low-boiling azeotrope with water. Also disclosed is a method for preparing a compound of Formula 2 comprising (1) forming a reaction mixture comprising a Grignard reagent derived from contacting a compound of Formula 5 wherein X is Cl, Br or I with magnesium metal or an alkylmagnesium halide in the presence of an ethereal solvent, and then (2) contacting the reaction mixture with a compound of Formula 6 wherein Y is OR11 or NR12R13, and R11, R12 and R13 are as defined in the disclosure. Further disclosed is a method for preparing a compound of Formula 7 wherein Q and Z are as defined in the disclosure, using a compound of Formula 1 characterized by preparing the compound of Formula 1 by the method disclosed above or using a compound of Formula 1 prepared by the method disclosed above.




tri

Optical resolution methods for bicyclic compounds using asymmetric catalysts

An optically active bicyclic compound is efficiently produced by optical resolution using an optically active amine.




tri

Control device and control method for electric powered vehicle

In an electric powered vehicle in which vehicle driving force for reverse running is produced by a traction motor, vehicle driving force is set by a product of a base value set at least based on an accelerator opening and an amplification factor. The amplification factor is set at k1=1.0 during reverse running (V1.0 at the start of reverse running (V≧0) depending on the vehicular speed. The vehicle driving force at the start of reverse running can thereby be made larger than the vehicle driving force after the start of reverse running at the same accelerator opening.




tri

Integrated circuit floorplan for compact clock distribution

An integrated circuit includes core logic and a plurality of interface blocks disposed about a periphery of the core logic. A plurality of input or output (I/O) circuits is assigned to one of the plurality of interface blocks. The I/O circuits include external I/O circuits coupled to a device other than the integrated circuit and internal I/O circuits coupled to the integrated circuit. Each interface block includes a first plurality of I/O circuits disposed on a first side of the interface block and a second plurality of I/O circuits disposed on a second side of the interface block. Each interface block also includes interface logic for the interface block between the first plurality of I/O circuits and the second plurality of I/O circuits, and a logic hub that includes a clock distribution of minimal length that drives launch logic and capture logic to form the I/O circuits of the interface block.




tri

Metal conservation with stripper solutions containing resorcinol

Resist stripping agents useful for fabricating circuits and/or forming electrodes on semiconductor devices for semiconductor integrated circuits and/or liquid crystals with reduced metal and metal alloy etch rates (particularly copper etch rates and TiW etch rates), are provided with methods for their use. The preferred stripping agents contain low concentrations of resorcinol or a resorcinol derivative, with or without an added copper salt, and with or without an added amine to improve solubility of the copper salt. Further provided are integrated circuit devices and electronic interconnect structures prepared according to these methods.




tri

Superconducting direct-current electrical cable

A superconductive electrical direct current cable with at least two conductors insulated relative to each other is indicated, where the cable is placed with at least two conductors insulated relative to each other, where the conductors are arranged in a cryostat suitable for guidance of the cooling agent, wherein the cryostat is composed of at least one metal pipe which is surrounded by a circumferentially closed layer with thermally insulating properties. In the cryostat is arranged a strand-shaped carrier composed of insulating material, where the carrier has at least two diametrically oppositely located outwardly open grooves in each of which is arranged one of the conductors. Each conductor is composed of a plurality of superconductive elements.




tri

Superconducting rotating electrical machine and manufacturing method for high temperature superconducting film thereof

The present disclosure relates to a superconducting rotating electrical machine and a manufacturing method for a high temperature superconducting film thereof. The superconducting rotating electrical machine includes a stator, and a rotor rotatable with respect to the stator, the rotor having a rotary shaft and a rotor winding. Here, the rotor winding includes tubes disposed on a circumference of the rotary shaft and each forming a passage for a cooling fluid therein, superconducting wires accommodated within the tubes, and a cooling fluid flowing through the inside of the tubes. This configuration may allow for direct heat exchange between the superconducting wires and a refrigerant, resulting in improvement of heat exchange efficiencies of the superconducting wires.




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Additive manufacturing method for SRF components of various geometries

An additive manufacturing method for forming nearly monolithic SRF niobium cavities and end group components of arbitrary shape with features such as optimized wall thickness and integral stiffeners, greatly reducing the cost and technical variability of conventional cavity construction. The additive manufacturing method for forming an SRF cavity, includes atomizing niobium to form a niobium powder, feeding the niobium powder into an electron beam melter under a vacuum, melting the niobium powder under a vacuum in the electron beam melter to form an SRF cavity; and polishing the inside surface of the SRF cavity.




tri

Electricity transmission cooling system

A cooling system includes a first section of high temperature superconducting (HTS) cable configured to receive a first flow of coolant and to permit the first flow of coolant to flow therethrough. The system may further include a second section of high temperature superconducting (HTS) cable configured to receive a second flow of coolant and to permit the second flow of coolant to flow therethrough. The system may further include a cable joint configured to couple the first section of HTS cable and the second section of HTS cable. The cable joint may be in fluid communication with at least one refrigeration module and may include at least one conduit configured to permit a third flow of coolant between said cable joint and said at least one refrigeration module through a coolant line separate from said first and second sections of HTS cable.




tri

Comparison of character strings

A computer-readable, non-transitory medium storing a character string comparison program is provided. The program causes, when executed by a computer, the computer to perform a process including splitting a first character string and a second character string into words; acquiring information including a semantic attribute that represents a semantic nature of each of the words and a conceptual code that semantically identifies said each of the words, from a storage device; identifying a pair of the words having a common semantic attribute between the first character string and the second character string; comparing the conceptual codes of the specified pair of the words between the first character string and the second character string; and generating a comparison result between the first character string and the second character string based upon a comparison result of the conceptual codes.




tri

Biometric voice command and control switching device and method of use

A biometric voice command and control switching device has a microphone assembly for receiving a currently spoken challenge utterance and a reference utterance, and a voice processing circuit for creating electronic signals indicative thereof. The device further includes a memory for storing the electronic signals, and a processor for comparing the electronic signals to determine if there is a match. If there is a match, an interface circuit enables the operable control of the controlled device.




tri

Service distribution device and service display device

A service distribution device is provided that, when acquiring services to be used in an information terminal mounted in a vehicle or used in its passenger compartment, recognizes service availability beforehand, thereby improving usability of the services. A service distribution device includes an information correlation unit for correlating information that denotes service utilization conditions in relation to travel condition of the vehicle with the services. The service distribution device distributes to an information terminal the information that denotes the service utilization conditions correlated by the information correlation unit along with contents of the relevant service so that the information and the contents can be visibly displayed on a display unit in the information terminal.




tri

Synthesis of and curing additives for phthalonitriles

A composition having a mixture of the below compounds having a mole ratio of at least 1:20. Ar1 and Ar2 are independently selected aromatic groups. A composition comprising phthalonitrile compounds that comprise at least 5 mol % of the first compound below. A method of: providing a solution of a dichloroaromatic compound having an electron-withdrawing group bound to each aromatic ring containing one of the chloride groups; a dihydroxyaromatic compound or anion thereof; an organic transition metal complex or a transition metal salt; an alkaline hydroxide base; and a solvent; and heating the solution to a temperature at which the dichloroaromatic compound and the dihydroxyaromatic compound react to form a dimetallic salt of an aromatic ether oligomer. The molar ratio of the dihydroxyaromatic compound to the dichloroaromatic compound is greater than 2:1. Water formed during the heating is concurrently distilled from the solution.




tri

Process of producing phosphinothricin employing nitrilases

The present invention generally relates to processes for the enzymatic production of a phosphinothricin product or precursor thereof from a nitrile-containing substrate.




tri

Point of use generation of amyl nitrite

The present disclosure relates to devices and methods for the preparation of amyl nitrite formulations at a point of use location from relatively shelf-stable reagents employing acidic cationic exchange resins.




tri

Process for preparing triorgano borates with low alcohol content

The present invention provides a process for preparing triorgano borates with low alcohol content.




tri

Method for producing silica-supported catalyst, and method for producing unsaturated carboxylic acid or unsaturated nitrile

A method for producing a silica-supported catalyst comprising Mo, V. Nb, and a component X (Sb and/or Te) to be used in a vapor phase catalytic oxidation or ammoxidation of proprane, comprising the steps of: (I) preparing a raw material mixture solution by mixing Mo, V, Nb, component X, a silica sol, and water;(II) obtaining a dry powder by drying the raw material mixture solution; and(III) obtaining a silica-supported catalyst by calcining the dry powder, wherein the silica sol contains 10 to 270 wt ppm of nitrate ions based on SiO2.




tri

Crystalline form of 3-methylsulfonylpropionitrile

The present invention relates to processes for preparing 3-methylsulfonylpropionitrile. The processes provide a good yield and a good purity of the final product and provide a controllable reaction. The present invention also relates to a crystalline form of 3-methylsulfonylpropionitrile having X-ray diffraction peaks at 13.9±0.1, 19.2±0.1, 20.0±0.1, 22.5±0.1, 23.2±0.1, 25.7±0.1, 28.1±0.1, 29.9±0.1, and 30.6±0.1 degrees 2θ, and wherein the most intense peak is the peak at 13.9±0.1 degrees 2θ.